EP 0866781 A1 19980930 - PROCESS FOR PRODUCING SINTERED SILICIUM NITRIDE
Title (en)
PROCESS FOR PRODUCING SINTERED SILICIUM NITRIDE
Title (de)
VERFAHREN ZUR HERSTELLUNG VON GESINTERTEM SILICIUMNITRID
Title (fr)
PROCEDE POUR PRODUIRE DU NITRURE DE SILICIUM FRITTE
Publication
Application
Priority
- DE 19546238 A 19951212
- EP 9605571 W 19961212
Abstract (en)
[origin: DE19546238A1] By providing a new production process for sintered silicium nitride, the present invention takes into account that parts made of Si3N4 material are often used in temperature ranges below 1200 DEG C, and sometimes even below 500 DEG C, and therefore need not be designed for temperatures above 1200 DEG C. A thus adapted material is obtained by sintering a silicium nitride powder of less than 2 mu m with 5 to 20 % by weight of one or several glass components having particles of the same size at temperatures below 1400 DEG C. It is essential that the glass components used, preferably alkali borate glasses, with a heat expansion coefficient alpha that matches the Si3N4, have a transformation point Tg below 750 DEG C, and that the individual glass elements have a free enthalpy DELTA G equal to at least 60 % of the free enthalpy of SiO2. Such economically produced Si3N4 parts most satisfactorily meet material quality requirements for low temperature uses, such as density, solidity and beta -phase proportion.
IPC 1-7
IPC 8 full level
C03C 10/02 (2006.01); C03C 14/00 (2006.01); C04B 35/584 (2006.01)
CPC (source: EP US)
C03C 14/004 (2013.01 - EP US); C04B 35/584 (2013.01 - EP US)
Citation (search report)
See references of WO 9721644A1
Designated contracting state (EPC)
DE FR GB IT
DOCDB simple family (publication)
DE 19546238 A1 19970619; EP 0866781 A1 19980930; US 5998319 A 19991207; WO 9721644 A1 19970619
DOCDB simple family (application)
DE 19546238 A 19951212; EP 9605571 W 19961212; EP 96943937 A 19961212; US 7773898 A 19980610