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EP-0320114-A1-19890614
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EP-0320114-A1-19890614
A faujasite polymorph has a silica to alumina mol ratio greater than 6, and contains tetrapropyl ammonium and/or tetrabutyl ammonium trapped within the supercages of said structure.A process for preparing the alumino�silicate comprises:(a) preparing a reaction mixture comprising an oxide of sodium, a tetrapropyl or tetra hydroxy�propyl (or similar tetrabutyl) organic ammonium salt, water, a source of silica, a source of alumina, and sodium aluminosilicate nucleating seeds, said reaction mixture having a composition, in terms of mole ratios of oxides, within the following ranges: (Na,T)₂O:Al₂O₃3 to 15SiO₂:Al₂O₃9 to 36H₂O:Al₂O₃120 to 500 where T represents the cation of the organic ammonium template, and said seeds being present in an amount to yield 0.1 to 10 mole percent of the total final alumina content in said aluminosilicate;(b) blending the reaction mixture suffi�ciently to form a substantially homogeneous mixture;(c) maintaining the reaction mixture at between about 90°C and 160°C under autogenous pressure for a sufficient period of time to form crystals of said aluminosilicate; and(d) recovering said aluminosilicate crys�tals.
A faujasite polymorph has a silica to alumina mol ratio greater than 6, and contains tetrapropyl ammonium and/or tetrabutyl ammonium trapped within the supercages of said structure.A process for preparing the alumino�silicate comprises:(a) preparing a reaction mixture comprising an oxide of sodium, a tetrapropyl or tetra hydroxy�propyl (or similar tetrabutyl) organic ammonium salt, water, a source of silica, a source of alumina, and sodium aluminosilicate nucleating seeds, said reaction mixture having a composition, in terms of mole ratios of oxides, within the following ranges: (Na,T)₂O:Al₂O₃3 to 15SiO₂:Al₂O₃9 to 36H₂O:Al₂O₃120 to 500 where T represents the cation of the organic ammonium template, and said seeds being present in an amount to yield 0.1 to 10 mole percent of the total final alumina content in said aluminosilicate;(b) blending the reaction mixture suffi�ciently to form a substantially homogeneous mixture;(c) maintaining the reaction mixture at between about 90°C and 160°C under autogenous pressure for a sufficient period of time to form crystals of said aluminosilicate; and(d) recovering said aluminosilicate crys�tals.
en
European Patent Office
EP0320114
EP 0320114
C01B 33/28
Faujasite-type zeolite and process for making it
Faujasite-type zeolite and process for making it - European Patent Office - EP 0320114 A1
Faujasite-type zeolite and process for making it - European Patent Office - EP 0320114 A1
Adobe PDF Library 8.0
"EP0320114"; "EP 0320114"; "C01B 33/28"; "Faujasite-type zeolite and process for making it"
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0320114
A1
1989-06-14
88310389
1988-11-04
US
122789
1987-11-19
C01B 33/28
Exxon Research and Engineering Company
Strohmaier, Karl Gottlieb
Vaughan, David Evan William
Faujasite-type zeolite and process for making it
Zeolith vom Faujasit-Typ und Verfahren zu dessen Herstellung
Faujasite-type zeolite and process for making it
Zéolite de type faujasite et son procédé de préparation
A faujasite polymorph has a silica to alumina mol ratio greater than 6, and contains tetrapropyl ammonium and/or tetrabutyl ammonium trapped within the supercages of said structure.A process for preparing the alumino�silicate comprises:(a) preparing a reaction mixture comprising an oxide of sodium, a tetrapropyl or tetra hydroxy�propyl (or similar tetrabutyl) organic ammonium salt, water, a source of silica, a source of alumina, and sodium aluminosilicate nucleating seeds, said reaction mixture having a composition, in terms of mole ratios of oxides, within the following ranges: (Na,T)₂O:Al₂O₃3 to 15SiO₂:Al₂O₃9 to 36H₂O:Al₂O₃120 to 500 where T represents the cation of the organic ammonium template, and said seeds being present in an amount to yield 0.1 to 10 mole percent of the total final alumina content in said aluminosilicate;(b) blending the reaction mixture suffi�ciently to form a substantially homogeneous mixture;(c) maintaining the reaction mixture at between about 90°C and 160°C under autogenous pressure for a sufficient period of time to form crystals of said aluminosilicate; and(d) recovering said aluminosilicate crys�tals.
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