[0001] The present invention relates to a spinneret plate provided with a spinning nozzle
which is most suitably employed in melt spinning such as the spinning of pitch carbon
fibers.
[0002] Hitherto, the spinning of materials such as pitch has been carried out using a spinneret
plate with a plurality of nozzle holes formed therein and arranged in circumferential
rows around the center of the plate. In order to satisfactorily melt-spin a fine fiber
over a long period of time, it is important that each nozzle hold provided in the
spinneret plate should be sufficiently small and have a smooth inner surface and a
uniform inner diameter, i.e., a uniform aspect ratio.
[0003] In the manufacture of such a spinneret plate the nozzle holes are generally formed
by boring through a nozzle plate using a drill or an electron beam. The method in
which boring is effected using a drill, however, encounters various problems as the
nozzle hole diameter decreases. The first of the problems is that it is difficult
to machine the nozzle holes to a high degree of accuracy. More specifically, the drill
itself has a tendency to oscillate when rotating. In addition, when drilling the nozzle
plate, the drill oscillates owing to drilling resistance, resulting in a hole which
had different diameters at the start of drilling and the end of drilling, as shown
in Fig. 1. Moreover, as the drill diameter is reduced, the edge of the drill blunts
faster, resulting in a marked reduction in drilling capacity. It is impossible to
grind the edge of such a small-diameter drill; hence, it is necessary to replace the
drill frequently. In addition, the frequency with which the drill breaks increases,
which not only lowers the drilling efficiency, but also increases the cost of manufacturing
the spinneret plate.
[0004] The electron beam method has been proposed in order to overcome these disadvantages
with the boring method using a drill. This method, however, has the disadvantage that
the electron beam remains inside the hole during the boring to form a hole whose inner
part is expanded, as shown in Fig. 2, so that a nozzle with such a hole would degrade
the orientation of the fiber.
Summary of the Invention
[0005] Accordingly, it is a primary object of the invention to provide a spinneret plate
which has a plurality of nozzles, each with a smooth inner surface as well as a uniform
hole diameter so that it is able to spin a fine fiber, such as a pitch carbon fiber,
over a long period of time.
[0006] It is another object of the invention to provide a method of manufacturing a spinneret
plate which makes it possible to manufacture a spinneret plate provided with a plurality
of nozzles, each with a smooth inner surface as well as a uniform hole diameter, at
an extremely high accuracy and a high efficiency within a short period of time.
[0007] The spinneret plate comprises a metal nozzle plate having at least one hole formed
therein and a metal hollow tube or pipe press fit mounted in said hole. The upper
and lower ends of the pipe are shaped to conform to the inlet and outlets of the nozzle
plate. The press fitting procedure may be achieved by heating the nozzle plate, preferably
composed of steel, inserting the hollow pipe, also preferably composed of steel, into
the hole, and thereafter cooling the plate thereby producing a pipe press fit mounted
in the nozzle plate hole.
Brief Description of the Drawings
[0008]
Figures 1 and 2 illustrate in cross section nozzles prepared in accordance with prior
art techniques.
Figures 3-5 illustrate in vertical cross section different embodiments of spinneret
plates of the present invention, with the same reference numerals representing corresponding
parts in the embodiments.
Figures 6-8 are drawings illustrating the sequential preparation of the spinneret
plates of the embodiments shown in Figs. 3-5.
Description of the Preferred Embodiments of the Invention
[0009] A spinneret plate 1 constructed in accordance with the present invention in the embodiment
shown in Fig. 3, comprises a nozzle plate 2 of a predetermined thickness, and a hollow
tube or pipe 4 of a desired diameter which is mounted in or attached to the nozzle
plate 2 by press fitting or the like, into a hole formed in the plate. The interior
of the pipe 4 defines the nozzle hole for the spinneret.
[0010] Preferably, the nozzle plate 2 is made of a stainless steel plate (SUS 304), and
typically has a thickness of 4 mm when melt spinning pitch carbon fibers or the like.
The hollow pipe 4 may also be made of a stainless steel and, by way of example, may
have the following sizes: inner diameter of 0.55 mm and an outer diameter of 1.5 mm.
In addition, although the nozzle holes formed by the hollow pipes 4 can be disposed
in any desired arrangement, they preferably are arranged in one or more concentric
rows in the circumferential direction around the center of nozzle plate 2, when a
melt spinning pitch carbon fibers, for example.
[0011] Spinneret plates la and lb in accordance with other embodiments of the invention
are illustrated in Figs. 4 and 5. In the spinneret plate la shown in Fig. 4, the hollow
pipe 4 mounted in nozzle plate 2, the pipe 4 does extend through the entire thickness
of the nozzle plate 2, but is provided through substantial portion (e.g., about half)
of the thickness of the nozzle plate 2 on the outlet side thereof. An enlarged, tapered
inlet 6 in the upstream side of the nozzle plate 2 guides the molten spinning material
into the nozzle hole defined by the hollow pipe 4.
[0012] The spinneret plate lb shown in Fig. 5 has a structure substantially similar to that
of the spinneret plate la of Fig. 4. The spinneret plate lb, however, differs from
the spinneret plate la in that the hollow pipe 4 projects slightly beyond the outlet
surface of the nozzle plate 2 so as to form a projecting nozzle. The spinneret plate
lb with such a projecting nozzle provides an excellent shedding effect between the
molten spinning material and the spinneret plate. In order to reinforce the projecting
part of the hollow pipe 4 on the outlet side of the nozzle plate 2, it is preferable
to secure the projecting part to the nozzle plate 2 by forming brazed reinforcing
shoulders 8.
[0013] Spinneret plates 1, la, and 1b may be manufactured by processes which will be described
with reference to the sequential drawings of Fig. 6, 7 and 8.
[0014] Referring first to Fig. 6, the nozzle plate 2 is provided with a preliminary hole
4' bored at the position at which the spinning nozzles is to be formed, as illustrated
in 6(a). The hollow pipe 4 is press-fitted into the prepared hole 4', as illustrated
in 6(b). The press-fitting operation may be carries out as follows. When a stainless
steel pipe with an outer diameter of 1.5 mm and an inner diameter of 0.55 mm, for
example, is employed as the hollow pipe 4, the preliminary hole 4' is finished so
as to have an inner diameter of 1.5 mm, and the nozzle plate 2 is heated to between
150 and 300°C to expand the hole slightly. The hollow pipe 4 is maintained at room
temperature, or is cooled at lower temperature and is inserted into the preliminary
hole 4', and then the nozzle plate 2 is cooled resulting in an interference fit. Subsequently,
if the hollow pipe 4 projects from the nozzle plate 2, the projecting parts of the
hollow pipe 4 are ground so that the end of the hollow pipe 4 is flush with the upper
and lower surfaces of the nozzle plate 2, as illustrated in 6(c).
[0015] Fig. 7 illustrates the method of manufacturing the spinneret plate of Fig. 4. In
this embodiment, the preliminary hole illustrated in 7(a) formed in the nozzle plate
2 may be formed: by drilling a small-diameter part 4' through the plate 2 and then
enlarging the inlet side of the hole at 4''' and tapering the section between 4' and
4''' forming transition section 4". The hollow pipe 4 is press-fitted into the small-diameter
part 4 of the preliminary hole in the same way as above method described with reference
to Fig. 6, resulting in the assembly illustrated in 7(b). The part of the hollow pipe
4 projecting upward from the small-diameter part 4
1 of the preliminary hole is then expanded toward the transition part 4" of the preliminary
hole to bring it into close contact with the wall surface of the transition part 4"
(see Fig. 7(c)). Then the part of the hollow pipe 4 projecting beyond the outlet side
of the nozzle plate 2 is ground so that the end of the hollow pipe 4 is flush with
the surface of the nozzle plate 2. In addition, if desired, the part of the hollow
pipe 4 in close contact with the transition part 4'" of the preliminary hole can be
ground by-a special tip to provide a smoother transition from section 4'" to the passage
in nozzle 4. Thus, the large-diameter part 4'" and the transition part 4" in combination
form the inlet hole 6 as illustrated in 7(d).
[0016] Fig. 8 illustrates the method of manufacturing the spinneret plate lb with a projecting
nozzle. The step of machining the preliminary hole in the nozzle plate 2 and the step
of press-fitting the hollow pipe (see Figs. 8a and 8b, respectively) are similar to
those described with reference to Fig. 7. This method differs from the previous method
only in that the hollow pipe 4 projects further beyond the outlet side of the nozzle
plate 2. The upper end of the thus press-fitted hollow pipe 4 is expanded toward the
transition part of the preliminary hole. In addition, brazing 8 is applied to the
outer peripheral portion of the projecting part of the hollow pipe 4 (see Fig. 8c).
This brazing operation may be effected by a conventional method, e.g., by heating
in an electric furnace. Upon the completion of the brazing operation, both the part
of the hollow pipe projecting from the outlet side of the nozzle plate 2 and the brazed
part of the hollow pipe 4 are ground to a predetermined configuration. Finally, if
desired, the part of the hollow pipe 4 in close contact with the transition part of
the prepared hole can be ground by a special tip to cut off the bent part forming
the plate lb illustrated in 8d.
[0017] The present invention thus provides spinning nozzle a ready-made hollow pipe which
has excellent roundness and straightness. Therefore it is possible to provide an accurate
spinneret plate which has a spinning nozzle with an extremely smooth inner surface
and a uniform aspect ratio. Further, according to the invention, it is possible to
provide a multi-nozzle spinneret plate provided with a plurality of such accurate
nozzle holes. The employment-of the spinneret plate in accordance with the present
invention makes it possible to spin pitch carbon fibers or the like stably over a
long period of time.
1. A spinneret plate for melt spinning comprising (a) a nozzle plate having a hole
formed therein and (b) a hollow pipe of a predetermined inner diameter mounted in
said plate for conducting melt spinning material.
2. The spinneret plate of claim 1 wherein said pipe is press fit mounted in said hole
of said plate.
3. The spinneret plate of claim 2 wherein the opposite ends of the pipe are flush
with the upper and lower surface of the said nozzle plate.
4. The spinneret plate of claim 2 wherein the pipe extends only through a lower portion
of the nozzle plate and the hole in an upper portion of the nozzle plate is larger
in diameter than the pipe.
5. A method of manufacturing a spinneret plate for melt spinning comprising the steps
of (a) forming a preliminary hole in a metal nozzle plate; (b) press-fitting a hollow
metal pipe into said preliminary hole, and (c) shaping the end parts of the hollow
pipe press-fitted into said preliminary hole into predetermined configurations.
6. The method as defined in claim 5 wherein the upper and lower ends of the pipe are
shaped to be flush with the upper surface and lower surface, respectively, of the
nozzle plate.
7. The method of manufacturing a spinneret plate for melt spinning according to claim
5, wherein said press-fitting step is carried out by: heating said nozzle plate to
between 150 and 300°C; maintaining said hollow pipe at room temperature or cooling
it at a lower temperature; inserting said hollow pipe into said nozzle plate; and
cooling said nozzle plate.
8. The method of manufacturing a spinneret plate for melt spinning according to claim
5, wherein said preliminary hole has a large-diameter inlet part and a small-diameter
part, and said hollow pipe is press-fitted into said small-diameter part.
9. The method of manufacturing a spinneret plate for melt spinning according to claim
8, wherein said hollow pipe is positioned so as to project below the lower surface
of said nozzle plate.
10. The method as defined in claim 5 wherein said nozzle plate and said pipe are made
of steel.