(19)
(11) EP 0 263 508 A3

(12) EUROPEAN PATENT APPLICATION

(88) Date of publication A3:
03.08.1988 Bulletin 1988/31

(43) Date of publication A2:
13.04.1988 Bulletin 1988/15

(21) Application number: 87114626

(22) Date of filing: 07.10.1987
(84) Designated Contracting States:
BE CH DE FR GB IT LI LU NL SE

(30) Priority: 10.10.1986 US 917505

(71) Applicant: E.I. DU PONT DE NEMOURS AND COMPANY
 ()

(72) Inventor:
  • Ellis, Charles Daniel
     ()

   


(54) Process for preparing a photographic emulsion containing tabular grains exhibiting high speed


(57) Process for preparing a photographic emulsion containing tabular silver halide grains, which exhibit high speed upon sensitization, having a thickness of about 0.05 to 0.5 µm, average grain volume of about 0.05 to 1.0 µm³ and mean aspect ratio of greater than 2:1 comprising

A. adding silver nitrate to a vessel containing dispersing medium/bromide mixture, initial bromide ion concentration 0.08 to 0.25 N, to form tabular seed grains;

B. adding an ammoniacal base solution, to achieve 0.002 to 0.2 normal of the base (e.g., after at least 2% of total silver nitrate has been added); and

C. adding additional silver nitrate and halide, i.e., Br⁻ or BrI⁻, by balanced double jet procedure. The emulsions are used in photographic elements for x-ray, graphic arts, etc.







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