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(11) | EP 0 301 915 A3 |
(12) | EUROPEAN PATENT APPLICATION |
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(54) | Method for producing oxidized filaments |
(57) In a method for producing oxidized filaments (102) by treating precursor filaments
(101) in a bed (5a) fluidized by an oxidizing gas and heat treating the precursor
filaments (101) in the fluidized bed (5a), the fluidized bed (5a) is formed with heat-medium
particles (5), not less than 80% by weight of which are of solid particles each having
a particle diameter of not greater than 10 mesh, and the oxidation is carried out
under optimum conditions within an optimum range of the treatment temperatures, an
optimum range of depths H of the fluidized bed (5a) and an optimum gas speed of the
oxidizing gas. By the method, the period of time required for the oxidation can be
greatly shortened and oxidized filaments (102) having excellent characteristics can
be obtained Furthermore, where the oxidized filaments thus obtained are carbonized,
carbon fibers having excellent mechanical properties can be produced. |