<?xml version="1.0" encoding="UTF-8"?>
<!DOCTYPE ep-patent-document PUBLIC "-//EPO//EP PATENT DOCUMENT 1.1//EN" "ep-patent-document-v1-1.dtd">
<ep-patent-document id="EP89300720B1" file="EP89300720NWB1.xml" lang="en" country="EP" doc-number="0328272" kind="B1" date-publ="19940302" status="n" dtd-version="ep-patent-document-v1-1">
<SDOBI lang="en"><B000><eptags><B001EP>ATBECHDE..ESFRGBGRITLILUNLSE......................</B001EP><B005EP>R</B005EP><B007EP>DIM360   - Ver 2.5 (21 Aug 1997)
 2100000/1 2100000/2</B007EP></eptags></B000><B100><B110>0328272</B110><B120><B121>EUROPEAN PATENT SPECIFICATION</B121></B120><B130>B1</B130><B140><date>19940302</date></B140><B190>EP</B190></B100><B200><B210>89300720.3</B210><B220><date>19890126</date></B220><B240><B241><date>19901214</date></B241><B242><date>19920630</date></B242></B240><B250>en</B250><B251EP>en</B251EP><B260>en</B260></B200><B300><B310>6679/88</B310><B320><date>19880210</date></B320><B330><ctry>AU</ctry></B330></B300><B400><B405><date>19940302</date><bnum>199409</bnum></B405><B430><date>19890816</date><bnum>198933</bnum></B430><B450><date>19940302</date><bnum>199409</bnum></B450><B451EP><date>19930524</date></B451EP></B400><B500><B510><B516>5</B516><B511> 5G 01N   3/26   A</B511><B512> 5G 01N  33/34   B</B512></B510><B540><B541>de</B541><B542>Schersteifheitsmessverfahren</B542><B541>en</B541><B542>Shear stiffness measuring method</B542><B541>fr</B541><B542>Méthode de mesure de rigidité en cisaillement</B542></B540><B560><B561><text>DE-C-    96 334</text></B561><B561><text>US-A- 2 843 390</text></B561><B562><text>INSTRUMENTS AND CONTROL SYSTEMS, vol. 44, no. 5, May 1971, pages 97-98; M.W. POORE et al.: "Torsion testing using a digital computer"</text></B562><B562><text>MICROTECNIC, vol. 18, no. 4, August 1964, pages 192-193; M.I. TSCHAJEWSKI: "Machine for elastic-plastic torsional strain tests"</text></B562><B562><text>ANNUAL BOOK OF ASTM STANDARDS 1987, Standard T803 om-79, TAPPI, Atlanta, US, pages 1265-1267</text></B562></B560></B500><B700><B720><B721><snm>McKinlay, Peter Robert</snm><adr><str>4 Southgate</str><city>South Melbourne
Victoria 3205</city><ctry>AU</ctry></adr></B721></B720><B730><B731><snm>AMCOR LIMITED</snm><iid>00787824</iid><adr><str>Level 23 Southgate Tower East
40 City Road</str><city>South Melbourne
Victoria 3205</city><ctry>AU</ctry></adr></B731></B730><B740><B741><snm>Marles, Alan David</snm><sfx>et al</sfx><iid>00059622</iid><adr><str>Stevens, Hewlett &amp; Perkins
1 St Augustine's Place</str><city>Bristol BS1 4UD</city><ctry>GB</ctry></adr></B741></B740></B700><B800><B840><ctry>AT</ctry><ctry>BE</ctry><ctry>CH</ctry><ctry>DE</ctry><ctry>ES</ctry><ctry>FR</ctry><ctry>GB</ctry><ctry>GR</ctry><ctry>IT</ctry><ctry>LI</ctry><ctry>LU</ctry><ctry>NL</ctry><ctry>SE</ctry></B840><B880><date>19901003</date><bnum>199040</bnum></B880></B800></SDOBI><!-- EPO <DP n="1"> -->
<description id="desc" lang="en">
<p id="p0001" num="0001">This invention relates to an instrument and method for testing paperboard products and assessing the structural properties of paperboard during manufacture. In particular, this invention is concerned with measuring shear stiffness of the corrugating medium in corrugated paperboard.</p>
<p id="p0002" num="0002">Measurement of shear stiffness provides an important parameter in defining the structural properties of paperboard and for determining the strength of corrugated paperboard panels for end use applications.</p>
<p id="p0003" num="0003">Various methods have been investigated for measuring the core (medium) shear stiffness of corrugated board. The methods currently used are:
<ul id="ul0001" list-style="none">
<li>1) Three point beam test at various spans;</li>
<li>2) Direct shear.</li>
</ul></p>
<p id="p0004" num="0004">The first of these methods requires a lot of testing and for relatively stiff cores can give low results due to local buckling at the point of application of the central load.</p>
<p id="p0005" num="0005">The second method requires attaching the specimen to a rigid backing strip by gluing or some other means. This procedure is tedious and the results from this method are very variable due to the very small deflections involved during measurement.</p>
<p id="p0006" num="0006">It is an object of this invention to provide a simpler method of determining shear stiffness using a few samples.</p>
<p id="p0007" num="0007">In another aspect this invention relates to a method of asssessing damage to corrugated board mediums during printing and box manufacture.</p>
<p id="p0008" num="0008">At present the recommended method of assessing medium damage is by thickness measurements of the board in accordance with 1987 Tappi Report 30304-11.</p>
<p id="p0009" num="0009">This invention provides a more accurate measure of medium damage by measuring medium shear stiffness in the machine direction.<!-- EPO <DP n="2"> --></p>
<p id="p0010" num="0010">US-A-2843390 discloses a fluid operated clamping jaw which could be used in a torsion testing machine employing a method of determining the shear stiffness of a material as an aid in processing the material, comprising placing a sample of the material between two clamps and subjecting the sample to a twisting force.</p>
<p id="p0011" num="0011">According to the present invention the material is corrugated paperboard, one or more of the following tests are conducted: a) measuring the initial angle of twist for a given load; or b) measuring the change in the angle of twist over time under a constant load; or c) measuring the force required to achieve an initial angle of twist; or d) measuring the change over time in the force required to maintain a given angle of twist; and the shear stiffness S is determined according to the equation <maths id="math0001" num=""><math display="inline"><mrow><mtext>M = KϑS</mtext></mrow></math><img id="ib0001" file="imgb0001.tif" wi="17" he="5" img-content="math" img-format="tif" inline="yes"/></maths>  wherein M is the twisting torque, ϑ is the angle of clamp rotation and K is the proportionality constant <maths id="math0002" num=""><math display="inline"><mrow><mtext>K = 4a³/3L</mtext></mrow></math><img id="ib0002" file="imgb0002.tif" wi="21" he="5" img-content="math" img-format="tif" inline="yes"/></maths>  where a = halfwidth of the sample and L is the distance between the clamps.</p>
<p id="p0012" num="0012">By twisting a sample shear strains are produced in the core.</p>
<p id="p0013" num="0013">The measurements can also be made with varying conditions of humidity and varying degrees of crush applied to the sample to determine performance of the medium under varying conditions.</p>
<p id="p0014" num="0014">By assessing a range of products it is possible to establish a scale of performance with small deflections for a given force or large forces to achieve a given deflection being the desirable characteristics of better quality paperboards.</p>
<p id="p0015" num="0015">The device useful in carrying out the method of this invention essentially comprises a pair of axially aligned clamps at least one clamp being pivoted for rotation in a plane perpendicular to the alignment axis and means for measuring the force applied to rotate one of said clamps and means for measuring the angle of rotation.</p>
<p id="p0016" num="0016">The device can be manually operable with the<!-- EPO <DP n="3"> --> addition of weights to a lever arm or the like to produce rotation of one clamp relative to the other. Alternatively, the device can be mounted on a force measuring instrument such as an INSTRON and the rotatable clamp moved to a constant maximum angle of rotation with measurement of the force required to achieve that. Such a measurement can be repeated serially to determine the performance of the sample under such repetitive twist over time.</p>
<p id="p0017" num="0017">The method of this invention is used to measure shear stiffness in the Machine Direction (MD) of corrugated board. This means that the flutes are visible along the longside of the sample. This measure of MD shear measures approximately 80% of the required property and although not a pure measurement has great experimental advantages.</p>
<p id="p0018" num="0018">The various types of readings which can be gained provide a number of means of assessing the decay in shear stiffness over time as well as an initial assessment of shear stiffness. This enables a consistent comparison to be made of the quality of paperboard being produced or being utilised.</p>
<p id="p0019" num="0019">Thus, it con be used not only to assess the quality of board at a particular time but to also assess its likely behaviour in various humidities or after crushing to varying degrees.</p>
<p id="p0020" num="0020">A preferred form of this invention will now be described with reference to the drawings in which Figure 1 is a schematic side view of a simple mechanical form of the device and Figure 2 is an end view. Figure 3 is a schematic view of a form of device with microprocessor controls and digital display. Figure 4 is a block diagram of such a device, Figures 5, 6 and 8 are graphical results using the method of this invention and Figure 7 is a graphical result for a prior art method.</p>
<p id="p0021" num="0021">The device comprises a base 9, two axial supports 11 and 12 which support clamping heads 13 and 14 on a common axis 10. The clamping heads 13 and 14 are both rotatable in a plane perpendicular to the axis 10.<!-- EPO <DP n="4"> --></p>
<p id="p0022" num="0022">The sample to be tested is held with its longitudinal axis aligned with axis 10 in the clamps 13 and 14. Screws 15 enable clamps 13 and 14 to be tightened to effectively grip the sample 21 without producing out of balance in the clamps.</p>
<p id="p0023" num="0023">Clamp 13 can be fixed in position by preventing rotation of the connecting clamp 13 about the axis 10 relative to the axial support 11 by way of adjustment screw 20.</p>
<p id="p0024" num="0024">Clamp 14 which is on a common axis with the wheel 16 is finely balanced to freely turn its axis. The wheel 16 can have a wire 17 wound on to it to support a weight.</p>
<p id="p0025" num="0025">Alternatively, the instrument can be mounted on a force measuring instrument via support 19 and the wire 17 can also be connected. The wheel 16 is marked with an angular scale 18 and the marker 22 is used to align the axis with the beginning of the scale.</p>
<p id="p0026" num="0026">To carry out testing, a specimen board is cut into test pieces of normal test size 100mm by 25mm.</p>
<p id="p0027" num="0027">A test piece 21 is then mounted into the clamp and the clamps 13 and 14 tightened. The clamps are rotated to bring the beginning of the scale 18 into alignment with marker 22 and the clamp 13 is fixed by tightening screw 20.</p>
<p id="p0028" num="0028">The embodiment shown in figure 3 comprises a base 30 supporting the instrument which comprises
<ul id="ul0002" list-style="none">
<li>(i) a load cell 31 and its associated bearing housing 32 for the sample jaws 33.</li>
<li>ii) an electric motor 35 and associated gearbox 36 connected via the soft coupling 37 to the rotary encoder 38 to which the sample jaws 39 are connected.</li>
</ul></p>
<p id="p0029" num="0029">A cam and microswitch 40 are located between the sample jaw 39 and rotary encoder 38. The covers 41 enclose the stationary parts of the apparatus so that only the sample 42 and the jaws 33 and 39 are exposed.</p>
<p id="p0030" num="0030">This form of the testing device is microprocessor controlled as illustrated in the block diagram of Figure 4. Inputs are received from the load cell and the rotary<!-- EPO <DP n="5"> --> encoder to measure force and angular displacement. Desired loads or angular deflections for samples can be keyed in. Readouts of force or displacement are shown on a LCD display panel. The electronic circuitry and the programming of the microprocessor are conventional.</p>
<p id="p0031" num="0031">Either apparatus can be operated in a number of modes to measure:
<ul id="ul0003" list-style="dash">
<li>initial deflection under constant load</li>
<li>initial load for a constant deflection and</li>
<li>variations of these over time in either fixed or varying atmospheric and humidity conditions.</li>
</ul></p>
<p id="p0032" num="0032">The twisting movement (M) at the jaws 13, 14 is proportional to the angle of jaw rotation (O) and the MD Shear stiffness (S) of the corrugated sample. The constant of proportionality (K) is related to the geometry of the sample, namely its width (2a) (a being half the sample width with the corrugations transverse to the axis of rotation), and the geometry of the apparatus, namely the free length (L) between the jaws 13, 14. That is: <maths id="math0003" num=""><math display="inline"><mrow><mtext>M = KϑS</mtext></mrow></math><img id="ib0003" file="imgb0003.tif" wi="16" he="5" img-content="math" img-format="tif" inline="yes"/></maths>  where <maths id="math0004" num=""><math display="inline"><mrow><mtext>K = 4a³/3L</mtext></mrow></math><img id="ib0004" file="imgb0004.tif" wi="18" he="5" img-content="math" img-format="tif" inline="yes"/></maths><br/>
    Figure 5 shows the average performance of samples of waxed, unwaxed, unprinted and unwaxed printed boards over time under constant stress. The graphs illustrate the increase in deflection over time and demonstrate the superior shear stiffness of the waxed boards.</p>
<p id="p0033" num="0033">Comparative tests have been carried out to compare the industry recommended method of measuring medium damage with the method according to this invention.</p>
<p id="p0034" num="0034">Tests were carried out on samples from corrugated board used in making boxes in accordance with the following specifications:
<tables id="tabl0001" num="0001"><img id="ib0005" file="imgb0005.tif" wi="150" he="41" img-content="table" img-format="tif"/>
</tables><!-- EPO <DP n="6"> -->
<tables id="tabl0002" num="0002"><img id="ib0006" file="imgb0006.tif" wi="147" he="91" img-content="table" img-format="tif"/>
</tables></p>
<p id="p0035" num="0035">Figure 6 shows the load readings for shear stiffness measured in Milli Newton metres in accordance with the present invention and Figure 7 shows the thickness of the same board.</p>
<p id="p0036" num="0036">A comparison of Figures 6 and 7 clearly shows that a much better measure of the board damage at various moisture levels in the board can be ascertained from Shear Stiffness measurements than from thickness. This is probably due in part to thickness recovery after damage has occurred.</p>
<p id="p0037" num="0037">Figure 8 illustrates another application of the present invention in assessing damage for quality control purposes across the corrugator machine.</p>
<p id="p0038" num="0038">By measuring the medium shear at various distances from the operator side of the corrugator a profile of the machine's effect on board quality is shown for different corrugator speeds.</p>
<p id="p0039" num="0039">The information derived from tests of the sort illustrated in Figures 6 and 8 enable operators to adjust machine speed or other operating conditions to maintain desired structural properties in the corrugated board.</p>
<p id="p0040" num="0040">Although the measurement of shear stiffness by this method is not a "pure" measurement it has experimental advantages. The apparatus is simple to use and requires minimal sample preparation.</p>
</description><!-- EPO <DP n="7"> -->
<claims id="claims01" lang="en">
<claim id="c-en-01-0001" num="0001">
<claim-text>A method of determining the shear stiffness of a material as an aid in processing the material, comprising placing a sample (21) of the material between two clamps (13,14) and subjecting the sample (21) to a twisting force characterised in that the material is corrugated paperboard and in that one or more of the following tests are conducted: a) measuring the initial angle of twist for a given load; or b) measuring the change in the angle of twist over time under a constant load; or c) measuring the force required to achieve an initial angle of twist; or d) measuring the change over time in the force required to maintain a given angle of twist; and in that the shear stiffness, S, is determined according to the equation <maths id="math0005" num=""><math display="inline"><mrow><mtext>M = KϑS</mtext></mrow></math><img id="ib0007" file="imgb0007.tif" wi="17" he="5" img-content="math" img-format="tif" inline="yes"/></maths>  wherein M is the twisting torque, ϑ is the angle of clamp rotation and K is the proportionality constant <maths id="math0006" num=""><math display="inline"><mrow><mtext>K = 4a³/3L</mtext></mrow></math><img id="ib0008" file="imgb0008.tif" wi="20" he="6" img-content="math" img-format="tif" inline="yes"/></maths>  where a = halfwidth of the sample (21) and L is the distance between the clamps (13,14).</claim-text></claim>
<claim id="c-en-01-0002" num="0002">
<claim-text>A method according to claim 1 characterised in that the sample (21) is rectangular in shape and is held lengthwise by said clamps (13,14) located at each end and in that one end only is subjected to a twisting force.</claim-text></claim>
<claim id="c-en-01-0003" num="0003">
<claim-text>A method according to claim 2 characterised in that the clamps (13,14) are axially aligned and one clamp (14) is pivoted for rotation in a plane perpendicular to the alignment axis (10).<!-- EPO <DP n="8"> --></claim-text></claim>
<claim id="c-en-01-0004" num="0004">
<claim-text>A method according to claim 3 characterised in that the force needed to rotate said one clamp (14) is measured and the angle of rotation of said one clamp (14) is also measured.</claim-text></claim>
</claims><!-- EPO <DP n="9"> -->
<claims id="claims02" lang="de">
<claim id="c-de-01-0001" num="0001">
<claim-text>Verfahren zum Bestimmen der Schersteifheit eines Materials als Hilfsmittel beim Verarbeiten des Materials, wobei eine Probe (21) des Materials zwischen zwei Klemmen (13,14) angeordnet und einer Verwindungskraft unterworfen wird, dadurch gekennzeichnet, daß das Material Wellpappe ist und einer oder mehrere der folgenden Tests durchgeführt wird: a) Messen des Anfangswinkels der Verwindung für eine gegebene Belastung oder b) Messen der Änderung des Verwindungswinkels über die Zeit unter einer konstanten Belastung oder c) Messen der für einen Anfangsverwindungswinkel erforderlichen Kraft oder d) Messen der Änderung der zur Aufrechterhaltung eines gegebenen Verwindungswinkels erforderlichen Kraft über die Zeit, und dadurch, daß die Schersteifheit S gemäß der Gleichung <maths id="math0007" num=""><math display="inline"><mrow><mtext>M = KΘS</mtext></mrow></math><img id="ib0009" file="imgb0009.tif" wi="6" he="5" img-content="math" img-format="tif" inline="yes"/></maths><maths id="math0008" num=""><img id="ib0010" file="imgb0010.tif" wi="12" he="5" img-content="math" img-format="tif" inline="yes"/></maths>  bestimmt wird, in der M das Verwindungsdrehmoment Θ der Winkel der Klemmendrehung und K die Propertionalitätskonstante <maths id="math0009" num=""><math display="inline"><mrow><mtext>K = 4a³/3L</mtext></mrow></math><img id="ib0011" file="imgb0011.tif" wi="20" he="5" img-content="math" img-format="tif" inline="yes"/></maths>  bedeuten, worin a die halbe Breite der Probe (21) und L der Abstand zwischen den Klemmen (13,14) ist.</claim-text></claim>
<claim id="c-de-01-0002" num="0002">
<claim-text>Verfahren nach Anspruch 1, dadurch gekennzeichnet, daß die Probe (21) eine rechteckige Form aufweist und der Länge nach durch die genannten Klemmen (13,14) gehalten wird, die an jedem Ende angeordnet sind, und daß nur ein Ende einer Verwindungskraft unterworfen wird.</claim-text></claim>
<claim id="c-de-01-0003" num="0003">
<claim-text>Verfahren nach Anspruch 2, dadurch gekennzeichnet, daß die Klemmen (13,14) axial ausgerichtet sind und eine<!-- EPO <DP n="10"> --> Klemme (14) zur Drehung in einer Ebene senkrecht zur Ausrichtungsachse (10) drehbar angelenkt ist.</claim-text></claim>
<claim id="c-de-01-0004" num="0004">
<claim-text>Verfahren nach Anspruch 3, dadurch gekennzeichnet, daß sowohl die zum Drehen der einen Klemme (14) nötige Kraft als auch der Drehwinkel dieser Klemme (14) gemessen werden.</claim-text></claim>
</claims><!-- EPO <DP n="11"> -->
<claims id="claims03" lang="fr">
<claim id="c-fr-01-0001" num="0001">
<claim-text>Procédé pour déterminer la rigidité en cisaillement d'un matériau, en tant qu'auxiliaire du traitement du matériau, consistant à placer un échantillon (21) du matériau entre deux mâchoires de serrage (13, 14) et à soumettre l'échantillon (21) à une force de torsion, caractérisé en ce que le matériau est du carton ondulé, en ce qu'un ou plusieurs des essais suivants sont effectués :
<claim-text>a) mesure de l'angle de torsion initial pour une charge donnée ; ou</claim-text>
<claim-text>b) mesure de la variation de l'angle de torsion, dans le temps, sous une charge constante ; ou</claim-text>
<claim-text>c) mesure de la force nécessaire pour former un angle de torsion initial ; ou</claim-text>
<claim-text>d) mesure de la variation dans le temps de la force nécessaire pour maintenir un angle de torsion donné; et</claim-text>    en ce que la rigidité en cisaillement S est déterminée suivant l'équation <maths id="math0010" num=""><math display="inline"><mrow><mtext>M = KΘS</mtext></mrow></math><img id="ib0012" file="imgb0012.tif" wi="16" he="6" img-content="math" img-format="tif" inline="yes"/></maths> , dans laquelle M représente le couple de torsion, Θ représente l'angle de rotation de la mâchoire de serrage, et K représente la constante de proportionnalité <maths id="math0011" num=""><math display="inline"><mrow><mtext>K = 4a³ /3L</mtext></mrow></math><img id="ib0013" file="imgb0013.tif" wi="20" he="5" img-content="math" img-format="tif" inline="yes"/></maths>  où a = la moitié de la largeur de l'échantillon (21) et L est la distance entre les mâchoires de serrage (13,14).</claim-text></claim>
<claim id="c-fr-01-0002" num="0002">
<claim-text>Procédé selon la revendication 1, caractérisé en ce que l'échantillon (21) est de forme rectangulaire et est maintenu longitudinalement par lesdites mâchoires de serrage (13, 14) situées à chaque extrémité et en ce que seulement l'une des extrémités est soumise à une force de torsion.</claim-text></claim>
<claim id="c-fr-01-0003" num="0003">
<claim-text>Procédé selon la revendication 2, caractérisé en ce que les mâchoires de serrage (13, 14) sont alignées axialement et une mâchoire de serrage (14) est montée à pivotement de manière à tourner dans un plan perpendiculaire à l'axe d'alignement (10).</claim-text></claim>
<claim id="c-fr-01-0004" num="0004">
<claim-text>Procédé selon la revendication 3, caractérisé en ce que la force nécessaire pour faire tourner ladite mâchoire (14) est mesurée et l'angle de rotation de ladite mâchoire (14) est également mesuré.</claim-text></claim>
</claims><!-- EPO <DP n="12"> -->
<drawings id="draw" lang="en">
<figure id="f0001" num=""><img id="if0001" file="imgf0001.tif" wi="159" he="221" img-content="drawing" img-format="tif"/></figure>
<figure id="f0002" num=""><img id="if0002" file="imgf0002.tif" wi="116" he="219" img-content="drawing" img-format="tif"/></figure>
<figure id="f0003" num=""><img id="if0003" file="imgf0003.tif" wi="149" he="220" img-content="drawing" img-format="tif"/></figure>
<figure id="f0004" num=""><img id="if0004" file="imgf0004.tif" wi="160" he="225" img-content="drawing" img-format="tif"/></figure>
<figure id="f0005" num=""><img id="if0005" file="imgf0005.tif" wi="158" he="240" img-content="drawing" img-format="tif"/></figure>
<figure id="f0006" num=""><img id="if0006" file="imgf0006.tif" wi="155" he="233" img-content="drawing" img-format="tif"/></figure>
<figure id="f0007" num=""><img id="if0007" file="imgf0007.tif" wi="152" he="240" img-content="drawing" img-format="tif"/></figure>
</drawings>
</ep-patent-document>
