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EP 0 364 009 B1 |
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EUROPEAN PATENT SPECIFICATION |
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Mention of the grant of the patent: |
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23.03.1994 Bulletin 1994/12 |
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Date of filing: 30.01.1989 |
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Dispenser for dispensing cryogenic liquid
Ausgabegerät zum Zapfen von kryogenen Flüssigkeiten
Distribution pour distribuer des liquides cryogéniques
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Designated Contracting States: |
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AT BE CH DE ES FR GR IT LI LU NL SE |
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Priority: |
29.02.1988 GB 8804760
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Date of publication of application: |
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18.04.1990 Bulletin 1990/16 |
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Application number of the earlier application in accordance with Art. 76 EPC: |
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89300891.2 / 0331287 |
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Proprietor: AIR PRODUCTS AND CHEMICALS, INC. |
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Allentown, Pennsylvania 18105 (US) |
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Inventor: |
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- Miller, Jeremy Paul
Staffs DE3 9QP (GB)
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Representative: Lucas, Brian Ronald |
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Lucas & Co.
135 Westhall Road Warlingham
Surrey CR6 9HJ Warlingham
Surrey CR6 9HJ (GB) |
| (56) |
References cited: :
US-A- 4 407 340
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US-A- 4 469 304
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| Note: Within nine months from the publication of the mention of the grant of the European
patent, any person may give notice to the European Patent Office of opposition to
the European patent
granted. Notice of opposition shall be filed in a written reasoned statement. It shall
not be deemed to
have been filed until the opposition fee has been paid. (Art. 99(1) European Patent
Convention).
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[0001] This invention relates to a dispenser for dispensing slugs of cryogenic liquid to
bottles or cans on a bottling or canning line and to a method for dispensing slugs
of cryogenic liquid from such a dispenser.
[0002] In the canning and bottling industries it is common practice to insert a small quantity
of liquid nitrogen into the cans or bottles immediately prior to closure. The liquid
nitrogen vaporizes in the can or bottle and displaces air from the can or bottle before
the closure is applied.
[0003] When filling cylindrical cans of uniform diameter it is quite convenient to dispense
liquid nitrogen in a continuous spray since the percentage of liquid nitrogen wasted
is relatively small. Such a method is disclosed in US-A-4 612 773. However, this technique
is extremely wasteful for bottles having relatively small necks, for example beer
bottles.
[0004] In order to introduce liquid nitrogen into beer bottles it has been proposed to drop
a discrete quantity of liquid nitrogen into each beer bottle immediately prior to
closure.
[0005] US-A-4 407 340 discloses a dispenser for dispensing slugs of cryogenic liquid to
bottles or cans on a bottling or canning line, which dispenser comprises a vessel
for holding cryogenic liquid, a dispenser tube mounted on said vessel, a valve associated
with said dispenser tube and operable in use, to allow or inhibit the flow of cryogenic
liquid from said vessel. In this dispenser the valve is opened and closed by a solenoid
mounted on top the vessel. This dispenser has two disadvantages, viz:-
1. Instead of discrete slugs or droplets of liquid nitrogen descending into the bottles
from a dispenser the bottles have been assailed by a diverging cone of minute droplets
only a tiny portion of which enter the bottle; and
2. Insofar as the output of the dispenser might be regarded as slugs, the maximum
continuous output which can be achieved in practice is around 500 slugs/minute.
[0006] A solution to reduce the former problem is disclosed in our co-pending European Patent
Application No. 89 300 891.2 (EP-A-0 331 287).
[0007] In order to help overcome the later problem the present invention provides a dispenser
for dispensing slugs of cryogenic liquid to bottles or cans on a bottling or canning
line, which dispenser comprises a vessel for holding cryogenic liquid, a dispenser
tube mounted on said vessel, a valve associated with said dispenser tube and operable,
in use, to allow or inhibit the flow of cryogenic liquid from said vessel, and means
for opening and closing said valve, characterized in that said means for opening and
closing said valve are wholly contained within said vessel and are capable of opening
and closing said valve at least 600 times per minute.
[0008] Preferably, said means for opening and closing said valve comprises a permanent magnet
connected to said valve, and a coil circumjacent said permanent magnet and arranged
to receive, in use, direct current.
[0009] In conventional dispensers a globule of liquid nitrogen remains in the dispenser
tube after each injection due to surface tension. If the canning or bottling line
is stopped for any reason part of the globule evaporates. The vapour thus formed collects
between the valve and the globule and ejects the globule downwardly. If a can or bottle
is below the dispenser tube at the time it thus receives more liquid nitrogen than
intended. If the canning or bottling line is restarted soon after this happens the
can or bottle can be sealed whilst it contains excess nitrogen. Because of the 700:1
volumetric expansion when liquid nitrogen evaporates this can be followed by the can
or bottle closure being blown off or, in some cases, the can or bottle breaking or
exploding.
[0010] In order to reduce this problem dispensers in accordance with the present invention
are preferably provided with a gas relief tube which communicates with said dispenser
tube between the valve and the outlet of the dispenser tube.
[0011] Preferably, said gas relief tube is arranged to relieve gas from said dispenser tube
into said dispenser, preferably at a level which, when said dispenser is in use, is
above the level of the cryogenic liquid in said vessel.
[0012] The present invention also provides a method for dispensing slugs of cryogenic liquid
from a dispenser according to the invention, which method comprises the step of opening
and closing said valve at least 600 times per minute.
[0013] Advantageously, said method includes the step of opening and closing said valve at
a rate greater than 1000 cycles per minute.
[0014] For a better understanding of the present invention reference will now be made, by
way of example, to the accompanying drawing which is a diagrammatic vertical section
through a dispenser for dispensing cryogenic liquid in accordance with the invention.
[0015] Referring to the drawing, there is shown a dispenser which is generally identified
by reference numeral 1.
[0016] The dispenser 1 comprises a vacuum insulated vessel 2. An inlet conduit or pipe 3
extends downwardly through the vacuum insulated vessel 2 to a float valve 4. A vent
pipe 5 extends upwardly from the vacuum insulated vessel 2 and is provided with a
sensor 6 which is arranged to close safety valve 7 in pipe 3 if liquid is detected
in the vent pipe 5.
[0017] A dispenser head 8 is mounted on the bottom of the vacuum insulated vessel 2. The
dispenser head 8 is provided with a central bore 9 which is disposed circumjacent
and in intimate thermal contact with a dispenser tube 10 which extends downwardly
from the inside of the vacuum insulated vessel 2.
[0018] The dispenser head 8 is provided with a heater 11 which can be connected to a source
of electric power via wires 12 and 13.
[0019] The upper end of the dispenser tube 10 can be opened or closed by means of a tapered
valve 14 which is biased downwardly by a spring 15. The tapered valve member 14 is
connected to a permanent magnet 16 disposed in a coil 17 which, when actuated by a
DC current in one sense, raises the tapered valve member 14 to open the upper end
of the dispenser tube 10. When the DC field is reversed the tapered valve member 14
is driven down. This arrangement gives positive control compared with the solenoid
and spring arrangement of the prior art which relies on the spring to close the valve.
[0020] A gas relief tube 18 extends from a position in the dispenser tube 10 between the
tapered valve member 14 and the outlet of the dispenser tube 10 and opens in the vacuum
insulated vessel 2 above the float valve 4.
[0021] In use, safety valve 7 is opened and liquid nitrogen flows into the interior of the
vacuum insulated vessel 2 through pipe 3 until it reaches level 19 when the float
valve 4 closes. Vapour leaves the vacuum insulated vessel 2 via the vent pipe 5.
[0022] Power is applied to heater 11 to warm the dispenser head 8.
[0023] When a slug of nitrogen is required a DC current is applied in the appropriate sense
to coil 17 thereby raising permanent magnet 16 against the bias of spring 15. Liquid
nitrogen then enters the top of dispenser tube 10.
[0024] The heater 11 transmits sufficient heat such that a film of gas is formed on the
inner surface of the dispenser tube 10. This acts as an insulating and lubricating
barrier which permits individual slugs of liquid nitrogen to pass downwardly through
the dispenser tube 10. The liquid nitrogen emerges from the bottom of the dispenser
tube 10 in the form of slugs of liquid with negligible or little dispersion compared
with the prior art. Vapour in the dispenser tube 10 rises through the gas relief tube
18 into the vacuum insulated vessel 2 and thence to vent pipe 5.
[0025] Clearly the power input to the heater 11 depends on the frequency with which the
coil 17 is actuated and the volume of liquid nitrogen being released with each operation.
[0026] In order to set up the equipment correctly the coil 17 is first operated at the desired
frequency with the level of liquid nitrogen in the vacuum insulated vessel 2 being
maintained substantially constant by float valve 4.
[0027] At first the nitrogen leaves the bottom of the dispenser tube 10 in the form of a
diffuse atomized cone, i.e., in the form common to the prior art. Power is then applied
to heater 11 slowly to allow for the heat capacity of the dispenser head 8.
[0028] As the power increases the volume of the spray appears to decrease. However, beyond
a certain point the discharge turns into a stream of discrete slugs of liquid nitrogen
which fall vertically downwardly like droplets of water. These slugs can be directed
into the necks of beer bottles and the like with little or no difficulty. Furthermore,
work with a prototype according to the invention suggests that a single dispenser
may be capable of delivering discrete slugs of liquid nitrogen to as many as 2000
bottles per minute on a high speed bottling line.
[0029] As a by-product of the heater 11 ice does not accumulate on the base of the dispenser
head 8. In this connection it should be noted that heaters have previously been used
to prevent ice accumulating on the base of dispenser heads (see UK 2 091 228A). However,
in such arrangements special arrangements have been made to ensure that the dispensing
tube is kept cold, in particular by passing cold nitrogen vapour circumjacent the
dispensing tube in the aforesaid patent specification and positioning the dispensing
tube well away from the base. It should also be noted that the aforesaid specification
discloses the use of a separate heater for removing ice from the dispenser during
shutdown. However, it is explained that this heater is deactivated during start-up,
i.e., it is not used whilst the dispenser is dispensing liquid.
Example:-
[0030] Liquid nitrogen slugs having an average volume of 0.037 cc were dispensed at a rate
of 600 slugs/minute through a dispenser tube made of brass and having a nominal external
diameter of 5 mm and a nominal internal diameter of 3 mm. The dispenser head 8 was
made from high purity copper.
[0031] At equilibrium the heater 11 consumed 32 watts of power.
1. A dispenser (1) for dispensing slugs of cryogenic liquid to bottles or cans on a bottling
or canning line, which dispenser comprises a vessel (2) for holding cryogenic liquid,
a dispenser tube (10) mounted on said vessel (2), a valve (14) associated with said
dispenser tube (10) and operable, in use, to allow or inhibit the flow of cryogenic
liquid from said vessel (2), and means (16,17) for opening and closing said valve,
characterized in that said means (16,17) for opening and closing said valve (14) are
wholly contained within said vessel (2) and are capable of opening and closing said
valve (14) at least 600 cycles per minute.
2. A dispenser as claimed in Claim 1, characterized in that said means (16,17) for opening
and closing said valve (14) comprises a magnet (16) connected to said valve (14),
and a coil (17) circumjacent said permanent magnet (16) and arranged to receive, in
use, direct current.
3. A dispenser as claimed in Claim 1 or 2, characterized in that a gas relief tube (18)
is provided which communicates with said dispenser tube (10) between said valve (14)
and the outlet of said dispenser tube (10).
4. A dispenser as claimed in Claim 3, characterized in that said gas relief tube (18)
is arranged to relieve gas from said dispenser tube (10) into said vessel (1).
5. A dispenser as claimed in Claim 4, characterized in that said gas relief tube (18)
is arranged to relieve gas from said dispenser tube (10) into said dispenser (1) at
a level which, when said dispenser (1) is in use, is above the level of the cryogenic
liquid in said vessel (2).
6. A method for dispensing slugs of cryogenic liquid from a dispenser according to any
preceding Claim, characterized in that said method comprises the step of opening and
closing said valve (14) at least 600 times per minute.
7. A method according to Claim 6, characterized in that it includes the step of opening
and closing said valve (14) at a rate greater than 1000 cycles per minute.
1. Ausgabegerät (1) zum Zapfen dosierter Mengen eines Tieftemperaturfluids in Flaschen
oder Dosen auf einer Abfüllstrecke für Flaschen oder Dosen, wobei dieses Ausgabegerät
ein Gefäß (2) zur Aufnahme des Tieftemperaturfluids, eine Ausgabeleitung (10), die
auf diesem Gefäß (2) angebracht ist, ein Ventil (14), das mit dieser Ausgabeleitung
(10) verbunden ist und bei Verwendung betätigt werden kann, um den Strom des Tieftemperaturfluids
aus dem Gefäß (2) zu gestatten oder zu unterbinden, und eine Einrichtung (16, 17)
umfaßt, um dieses Ventil zu öffnen und zu schließen, dadurch gekennzeichnet, daß diese
Einrichtung (16, 17) zum Öffnen und Schließen des Ventils (14) vollkommen innerhalb
des Gefäßes (2) enthalten ist, und das Ventil (14) mit mindestens 600 Zyklen pro Minute
öffnen und schließen kann.
2. Ausgabegerät nach Anspruch 1, dadurch gekennzeichnet, daß die Einrichtung (16, 17)
zum Öffnen und Schließen des Ventils (14) einen Magnet (16), der mit dem Ventil (14)
verbunden ist, und eine Spule (17) umfaßt, die den Dauermagnet (16) umgibt und so
angeordnet ist, daß sie bei Verwendung Gleichstrom empfängt.
3. Ausgabegerät nach Anspruch 1 oder 2, dadurch gekennzeichnet, daß eine Gasüberdruckleitung
(18) vorgesehen ist, die zwischen dem Ventil (14) und dem Auslaß der Ausgabeleitung
(10) mit dieser Ausgabeleitung (10) in Verbindung steht.
4. Ausgabegerät nach Anspruch 3, dadurch gekennzeichnet, daß die Gasüberdruckleitung
(18) so angeordnet ist, daß sie das Gas aus der Ausgabeleitung (10) in das Gefäß (1)
entspannt.
5. Ausgabegerät nach Anspruch 4, dadurch gekennzeichnet, daß die Gasüberdruckleitung
(18) so angeordnet ist, daß sie das Gas aus der Ausgabeleitung (10) an einem Niveau
in das Ausgabegerät (1) entspannt, das bei Verwendung dieses Ausgabegerätes (1) oberhalb
des Niveaus des Tieftemperaturfluids im Gefäß (2) liegt.
6. Verfahren zum Zapfen dosierter Mengen eines Tieftemperaturfluids aus einem Ausgabegerät
nach einem der vorstehenden Ansprüche, dadurch gekennzeichnet, daß dieses Verfahren
mindestens 600 mal pro Minute den Schritt des Öffnens und Schließens des Ventils (14)
umfaßt.
7. Verfahren nach Anspruch 6, dadurch gekennzeichnet, daß es den Schritt des Öffnens
und Schließens des Ventils (14) mit einer Geschwindigkeit von mehr 1000 Zyklen pro
Minute umfaßt.
1. Appareil distributeur (1) pour délivrer des doses de liquide cryogénique dans des
bouteilles ou des bidons sur une ligne de remplissage de bouteilles ou de bidons,
lequel appareil distributeur comprend un récipient (2) pour renfermer un liquide cryogénique,
un tube distributeur (10) monté sur ce récipient (2), une soupape (14) associée à
ce tube distributeur (10) et apte à fonctionner, en cours d'utilisation, pour permettre
ou empêcher l'écoulement du liquide cryogénique à partir du récipient (2) et des moyens
(16, 17) pour ouvrir ou fermer ladite soupage, caractérisé en ce que les moyens (16,
17) pour ouvrir ou fermer la soupape (14) sont entièrement contenus à l'intérieur
du récipient (2) et sont aptes à ouvrir et fermer la soupape (14) au moins 600 fois
par minute.
2. Appareil distributeur selon la revendication 1, caractérisé en ce que lesdits moyens
(16, 17) pour ouvrir et fermer la soupape (14) comprennent un aimant (16) relié à
la soupape (14) et une bobine (17) circonjacente audit aimant permanent (16) et agencée
pour recevoir, en cours d'utilisation, un courant continu.
3. Appareil distributeur selon la revendication 1 ou 2, caractérisé en ce qu'il est prévu
un tube de détente de gaz (18) qui communique avec ledit tube distributeur (10) entre
la soupape (14) et la sortie du tube distributeur (10).
4. Appareil distributeur selon la revendication 3, caractérisé en ce que le tube de détente
de gaz (10) est agencé pour décharger des gaz depuis le tube distributeur (10) dans
le récipient (1).
5. Appareil distributeur selon la revendication 4, caractérisé en ce que le tube de détente
de gaz (18) est agencé pour décharger des gaz depuis le tube distributeur (10) dans
l'appareil distributeur (1) à un niveau qui, lorsque ledit appareil distributeur (1)
est en fonctionnement, est situé au-dessus du niveau du liquide cryogénique dans le
récipient (2).
6. Procédé pour délivrer des doses de liquide cryogénique à partir d'un appareil distributeur
selon l'une quelconque des revendications précédentes, caractérisé en ce que ledit
procédé comprend l'étape consistant à ouvrir et fermer la soupape (14) au moins 600
fois par minute.
7. Procédé selon la revendication 6, caractérisé en ce qu'il comporte l'étape consistant
à ouvrir et fermer la soupape (14) à une vitesse supérieure à 1000 fois par minute.
