(19)
(11) EP 0 378 187 A3

(12) EUROPEAN PATENT APPLICATION

(88) Date of publication A3:
31.10.1990 Bulletin 1990/44

(43) Date of publication A2:
18.07.1990 Bulletin 1990/29

(21) Application number: 90100420.0

(22) Date of filing: 10.01.1990
(51) International Patent Classification (IPC)5C10C 3/00, D01F 9/155
(84) Designated Contracting States:
BE CH DE FR GB IT LI NL SE

(30) Priority: 13.01.1989 JP 4882/89
09.06.1989 JP 145117/89

(71) Applicant: IDEMITSU KOSAN COMPANY LIMITED
Tokyo 100 (JP)

(72) Inventors:
  • Ohta, Masakatsu
    Sodegaura-machi, Kimitsu-gun, Chiba-ken (JP)
  • Sawada, Teiken
    Sodegaura-machi, Kimitsu-gun, Chiba-ken (JP)
  • Uchida, Tsuneaki
    Sodegaura-machi, Kimitsu-gun, Chiba-ken (JP)
  • Fukushima, Ryutaro
    Sodegaura-machi, Kimitsu-gun, Chiba-ken (JP)
  • Nagasaki, Yoshikazu
    Sodegaura-machi, Kimitsu-gun, Chiba-ken (JP)

(74) Representative: Türk, Gille, Hrabal, Leifert 
Brucknerstrasse 20
40593 Düsseldorf
40593 Düsseldorf (DE)


(56) References cited: : 
   
       


    (54) Pitch for carbon fibers, process for production of said pitch, and process for production of carbon fibers using said pitch


    (57) The present invention relates to a process for producing pitch for use in production of carbon fiber which comprises subjecting a pitch starting material to a first stage heat treatment at a temperature of 380 to 500°C under a pressure of 1 to 1,500 mmHg and then to a second stage heat treatment at a temperature of 450 to 550°C under a pressure of 0.1 to 20 mmHg, wherein the pitch starting material has a number average molecular weight of 300 to 500, weight average molecular weight/number average molecular weight of 1.5/1 to 2.2/1, a boiling point of at least 450°C, a residue content as determined by heating up to 800°C in nitrogen gas at a rate of 10°C per minute of not more than 5% by weight, and a peak area at the starting point as determined by developing on a silica gel thin layer with a mixed solvent of 95% by volume of dichloromethane and 5% by volume of methyl alcohol of not more than 1%.
    The present invention further relates to novel pitch for use in production of carbon fibers as obtained by the above process and a process for producing carbon fibers using said pitch. According to the present invention, the pitch capable of providing carbon fibers having a high tensile strength and a high knot strength can be obtained.





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