(19) |
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(11) |
EP 0 378 187 A3 |
(12) |
EUROPEAN PATENT APPLICATION |
(88) |
Date of publication A3: |
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31.10.1990 Bulletin 1990/44 |
(43) |
Date of publication A2: |
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18.07.1990 Bulletin 1990/29 |
(22) |
Date of filing: 10.01.1990 |
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(84) |
Designated Contracting States: |
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BE CH DE FR GB IT LI NL SE |
(30) |
Priority: |
13.01.1989 JP 4882/89 09.06.1989 JP 145117/89
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(71) |
Applicant: IDEMITSU KOSAN COMPANY LIMITED |
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Tokyo 100 (JP) |
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(72) |
Inventors: |
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- Ohta, Masakatsu
Sodegaura-machi, Kimitsu-gun, Chiba-ken (JP)
- Sawada, Teiken
Sodegaura-machi, Kimitsu-gun, Chiba-ken (JP)
- Uchida, Tsuneaki
Sodegaura-machi, Kimitsu-gun, Chiba-ken (JP)
- Fukushima, Ryutaro
Sodegaura-machi, Kimitsu-gun, Chiba-ken (JP)
- Nagasaki, Yoshikazu
Sodegaura-machi, Kimitsu-gun, Chiba-ken (JP)
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(74) |
Representative: Türk, Gille, Hrabal, Leifert |
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Brucknerstrasse 20 40593 Düsseldorf 40593 Düsseldorf (DE) |
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(54) |
Pitch for carbon fibers, process for production of said pitch, and process for production
of carbon fibers using said pitch |
(57) The present invention relates to a process for producing pitch for use in production
of carbon fiber which comprises subjecting a pitch starting material to a first stage
heat treatment at a temperature of 380 to 500°C under a pressure of 1 to 1,500 mmHg
and then to a second stage heat treatment at a temperature of 450 to 550°C under a
pressure of 0.1 to 20 mmHg, wherein the pitch starting material has a number average
molecular weight of 300 to 500, weight average molecular weight/number average molecular
weight of 1.5/1 to 2.2/1, a boiling point of at least 450°C, a residue content as
determined by heating up to 800°C in nitrogen gas at a rate of 10°C per minute of
not more than 5% by weight, and a peak area at the starting point as determined by
developing on a silica gel thin layer with a mixed solvent of 95% by volume of dichloromethane
and 5% by volume of methyl alcohol of not more than 1%.
The present invention further relates to novel pitch for use in production of carbon
fibers as obtained by the above process and a process for producing carbon fibers
using said pitch. According to the present invention, the pitch capable of providing
carbon fibers having a high tensile strength and a high knot strength can be obtained.
