(19) |
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(11) |
EP 0 482 784 A1 |
(12) |
EUROPEAN PATENT APPLICATION |
(43) |
Date of publication: |
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29.04.1992 Bulletin 1992/18 |
(22) |
Date of filing: 08.10.1991 |
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(51) |
International Patent Classification (IPC)5: B27K 9/00 |
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(84) |
Designated Contracting States: |
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BE DE FR GB NL |
(30) |
Priority: |
09.10.1990 GB 9021960
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(71) |
Applicant: The Queen's University of Belfast |
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Belfast BT7 1NN,
Northern Ireland (GB) |
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(72) |
Inventor: |
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- Easson, David Lindsay
Lisburn, BRT28 3AQ (GB)
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(74) |
Representative: Low, Peter John et al |
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Wilson, Gunn, M'Caw,
41-51 Royal Exchange,
Cross Street Manchester, M2 7BD Manchester, M2 7BD (GB) |
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(57) A method of treating flax straw comprising infusing sulphur dioxide gas through sealed
batches of moist flax. The sulphur dioxide reacts with the moisture producing acidic
conditions which significantly reduce mould and bacterial deterioration of the flax
and also improves the processing characteristics of the flax.
[0001] This invention relates to the treatment of flax straw.
[0002] The traditional dew retting of flax can only be practised in areas where the climate
is suitable. Alternative retting methods are now being developed, including the use
of enzymes. These alternative retting methods work successfully in a variety of climates.
However, when flax is produced in damp climates, there is often little opportunity
for field drying prior to storage and significant mould or bacterial deterioration
often takes place during storage as a result of this.
[0003] The present invention seeks to provide a solution to this problem.
[0004] According to the present invention there is provided a method of treatment of flax
straw comprising the infusion of a gas through moist flax straw so as to provide conditions
which inhibit the activity of any micro-organism which causes deterioration of the
flax.
[0005] This treatment improves the processing characteristics of the straw; that is it aids
separation of the flax fibres from the waste material.
[0006] The gas is preferably sulphur dioxide. The gas preferably provides acidic conditions.
Preferably 2% or less of sulphur dioxide by weight of the dry flax straw is used.
The reaction of the sulphur dioxide with the moisture provides acidic conditions.
[0007] The flax may be fresh or partly dried but remains moist, having a preferred moisture
content in the range from 30 to 70% by weight of the dry flax. The flax may be deseeded.
[0008] The treatment of the flax preferably takes place in sealed containers such as in
containers made of plastics material, for example polythene bags.
[0009] In a preferred embodiment of the invention, sulphur dioxide is released into sealed
batches of moist flax, which may be in the forms of bales or beets. The sulphur dioxide
diffuses readily through the flax combining with the moisture present to form a weak
solution of sulphurous acid, thus reducing the pH of the flax.
[0010] The action of the sulphur dioxide inhibits the activity of micro-organisms likely
to produce cellulytic and other enzymes which can damage and weaken the flax fibres.
However, partial retting of the flax also occurs probably through the weakening of
bonds between fibre bundles by direct acidification.
[0011] In order that the invention may be more readily understood, two specific embodiments
thereof will now be described by way of example only:-
Example 1
[0012] Flax straw was pulled mechanically and picked up by a large round baler, making bales
of about 400 kg with a moisture content of about 65%. The bales were taken to the
store where they were weighed and placed into large 1000 gauge black polythene bags.
Sulphur dioxide equivalent to 2% by weight of the flax dry matter was released into
the bag from a cylinder, prior to sealing the bag. The sealed bags were opened after
3 months and the bales unrolled and made up into beets which were dried in the open
air. The flax was then deseeded, scutched and hackled in the normal way to produce
a slightly bleached and partly retted flax fibre.
Example 2
[0013] Flax straw was pulled mechanically and made up by hand into beets straight after
pulling (65% moisture content) or after a period of wilting (55% and 35% moisture
content). The beets were placed into large polythene sacks and sealed either without
treatment or after treatment with formic acid, propionic acid or sulphur dioxide at
2% by weight of dry flax.
[0014] The sacks were opened after a six week storage period and examined for the presence
of moulds and for the quality of the flax. It was found that the formic acid and propionic
treated flaxes, untreated by sulphur dioxide, showed visible mould development and
the strength of the fibre was reduced to a variable degree. The sulphur dioxide material
was bleached to a yellow colour, and had no visible mould growth present. It also
had a very consistent presentation in terms of fibre fineness and strength, and quality
was on average superior to that of the other treatments at all three moisture contents.
[0015] It is to be understood that the above described embodiments are by way of illustration
only and many modifications and variations may be made within the scope of the invention.
1. A method of treatment of flax straw comprising the infusion of a gas through moist
flax straw so as to provide conditions which inhibit the activity of any micro-organism
which causes deterioration of the flax.
2. A method of treatment of flax straw as claimed in claim 1, wherein said method improves
the processing characteristics of the straw.
3. A method of treatment of flax straw as claimed in claim 1 or claim 2, wherein the
gas comprises sulphur dioxide.
4. A method of treatment of flax straw as claimed in claim 1, claim 2 or claim 3, wherein
2% or less of the gas by weight of the dry flax is used.
5. A method of treatment of flax straw as claimed in any preceding claim, wherein the
moisture content of the flax is in the range from 30% to 70% by weight of the dry
flax.
6. A method of treatment of flax as claimed in any preceding claim, wherein said method
is carried out in a sealed container.