(19)
(11) EP 0 510 746 A3

(12) EUROPEAN PATENT APPLICATION

(88) Date of publication A3:
08.09.1993 Bulletin 1993/36

(43) Date of publication A2:
28.10.1992 Bulletin 1992/44

(21) Application number: 92200993.1

(22) Date of filing: 07.04.1992
(51) International Patent Classification (IPC)5C11D 11/00, C11D 17/06
(84) Designated Contracting States:
AT BE CH DE DK ES FR GB GR IT LI LU NL PT SE

(30) Priority: 12.04.1991 EP 91870061
10.03.1992 EP 92870038

(71) Applicant: THE PROCTER & GAMBLE COMPANY
Cincinnati, Ohio 45202 (US)

(72) Inventors:
  • Goovaerts, Luc
    B-3150 Haacht (BE)
  • Vega, Jose Luis
    B-1853 Strombeek-Bever (BE)

(74) Representative: Canonici, Jean-Jacques et al
Procter & Gamble European Technical Center N.V. Temselaan 100
1853 Strombeek-Bever
1853 Strombeek-Bever (BE)


(56) References cited: : 
   
       


    (54) Process for preparing condensed detergent granules


    (57) The present invention relates to a process for making a free flowing granular detergent comprising : mixing an effective amount of an aqueous surfactant paste having a detergency activity of at least 40% and an effective amount of a dry detergency powder, said surfactant paste active and builder or powder having a ratio of 0.05:1 to 19:1 to form a mix; rapidly forming a uniform mixture from said mix at a temperature of from about 0°C to about 80 C; granulating said mixture into discrete detergent granules using a high speed mixing at a tip speed of about 5-50 m/sec; and wherein said surfactant paste is comprised of at least one anionic surfactant, and any other surfactants, if present, are selected from the group of anionic, zwitterionic, ampholytic and cationic surfactants and mixtures thereof; and wherein said mixing and granulating are conducted simultaneously, or immediately sequentially.
    The nil-surfactant components of the finished granular detergent other than the granulated active paste, comprise a (relatively small) part of the total amount of builder, another part of the builder having been used for granulation. The nil active components can be spray-dried to form a powder having good color, frangibility, dissolution properties and desirable density and size characteristics for direct dry mixing with other ingredients of the finished granular detergent.





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