| (19) |
 |
|
(11) |
EP 0 510 746 A3 |
| (12) |
EUROPEAN PATENT APPLICATION |
| (88) |
Date of publication A3: |
|
08.09.1993 Bulletin 1993/36 |
| (43) |
Date of publication A2: |
|
28.10.1992 Bulletin 1992/44 |
| (22) |
Date of filing: 07.04.1992 |
|
|
| (84) |
Designated Contracting States: |
|
AT BE CH DE DK ES FR GB GR IT LI LU NL PT SE |
| (30) |
Priority: |
12.04.1991 EP 91870061 10.03.1992 EP 92870038
|
| (71) |
Applicant: THE PROCTER & GAMBLE COMPANY |
|
Cincinnati,
Ohio 45202 (US) |
|
| (72) |
Inventors: |
|
- Goovaerts, Luc
B-3150 Haacht (BE)
- Vega, Jose Luis
B-1853 Strombeek-Bever (BE)
|
| (74) |
Representative: Canonici, Jean-Jacques et al |
|
Procter & Gamble European Technical Center N.V.
Temselaan 100 1853 Strombeek-Bever 1853 Strombeek-Bever (BE) |
|
| |
|
| (54) |
Process for preparing condensed detergent granules |
(57) The present invention relates to a process for making a free flowing granular detergent
comprising : mixing an effective amount of an aqueous surfactant paste having a detergency
activity of at least 40% and an effective amount of a dry detergency powder, said
surfactant paste active and builder or powder having a ratio of 0.05:1 to 19:1 to
form a mix; rapidly forming a uniform mixture from said mix at a temperature of from
about 0°C to about 80 C; granulating said mixture into discrete detergent granules
using a high speed mixing at a tip speed of about 5-50 m/sec; and wherein said surfactant
paste is comprised of at least one anionic surfactant, and any other surfactants,
if present, are selected from the group of anionic, zwitterionic, ampholytic and cationic
surfactants and mixtures thereof; and wherein said mixing and granulating are conducted
simultaneously, or immediately sequentially.
The nil-surfactant components of the finished granular detergent other than the granulated
active paste, comprise a (relatively small) part of the total amount of builder, another
part of the builder having been used for granulation. The nil active components can
be spray-dried to form a powder having good color, frangibility, dissolution properties
and desirable density and size characteristics for direct dry mixing with other ingredients
of the finished granular detergent.
