[0001] This invention relates to a steel hardening method and apparatus therefor, for example
for hardening steel parts which have previously had surface treatment such as carburizing,
carbonitriding, nitriding and the like.
[0002] A steel-hardening step is performed in various heat treatments in order to improve
the hardness of the steel. However there are problems associated with these methods,
for example changes in shape and distortions in size can easily occur in steel parts
during this hardening. Therefore, in order to prevent these changes and distortions
in the steel parts, it is important with these methods to cool quickly through the
critical temperature zone and then slowly through the dangerous temperature zone.
Ordinarily, the martempering or the time quenching is utilized as the hardening method
and salt or high temperature quenching oil is utilized as the cooling agent, particularly
for steel parts and the like in which any change in the shape and/or distortions are
unacceptable.
[0003] In the martempering process, steel parts maintained at the hardening temperature
are dipped into a salt bath or a high temperature quenching oil bath maintained at
a temperature higher than the Ms point of the steel parts to be treated. The parts
remain dipped in the bath whose temperature is preferably slightly higher than the
Ms point for a while and, when the steel parts reach a predetermined temperature,
the steel parts are picked up from the bath and cooled down so as to make the martensitic
transformation. Or, in the case where time quenching is simultaneously utilized, a
method of making the transformation is carried out by dipping the steel parts in a
secondary bath maintained at a temperature lower than the Ms point.
[0004] In the aforementioned ordinary hardening a steel part subjected to the martempering
was carburized at approximately 0.8% C and was limited to only the outer surface of
total carburization.
[0005] The inventors of present invention have found that by mixing the quenching oil by
the action of mixing blades, which is the technique usually carried out to maintain
the quenching bath at a predetermined uniform temperature in order to uniformly cool
down the steel parts dipped therein, there is a tendency for the steel parts to undergo
a change of shape and/or distortions.
[0006] The reason for this is that, when the mixing blades are rotated in the quenching
oil, air is sucked into the oil through turbulence, in particular from a rotary shaft
of the mixing blades. This air is mixed during the circulation process of the quenching
oil by the mixing blades and forms bubbles in the oil. The bubbles are dispersed in
the oil by the mixing blades and adhere on the surface of the steel parts which can
cause uneven cooling of the steel parts. This causes differences in the heat treatment,
in particular at the surface regions which can result in a change of shape and/or
distortions in measurement. This phenomenon was particularly significant when the
mixing blades were rotated at high speed for quick cooling because a large amount
of bubbles were formed in the quenching oil.
[0007] Further, it was found that the usual quenching baths were unnecessarily large in
order that the mixing blades could be installed to evenly mix the quenching oil and
to provide a path of circulating quenching oil. This frequently resulted in local
variations in the flow of the quenching oil and hence, variations in its temperature.
These variations, or even stagnation of the quenching oil can result in uneven cooling
of the steel parts which results in a variation of heat treatment, especially to the
treated surface regions, giving rise to internal stresses changing the shape and/or
distorting the size of the steel parts.
[0008] Furthermore, in a subsequent air cooling process, the characteristics of the environment
surrounding the steel parts such as air temperature, humidity, wind and the like were
factors which could cause variation in treatment of the steel part, again in particular
at the surface, which could result in a change in shape, distortions in measurement
and the like.
[0009] Further, in the time quenching method, the time difference in dipping the steel parts
into the secondary bath, that is, the time difference taken during dipping for the
top and bottom of the steel parts to be dipped, causes a further variation in cooling
time and therefore cooling rate between and throughout the steel parts since it takes
a relatively long time to dip items by a cylinder or a crane during batch dipping.
[0010] Therefore, at present the prevention of variations such as a change of the shape
and a distortion of measurement due to the transformation at the inner part of steel
parts maintained at lower carbon content than 0.8% C depends on experimental overlaying
method or improvement of an overlaying jig.
[0011] Viewed from one aspect the present invention provides a method of hardening steel,
comprising dipping steel to be hardened in a quenching region, characterised by causing
quenching fluid to flow upwardly from below the steel dipped into the quenching region,
and removing the quenching fluid from above the steel, whereby the steel is cooled
by said flow of quenching fluid.
[0012] Viewed from another aspect the present invention provides steel hardening apparatus
comprising a quenching region arranged to receive steel to be hardened, characterised
in that the quenching region is provided with inlet means for supplying quenching
fluid to a lower part thereof, and outlet means for removing quenching fluid from
an upper part thereof.
[0013] There is thus provided a hardening method and apparatus which avoids the formation
of bubbles in the quenching fluid, e.g. quenching oil, during hardening. For that
purpose, in the present invention, quenching fluid is supplied, preferably continuously,
from the bottom of the steel parts and circulated upwards without using mixing blades,
unlike the conventional method.
[0014] In order to help prevent any cooling variation due to uneven flow, stagnation or
the like of quenching fluid which may occur when a large quenching bath is used, the
quenching region may be defined in a quenching chamber which surrounds the up and
down path for an elevator for carrying the steel to be hardened. In other words, the
quenching region may be relatively small, preferably as small as possible whilst still
enabling the elevator to move up and down.
[0015] Preferably, the outlet means is in the form of an overflow. In a preferred embodiment
the quenching region is defined in a quenching chamber disposed in a quenching bath,
and the overflow from the quenching chamber is arranged to be above the level of quenching
fluid in the quenching bath.
[0016] Thus, a preferred hardening method comprises providing a separated quenching region
surrounding the up and down path of the elevator in said quenching bath, flowing quenching
fluid upward by supplying thereof from the bottom of the steel parts carried down
by the elevator into said quenching region and cooling down the steel parts during
overflow of said quenching fluid from the top of the quenching region into said quenching
bath.
[0017] Preferred apparatus is constructed so as to provide a quenching region surrounding
the up and down path of an elevator in a quenching bath so that the upper end of the
quenching region is lower than the upper end of said quenching bath and the quenching
region itself is separated from said quenching bath and a supplying part of quenching
fluid at the bottom of said quenching region.
[0018] Certain preferred embodiments of the present invention will now be described, by
way of example only, and with reference to the accompanying drawings, in which:
Fig. 1 shows the apparatus of a first preferred embodiment of the present invention;
Fig. 2 shows an enlargement of the quenching tank of a second preferred embodiment
of the present invention;
Fig. 3 shows a plan view of the apparatus shown in Fig. 2;
Fig. 4 shows the apparatus according to a third preferred embodiment of the present
invention;
Fig. 5 shows a plan view of the apparatus shown in Fig. 4;
Fig. 6 shows a perspective view of a test piece; and
Fig. 7 shows a plan view of the test piece of Fig. 6 indicating each measurement position.
[0019] In the drawings, a quenching tank 1 is provided with a quenching bath 2. An elevator
5, having transfer apparatus 4 to load and carry the steel parts 3 after their carburizing
treatment or the like, is provided within the quenching tank 1 to lower the steel
parts 3 into the quenching bath 2. Numeral 6 in the drawings designates a quenching
fluid, preferably oil.
[0020] In the preferred embodiments of the present invention, there is be provided a quenching
region 8 which surrounds the elevator when immersed in the quenching bath 2. This
region can be defined as the volume moved through by the up and down path of the steel
parts 3 in said quenching bath 2 and preferably the surface of the quenching oil 6
in the quenching region 8 is higher than the surface of the quenching oil 6 in the
quenching bath 2, with preferably a supply for the quenching oil 6 provided in a lower
region or bottom of the quenching region 8.
[0021] In the embodiment shown in Fig. 1, the quenching region 8 is arranged so as to have
a space 7 between the bottom part 18 of said quenching bath 2 and the quenching region
8. Further, said quenching region 8 is constructed so as to be as small as possible
but large enough to allow up and down movement of said elevator 5. Consequently, quenching
oil 6 can flow quickly upward to enhance the cooling effect experienced by the stel
parts 3, as explained in detail later.
[0022] Further, in this preferred embodiment, there is provided an auxiliary chamber 9 around
the bottom of said quenching region 8 so as to enclose the space 7 together with the
bottom part 18 of said quenching bath 2, and to separate the space 7 from the upper
part of the quenching bath 2. This auxiliary chamber 9 provided on the bottom part
18 of said quenching bath 2 can be used to support the quenching region 8.
[0023] Further, a supply pipe 10 of quenching oil 6 is connected to said auxiliary chamber
9. A circulating pipe line 13 is connected to a circulating pump 12 arranged to feed
said supply pipe 10 through a flow control valve 11, and hence the circulating pipe
line 13 is coupled to said quenching bath 2.
[0024] Preferably, the supply pipe 10 may be split into a number of further supply pipes
and connected to said auxiliary chamber 9 so that quenching oil is supplied evenly
into the auxiliary chamber 9. Consequently, an even supply of quenching oil 6 from
the auxiliary chamber 9 into said quenching region 8 results, thereby providing further
homogeneous cooling of the steel parts 3 in the quenching region 8 so that changes
of shape and/or distortions in size of the steel parts 3 can be substantially prevented.
[0025] A second preferred embodiment of the apparatus is shown in Figs. 2 and 3. These figures
show split supply pipes 10a, 10b, 10c and 10d branched from the supply pipe 10 extending
from the circulating pump 12 and the flow control valve 11, and these are evenly connected
to both sides of the auxiliary chamber 9 located in the center of the quenching bath
2.
[0026] Further, if the end of each split supply pipe 10a, 10b, 10c and 10d is constructed
so as to turn up as shown in Fig. 2, and the supplied quenching oil 6 is directed
towards the roof of the auxiliary chamber 9, then the quenching oil 6 supplied to
the quenching region 8 is further homogenized before being supplied to the bottom
of the quenching region 8, preferably in a laminar flow so that the steel parts are
cooled down evenly.
[0027] In Fig. 1, numeral 14 designates a circulation path connecting the upper and the
lower parts of the quenching region 8 which may be provided optionally. In the circulation
path 14, ideally a circulation pump 15 is provided at approximately mid-way. Further,
the circulation pump 15 is preferably of a reciprocal type.
[0028] This circulation path 14 and the circulation pump 15 are not shown in Figs. 2 and
3, but it is preferable to instal them also in these embodiments.
[0029] Furthermore, as shown in Fig. 1, there is provided an entrance door 16 to the quenching
tank 1 and an exit door 17 from the quenching tank 1.
[0030] Figs. 4 and 5 show apparatus according to a third preferred embodiment of the present
invention. The main difference between this embodiment and the embodiment shown in
Fig. 1 is that the supply pipe 10 is branched at the bottom of the quenching region
8 to form a series of supply pipes 10a, 10b, 10c and 10d, each with supply nozzles
19 arranged equidistantly therealong. In addition, the auxiliary chamber 9 is not
provided.
[0031] According to this embodiment, quenching oil 6 ie. supplied from the supply nozzles
19 on the supply pipes 10a, 10b, 10c and 10d, is directed towards the bottom part
18 before passing into the quenching region 8 to cool down the steel parts 3.
[0032] In the apparatus of the first embodiment shown in Fig. 1 or the second preferred
embodiment shown in Figs. 2 and 3, the steel parts 3 after heat treatment such as
carburizing and the like are loaded onto the elevator 5 in the quenching tank 1 through
the entrance door 16. Then both the elevator 5 and the steel parts 3 are lowered until
the steel parts 3 are dipped in the oil 6 in the quenching region 8 for their hardening
treatment. Before, or at the same time as the dipping, the flow control valve 11 is
opened and the circulation pump 12 is operated. Consequently, quenching oil 6 is supplied
into the auxiliary chamber 9 from the supply pipe 10. Quenching oil 6 flowing into
the auxiliary chamber 9, which is wider than the diameter of the supply pipe 10, reduces
its flow speed, which is controlled to remain constant, and allowed to uniformly flow
into the quenching region 8 from the whole area under the quenching region 8. The
steel parts 3 in the quenching region 8 are quickly cooled by the upward flowing quenching
oil 6, which can then overflow from the top of the quenching region 8 into the quenching
bath 2. Thus, quenching oil 6 is circulated. The cooling process aforementioned is
substantially the same for the apparatus of the embodiment shown in Figs. 4 and 5.
[0033] In the preferred embodiments of the present invention, substantially no bubbles are
generated in the quenching oil 6 because mixing blades are not used for maintaining
a uniform temperature of the quenching oil as aforementioned. Further, quenching oil
6 that is kept at a constant temperature, for example approximately 160°C, can be
supplied and allowed to flow upward around the steel parts 3 continuously and substantially
uniformaly at a predetermined rate.
[0034] Then, in a preferred embodiment, the flow control valve 11 is closed when the steel
parts 3 have been cooled down to a predetermined temperature, for example between
450 to 470°C. Consequently, quenching oil 6 in the quenching region 8 will be heated
up to a certain level by heat released from the cooling steel parts 3.
[0035] Further, if the steel parts 3 have still not sufficiently cooled down to the predetermined
temperature as a result of closing said flow control valve 11, the flow control valve
11 can be re-opened so that quenching oil 6 can be supplied until the steel parts
3 are cooled down to the predetermined temperature. Afterwards, the steel parts 3
may be kept for a further period of time in the quenching region to slowly cool down
further.
[0036] Furthermore, when the supply of quenching oil 6 is stopped, the circulation pump
15 may be operated so as to circulate quenching oil 6 in the quenching region 8 in
order to avoid temperature differences occurring between the upper and lower parts
of the quenching region 8.
[0037] Tests were carried out using test pieces 20 as shown in Fig. 6, that is, sleeves
(100mm in length and 60mm in diameter) with a notch or key gutter which had all been
subjected to the same carburizing treatment. With these test pieces, distortions after
various hardening treatments were determined. Results obtained are shown in the following
Tables 1 and 2. Fig. 7 shows the measurement points on the test piece 20. "Upper"
and "Lower" in Tables 1 and 2 indicate the upper and the lower parts of the test piece
20 shown in Fig. 6, respectively.

[0038] The data shown in Table 1 was taken from a test piece 20 before and after a hardening
treatment by the apparatus shown in Fig. 1, and the data shown in Table 2 was taken
from a test piece 20 before and after hardening treatment by the apparatus shown in
Figs. 4 and 5.
[0039] According to Tables 1 and 2, the range of actual measured distortion at both the
upper and lower parts of the test pieces 20 treated by the apparatus and the method
in accordance with the present invention was very small compared to each of the conventional
methods. These results confirm that the present invention can provide a superior effect
in preventing changes in shape and distortions of the steel parts. This also demonstrates
that there is no variation in the treated layer of the steel parts. The tests also
demonstrate that an advantageous treatment method can be effectively implemented by
the apparatus described above.
1. A method of hardening steel, comprising dipping steel to be hardened in a quenching
region, characterised by causing quenching fluid to flow upwardly from below the steel
dipped into the quenching region, and removing the quenching fluid from above the
steel, whereby the steel is cooled by said flow of quenching fluid.
2. Steel hardening apparatus comprising a quenching region arranged to receive steel
to be hardened, characterised in that the quenching region is provided with inlet
means for supplying quenching fluid to a lower part thereof, and outlet means for
removing quenching fluid from an upper part thereof.
3. Steel hardening apparatus as claimed in claim 2, wherein the outlet means is in the
form of an overflow.
4. Steel hardening apparatus as claimed in claim 3, wherein the quenching region is defined
in a quenching chamber disposed in a quenching bath, and wherein the overflow from
the quenching chamber is arranged to be above the level of quenching fluid in the
quenching bath.
5. Steel hardening apparatus as claimed in claim 4, wherein an auxiliary chamber separated
from the upper part of the quenching bath is provided adjacent to said lower part
of the quenching chamber.
6. Steel hardening apparatus as claimed in claim 5, comprising a supply pipe for supplying
quenching fluid to the auxiliary chamber via a plurality of inlets.
7. Steel hardening apparatus as claimed in claim 2, 3 or 4, wherein the inlet means comprises
a plurality of supply nozzles provided on the under surfaces of supply pipes.
8. A method of hardening steel by using the apparatus as claimed in any of claims 2 to
7.