(19) |
 |
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(11) |
EP 1 246 004 A3 |
(12) |
EUROPEAN PATENT APPLICATION |
(88) |
Date of publication A3: |
|
26.07.2006 Bulletin 2006/30 |
(43) |
Date of publication A2: |
|
02.10.2002 Bulletin 2002/40 |
(22) |
Date of filing: 15.02.2002 |
|
(51) |
International Patent Classification (IPC):
|
|
(84) |
Designated Contracting States: |
|
AT BE CH CY DE DK ES FI FR GB GR IE IT LI LU MC NL PT SE TR |
|
Designated Extension States: |
|
AL LT LV MK RO SI |
(30) |
Priority: |
29.03.2001 EP 01000093
|
(71) |
Applicant: AGFA-GEVAERT |
|
2640 Mortsel (BE) |
|
(72) |
Inventors: |
|
- Viaene, Kris
c/o AGFA-GEVAERT
2640, Mortsel (BE)
- Gilleir, Jan
c/o AGFA-GEVAERT
2640, Mortsel (BE)
- De Roover, Geert
c/o AGFA-GEVAERT
2640, Mortsel (BE)
|
|
|
|
(54) |
Method of preparing co-precipitated microcrystalline dye dispersions and layers coated
therewith in materials |
(57) A method has been disclosed for preparing a co-precipitated microcrystalline dye
dispersion, the absorption spectrum of which exceeds the summoned spectra of individually
dispersed dyes, which comprises, as consecutive preparation steps: adding to one vessel,
an amount of at least one pentamethine oxonol-type barbituric acid filter dye having
ionizable sites in its molecular structure; adding thereto an aqueous alkaline solution
in an amount sufficient to completely dissolve the said filter dye while stirring
the solution thus formed; adding in another vessel, to an amount of at least one pyrrole
type filter dye, an amount of water, followed by adding of an aqueous alkaline solution
and a surfactant; followed, after having completely dissolved (under stirring conditions)
the said pyrrole type filter dye, by adding to the solution thus formed in the other
vessel, the solution formed in the one vessel; adding an aqueous acidic solution up
to a pH of less than 3.0; adding an aqueous alkaline solution up to a pH in the range
from 4.0 up to 5.5; followed by adding a binder in order to make the dispersion thus
obtained ready-for-coating in a filter dye layer on a support, suitable for use as
antihalation undercoat layer between said support and a light-sensitive layer or as
a backing layer of said material, or as layer covering the light-sensitive layer,
thus providing safelight protection.

