(19)
(11) EP 1 250 558 B1

(12) EUROPEAN PATENT SPECIFICATION

(45) Mention of the grant of the patent:
23.03.2005 Bulletin 2005/12

(21) Application number: 01946931.1

(22) Date of filing: 24.01.2001
(51) International Patent Classification (IPC)7F26B 3/08, F26B 17/10
(86) International application number:
PCT/DK2001/000051
(87) International publication number:
WO 2001/055657 (02.08.2001 Gazette 2001/31)

(54)

METHOD AND APPARATUS FOR FLUID-BED DRYING

VERFAHREN UND VORRICHTUNG ZUR FLIESSBETTROCKNUNG

PROCEDE ET DISPOSITIF DE SECHAGE A LIT FLUIDISE


(84) Designated Contracting States:
DE DK GB

(30) Priority: 25.01.2000 DK 200000116

(43) Date of publication of application:
23.10.2002 Bulletin 2002/43

(73) Proprietor: APV Nordic A/S, Anhydro
2860 Soborg (DK)

(72) Inventor:
  • KRAGH, Ole, Teglhus
    DK-3100 Hornbaek (DK)

(74) Representative: Kyed, Iver et al
Zacco Denmark A/S Hans Bekkevolds Allé 7
2900 Hellerup
2900 Hellerup (DK)


(56) References cited: : 
EP-A- 0 141 403
DE-A- 2 315 879
DE-A- 1 629 070
DE-A- 3 612 049
   
       
    Note: Within nine months from the publication of the mention of the grant of the European patent, any person may give notice to the European Patent Office of opposition to the European patent granted. Notice of opposition shall be filed in a written reasoned statement. It shall not be deemed to have been filed until the opposition fee has been paid. (Art. 99(1) European Patent Convention).


    Description


    [0001] The present invention relates to a method and apparatus for fluid-bed drying, particularly for simultaneous drying and disintegrating a heat sensitive material comprising the features of the preamble of claim 1, respectively claim 7.

    [0002] Such a method and apparatus are known from DE-A-36 12 049.

    [0003] Fluid bed treatment of various materials has been known for decades and has become a widely used technology in industry and manufacturing, due to the many advances of the technology.

    [0004] EP 0 141 403 discloses an apparatus for heat treatment of a material in a fluid-bed. The material to be treated in the fluid-bed is led to the fluidised bed through an inlet in the side wall of the apparatus above a rotating fluidised layer. The drying air is supplied via an annular distributor surrounding the lower part of the cylindrical wall of the chamber and a circular slit between the conical bottom and the cylindrical wall.

    [0005] In this apparatus larger and smaller lumps of material fall by gravity downwards in the chamber through the fluidized layer and towards the bottom and the slit. Consequently the largest particles of the paste material will fall deepest down in this space and be exposed to a violent impact from the stirrer arm and to a simultaneous, intensive drying of their surfaces from the drying medium, which has its highest temperature in this area. By this combined effect the larger particles will be disintegrated and dried. Smaller and lighter particles will be carried upwards under a simultaneous final drying and eventually leave the drying chamber together with the drying medium through the outlet duct at the top. The drying medium is introduced tangentially through the supply duct into the annular distributor and the circular slit, in order to obtain a preferred rotation of particles and drying medium in the drying chamber.

    [0006] A large variety of cakes and pastelike materials can be successfully dried in the apparatus described in EP 0 141 403.

    [0007] Some materials, however, in particular in their moist form, are of a very sticky nature and tend to deposit on the interior surface of the drying chamber walls. This is particularly inconvenient for heat sensitive materials because of the risk of discolouring and decomposition.

    [0008] Furthermore, the apparatus described in EP 0 141 403 has the disadvantage of requiring a very rigid structure and a very high energy consumption for the stirrer arm at high capacities because of a required wide diameter of the dryer.

    [0009] German patent no. 3612049 and additionally application no. 3633125 discloses an apparatus for drying of hen droppings. The hen droppings are led to the drying chamber via the bottom of the apparatus and introduced to the drying chamber by use of compressed air or a fan which creates an upward stream of air. In the chamber the hen droppings are dried by use of warm air from the chicken run. In general the disclosed apparatus is very ineffective as a drying apparatus, as the temperature is low and the compressed air does not create a fluidised layer.

    [0010] Consequently there has been a need for an apparatus for continuous fluid-bed drying and disintegration of a material in the form of a paste or a filter cake, which is insensitive to a sticky nature of the material.

    [0011] Furthermore there has been a need for an apparatus for continuous fluid-bed drying which allows for large constructions with high capacity without the need for rigid, wide diameter stirrer arms.

    [0012] It is an object of the present invention to provide a method and an apparatus which are particularly useful for drying of heat sensitive materials.

    [0013] This object is obtained by the invention as defined in the claims.

    [0014] The present invention provides a method and apparatus by which heat sensitive material can be dried without the risk of discolouration and decomposition which may appear when drying heat sensitive material.

    [0015] The invention provides a method and apparatus in which the material to be dried is almost instantly after entering the drying chamber caught in an upwards stream of fluidization and drying medium thereby avoiding contact with the hot walls of the apparatus.

    [0016] As mentioned previously one aspect of the invention relates to a method for fluid-bed drying of wet material in a drying chamber comprising an upper part and a lower part, the upper part having an outlet for dry material and the lower part comprising a substantially horizontal bottom part with a least one inlet for wet material and at least one inlet for a stream of fluidization and drying medium, said method comprising the steps of:

    i) providing the wet material to be dried into the drying chamber vertically through an inlet in the horizontal bottom part of said drying chamber,

    ii) exposing the wet material to an upward stream of fluidization and drying medium introduced into said drying chamber, said stream of fluidization and drying medium preferably being introduced through openings partly or totally surrounding said inlet for the wet material,

    iii)drying the wet material in the upward stream of fluidization and drying medium to obtain dry material,

    iv) removing the dry material from the upper part of the drying chamber through the outlet,

    characterized in adjusting the residence time of the material to be dried in the drying chamber by adjusting the size of the opening of an adjustable orifice provided in the upper part of the drying chamber.

    [0017] The fluidization and drying medium is normally a gas, preferably atmospheric air which is heated to a temperature between 100-500 °C.

    [0018] The horizontal bottom part is constructed to be substantially horizontal and comprises one or more inlets for the fluidization and drying medium placed around one or more inlets for the wet material to be dried in such a away that the fluidization and drying medium constitutes a substantially circular or cylindrical upward stream of fluidization and drying medium, and the wet material to be dried enters substantially into the centre of the circular or cylindrical upward stream thereby being caught in the circular or cylindrical upward stream of fluidization and drying medium.

    [0019] In a preferred embodiment of the method according to the invention the wet material to be dried is in the form of a paste or filter cake. Preferably the wet material to be dried is in the form of a mixture of liquid and solid particles wherein the mixture contains 10-90 % by weight of solid material.

    [0020] In another preferred embodiment of the method according to the invention the wet material is stirred and/or disintegrated by stirring and/or disintegrating means in the drying chamber. Preferably the stirring or disintegrating means are blades, paddles, knifes or similar devices fastened to a vertical rotating shaft protruding from the centre of the horizontal bottom.

    [0021] Preferably the residence time for exposing the wet material to be dried to the stream of fluidization and drying medium is adjusted by adjusting the size of orifices. The residence time is the average time required for a given material to be exposed to the fluidization and drying medium to obtain a satisfactory dryness. The skilled person is able to determine the residence time for a material as a matter of routine.

    [0022] The adjustable orifices are placed in the upper part of the drying chamber. Preferably the orifices are adjustable in an annular wall protruding horizontally into at least a part of the upper drying chamber.

    [0023] In a preferred embodiment of the method according to the invention the wet material to be dried is provided to the substantially horizontal bottom part of the drying chamber vertically upwards, preferably by means of paddles or transporting screws or belts, etc.

    [0024] The invention also comprises use of the method for drying wet material, and preferably for drying heat sensitive material.

    [0025] In one aspect the invention relates to an apparatus for fluid-bed drying of wet material with a drying chamber comprising an upper part and a lower part, the upper part having an outlet for dry material and the lower part comprising a substantially horizontal bottom part comprising means for providing an upward stream of fluidization and drying medium in the drying chamber and an inlet for the wet material to be dried, characterized in that said upper part of the drying chamber comprises means for adjusting the upwards stream of fluidization and drying medium, said means being a substantially horizontal projecting edge with adjustable orifices.

    [0026] In a preferred embodiment of the apparatus for fluid-bed drying according to the invention the means for providing an upward stream of fluidization and drying medium is a slit in the substantially horizontal bottom part of the drying chamber, preferably the slit is annular-shaped and preferably the annular slit partly or totally surrounds the inlet for the wet material to be dried. Hereby it is possible to catch the wet material to be dried in the upward stream of fluidization and drying medium and avoid contact with the walls of the drying chamber.

    [0027] It is preferred that the apparatus for fluid-bed drying according to the invention has a drying chamber with an upper cylindrical part and a lower conical part tapering downwards to the substantially horizontal bottom part. Such a construction establishes the optimal conditions for the material flow in the drying chamber.

    [0028] Preferably the inlet for the wet material to be dried is placed substantially in the centre of the substantially horizontal bottom part of the drying chamber to provide the best distribution properties of the wet material to be dried in the upward stream of fluidization and drying medium.

    [0029] In a preferred embodiment of the apparatus for fluid-bed drying according to the invention the drying chamber is supplied with means for stirring and/or disintegrating said stirring and/or disintegrating means preferably being a coaxially placed rotating shaft with wings, paddles, knifes or rods. As the wet material to be dried is often cake or paste-like, there is a need for disintegrating the material to obtain a better drying. Preferably the wet material to be dried is provided upwards to the inlet in the horizontal bottom by means of paddles or transporting screws, belts or pumps.

    [0030] The invention also comprises use of the apparatus for drying wet material, and preferably for drying heat-sensitive material.

    [0031] The invention will hereafter be described in further details with reference to an example and drawings wherein
    Figure 1
    shows a schematically vertical axial section of the apparatus according to the invention.
    Figure 2
    shows the adjustable orifice to determine the residence time for the material in the drying chamber.


    [0032] The apparatus comprises a drying chamber 1 with a cylindrical part 2, a top part 3 and a conical part 4. The cylindrical part has an orifice 6 and an exhaust aperture 5 for the dried product, carried by the drying medium.

    [0033] The drying medium is introduced tangentially through the aperture 7 to the annular distributor 8 and directed into the drying chamber through an annular slit 11, delimited by the conical guide ring 9 and the outer member 10 of the central member 16.

    [0034] A rotating driving member 12 with a shaft 13 is placed . coaxially in the chamber 1 and in the member 16 and is equipped with paddles 14 in the part enclosed by the member 16 and with wings 15 in the part enclosed by the conical part 4 of the chamber 1.

    [0035] The member 16 is provided with a supply member for paste material in the form of a member 17 with a conveyor screw 18. The member 16 and its outer part 10 forms a water jacket containing a medium for control of the temperature of the member 16. Circulation of the medium can be provided for by means of an inlet pipe 19 and an outlet pipe, not shown.

    [0036] The apparatus operates as follows.

    [0037] The material in the form of a cake or paste, which is to be dried and disintegrated, is supplied to the member 16 by means of the screw 18. By rotation of the shaft 13 with the paddles 14 the paste is conveyed upwards and - by act of centrifugal forces - introduced radially outwards into the drying chamber.

    [0038] The diameter of the member 16, the number and design of the paddles 14 and the revolution of the shaft 13 are chosen to allow for a vertical transport mass rate of the paste several times that of the supply screw 18. The reason for this is that whereas the operation of the screw 18 is a part of the overall control of the drying process, the paddles 14 shall supply the paste material to the central drying zone of the chamber in the form of a dispersed cloud of wet material. The wet cloud is met by the hot drying medium emanating form the slit 11 and a violent fluidised bed is established in the lower part of the chamber. Immediate initial evaporation from the dispersed wet material takes place. This is supported by the impact from the wings 15, and possible remaining lumps of paste will dry and disintegrate. A part of the material in the fluidised bed will leave the bed in the form of small lumps and be carried by the rotating drying medium along the conical walls 4 to the upper parts of the chamber. These lumps will however be dry on the surface and consequently not present any risk of adhering to the chamber walls. Lumps, which have a still wet interior, will move upwards along the conical walls 4 until the flow pattern in the chamber will direct them back into the bed in the bottom.

    [0039] For most products it is essential to control the residence time of the product in the drying chamber in order to ensure sufficient drying. The diameter of the central aperture in the orifice 6 has a known effect in terms of the product residence time in the chamber.

    [0040] Due to the rotation of the drying medium the material in the chamber moves upwards in the form of a rotating fluidized bed, the inner limitation of which is the aperture diameter of the orifice 6. When dry material from the.process in the bottom of the chamber is.added to the rotating particle mass, the particles from the surface will escape over the edge of the aperture and a constant particle mass will be maintained in the chamber for a given diameter of the aperture.

    [0041] Consequently a given diameter of the aperture in the orifice together with a given supply of material to the process will define a thereby given residence time for the product mass in the chamber.

    [0042] The present invention incorporates means for control of the residence time during operation by introducing a segment cut out of the orifice ring 6 and equipped with a slide gate 6a which can be adjusted between an open and a closed position by means of an external activator, see figure 2. The activator can be operated manually or remotely and in such a way that the gate can be adjusted to any position between open and closed. In the open position the gate edge towards the centre of the chamber is in its maximum distance from the centre line of the chamber. In its closed position the gate edge towards the centre of the chamber is in line with the rim of the circular opening in the orifice 6.

    [0043] By nature of dynamics the mass of the rotating fluidized material will be defined by the position of the controlling edge of the gate. Consequently the residence time of the particle mass in the chamber can be controlled by adjustment of the gate position.

    [0044] Various modifications of the apparatus are possible within the scope of the claims: Various forms of the paddles 14 or even a full screw may be provided as required for pasty products of different nature.

    [0045] As the drying medium is supplied to the annular distributor 8 through the tangentially directed supply pipe 7, guide blades may be provided in the distributor 8 to change direction of the medium flow through the slit 11. Also one can imagine other executions of the slide gate 6a within the nature of the invention. As an example more gates than one can be applied and the geometry of the individual gate can be varied as well.

    [0046] Though the invention is particularly advantageous for the drying of heat sensitive materials and for high capacity fluid-bed dryers, the apparatus might also be advantageous for the drying of materials, which can be successfully dried on known apparatuses and at small/medium capacity

    Example



    [0047] The invention and the advantages by using it are elucidated by the result from the following experiment, performed in an apparatus as depicted in the drawing.

    [0048] The diameter of the cylindrical part of the apparatus was 1.6 m, and the height from air inlet (9) to the top (3) was 4.4 m. The opening in the orifice 6 was 1 meter . 4161 kg/h wet, pastelike whey concentrate with a total solid content of 85% was fed vertically upwards into the drying chamber and disintegrated by the rotating wings.

    [0049] The drying and fluidizing air in an amount of approx. 20,000 kg/h was introduced into the drying chamber through the annular slit (11) at a velocity of 55 m/s and a temperature of 140 °C.

    [0050] Partly dried material formed a rotating fluidised bed in the chamber, limited by the orifice 6 and the slit 6a, with 50 % opening.

    [0051] Outlet drying air (5) temperature was 70 °C.

    [0052] Dried powder was separated from drying air in a cyclone (not shown).

    [0053] The experiment was closed by the operator after 4 hours. The chamber was free of severe deposits.

    [0054] Flowability of a powder was measured by pouring approx. 10 grams of powder in a wide tipped funnel, resting on a table. When the funnel is removed carefully by hand, the powder will be left as a more or less cone-shaped pile.

    [0055] Flowability is expressed as the angle of repose, measured by means of a handheld goniometer. The normal range for spray dried powders is from 30 degrees or less ("good") to 45 degrees or more ("poor"). (Reference is made to Cheremisinoff, N., Hydrodynamics of Gas-Solids Fluidization,(1984), p. 6.)

    [0056] Residual moisture was measured by weight-loss after 6 hours in oven at 87 °C.

    [0057] Measurement of particle size was made by laser diffraction: The powders were distributed on a small vibrating powder-feeder, suspended in air and blown/sucked through the laser beam of a Malvern Particle Sizer Series 2600.

    [0058] Particle size measurements are expressed as Rosin-Rammler-Bennett (RRB) mean diameter d' and as RRB inclination parameter, n (See e.g. DIN Standard 66145 or many textbooks, including Perry's Chemical Engineers' Handbook, 6th edition (1984) p. 8-5).

    [0059] Caking properties are estimated by examining the crust formed on a spoonful of powder, subjected to 60% and 80% relative humidity at 20 °C for 24 hours.

    [0060] The obtained powder was characterised by a good flowability, residual moisture 2.0 %, no visible discolouring, RRB-particle size d'/n = 132 mum/2.9 and it was non-caking (NB).


    Claims

    1. A method for fluid-bed drying of wet material in a drying chamber (1) comprising an upper part (3) and a lower part (2) (4), the upper part having an outlet (5) for dry material and the lower part comprising a substantially horizontal bottom part with a least one inlet (17) for wet material and at least one inlet (7) for a stream of fluidization and drying medium, said method comprising the steps of:

    i) providing the wet material to be dried into the drying chamber vertically through an inlet (7) in the horizontal bottom part of said drying chamber,

    ii) exposing the wet material to an upward stream of fluidization and drying medium introduced into said drying chamber, said stream of fluidization and drying medium preferably being introduced through openings partly or totally surrounding said inlet for the wet material,

    iii) drying the wet material in the upward stream of fluidization and drying medium to obtain dry material,

    iv) removing the dry material from the upper part of the drying chamber through the outlet (5),

    characterized in adjusting the residence time of the material to be dried in the drying chamber by adjusting the size of the opening of an adjustable orifice provided in the upper part of the drying chamber.
     
    2. A method according to claim 1, characterized in that the wet material is in the form of paste or filter cake.
     
    3. A method according to any one of claims 1 and 2, characterized in that the wet material is heat sensible.
     
    4. A method according to any one of claims 1-3, characterized in that the wet material is stirred and/or disintegrated by stirring and/or disintegrating means (13, 14, 15) in the drying chamber.
     
    5. A method according to any one of claims 1-4, characterized in that the wet material to be dried is provided to the substantially horizontal bottom part of the drying chamber vertically upwards, preferably by means of paddles or transporting screws (18).
     
    6. Use of a method according to claims 1-5 for drying wet material, preferably heat sensitive material.
     
    7. An apparatus for carrying out the method according to claim 1-5 with a drying chamber (1) comprising an upper part (3) and a lower part (2) (4), the upper part having an outlet (5) for dry material and the lower part comprising a substantially horizontal bottom part comprising means (9, 10, 16) for providing an upward stream of fluidization and drying medium in the drying chamber and an inlet (17) for the wet material to be dried, characterized in that said upper part (3) of the drying chamber comprises means (6) for adjusting the upwards stream of fludization and drying medium, said means being a substantially horizontal projecting edge with an adjustable orifice.
     
    8. An apparatus according to claim 7, characterised in that said means for providing an upward stream of fluidization and drying medium is a slit in the substantially horizontal bottom part of said drying chamber, preferably said slit being annular and preferably said annular slit (11) partly or totally surrounds the inlet for the wet material to be dried.
     
    9. An apparatus according to any one of claims 7 and 8, characterized in that said drying chamber has an upper cylindrical part (2) and a lower conical part (4) tapering downwards to the substantially horizontal bottom part.
     
    10. An apparatus according to any one of claims 7-9, characterized in that said inlet for the wet material to be dried is placed substantially in the centre of the substantially horizontal bottom part of said drying chamber
     
    11. An apparatus according to any one of claims 7-10, characterized in that said drying chamber is supplied with means (13, 14, 15) for stirring and/or disintegrating said stirring and/or disintegrating means preferably being a coaxially placed rotating shaft with wings.
     
    12. An apparatus according to any one of claims 7-11, characterized in that the wet material to be dried is provided upwards to the inlet in the horizontal bottom by means of paddles or transporting screws (18).
     
    13. Use of an apparatus according to any one of claims 7-12 for drying wet material, preferably heat-sensitive material.
     


    Ansprüche

    1. Verfahren zur Fließbetttrocknung feuchten Materials in einer Trockenkammer (1) umfassend einen oberen Teil (3) und einen unteren Teil (2) (4), wobei der obere Teil einen Auslass (5) für trockenes Material aufweist und der untere Teil einen im Wesentlichen horizontalen Bodenteil mit wenigstens einem Einlass (17) für feuchtes Material sowie wenigstens einen Einlass (7) für einen Strom eines Fluidisierungs- und Trocknungsmediums umfasst, wobei das Verfahren die Schritte umfasst:

    i) Bereitstellen des feuchten, zu trocknenden Materials in die Trockenkammer vertikal durch einen Einlass (7) in dem horizontalen Bodenteil der Trockenkammer,

    ii) Aussetzen des feuchten Materials einem aufwärts gerichteten Strom eines Fluidisierungs- und Trocknungsmediums, der in die Trockenkammer eingebracht wird, wobei der Strom des Fluidisierungs- und Trocknungsmediums vorzugsweise durch Öffnungen eingebracht wird, die den Einlass für das feuchte Material teilweise oder vollständig umgeben,

    iii) Trocknen des feuchten Materials in dem aufwärts gerichteten Strom des Fluidisierungs- und Trocknungsmediums, um trockenes Material zu erhalten,

    iv) Entfernen des trockenen Materials von dem oberen Teil der Trockenkammer durch den Auslass (5),

       gekennzeichnet durch ein Einstellen der Verweildauer des zu trocknenden Materials in der Trockenkammer durch ein Einstellen der Größe der Öffnung einer einstellbaren Öffnung, die in dem oberen Teil der Trockenkammer bereitgestellt ist,
     
    2. Verfahren nach Anspruch 1, dadurch gekennzeichnet, dass das feuchte Material die Form einer Paste oder eines Filterkuchens aufweist.
     
    3. Verfahren nach einem der Ansprüche 1 oder 2, dadurch gekennzeichnet, dass das feuchte Material wärmeempfindlich ist.
     
    4. Verfahren nach einem der Ansprüche 1 bis 3, dadurch gekennzeichnet, dass das feuchte Material durch Durchmischungs- und/oder Zersetzungsmittel (13, 14, 15) in der Trockenkammer durchmischt und/oder zersetzt wird.
     
    5. Verfahren nach einem der Ansprüche 1 bis 4, dadurch gekennzeichnet, dass das feuchte, zu trocknende Material dem im Wesentlichen horizontalen Bodenteil der Trockenkammer vertikal nach oben vorzugsweise mittels Schaufelrädern oder Vorschubschrauben (18) zugeführt wird.
     
    6. Verwendung eines Verfahrens nach einem der Ansprüche 1 bis 5 zum Trocknen von feuchtem Material und vorzugsweise wärmeempfindlichen Material.
     
    7. Vorrichtung zum Durchführen des Verfahrens nach einem der Ansprüche 1 bis 5 mit einer Trockenkammer (1) umfassend einen oberen Teil (3) sowie einen unteren Teil (2) (4), wobei der obere Teil einen Auslass (5) für trockenes Material aufweist und der untere Teil einen im Wesentlichen horizontalen Bodenteil umfasst, der Mittel (9, 10, 16) zum Bereitstellen eines aufwärts gerichteten Stroms eines Fluidisierungs- und Trocknungsmediums in der Trockenkammer sowie einen Einlass (17) für das feuchte, zu trocknende Material umfasst, dadurch gekennzeichnet, dass der obere Teil (3) der Trockenkammer Mittel (6) zum Einstellen des aufwärts gerichteten Strom des Fluidisierungs- und Trocknungsmediums umfasst, wobei die Mittel eine im Wesentlichen horizontal abstehende Kante mit einer veränderbaren Öffnung sind.
     
    8. Vorrichtung nach Anspruch 7, dadurch gekennzeichnet, dass die Mittel zum Bereitstellen eines aufwärts gerichteten Stroms eines Fluidisierungs- und Trocknungsmediums ein Schlitz in dem im Wesentlichen horizontalen Bodenteil der Trockenkammer sind, wobei der Schlitz vorzugsweise ringförmig ist und. wobei vorzugsweise der ringförmige Schlitz (11) teilweise oder vollständig den Einlass für das feuchte, zu trocknende Material umgibt.
     
    9. Vorrichtung nach einem der Ansprüche 7 oder 8, dadurch gekennzeichnet, dass die Trockenkammer einen oberen zylindrischen Teil (2) sowie einen unteren konischen Teil (4) aufweist, der sich abwärts zu dem im Wesentlichen horizontalen Bodenteil verjüngt.
     
    10. Vorrichtung nach einem der Ansprüche 7 bis 9, dadurch gekennzeichnet, dass der Einlass für das feuchte, zu trocknende Material im Wesentlichen im Zentrum des im Wesentlichen horizontalen Bodenteils der Trockenkammer angeordnet ist.
     
    11. Vorrichtung nach einem der Ansprüche 7 bis 10, dadurch gekennzeichnet, dass die Trockenkammer mit Mitteln (13, 14, 15) zum Durchmischen und/oder Zersetzen ausgestattet ist, wobei die Durchmischungs- und/oder Zersetzungsmittel vorzugsweise eine koaxial angeordnete Rotationswelle mit Flügeln sind.
     
    12. Vorrichtung nach einem der Ansprüche 7 bis 11, dadurch gekennzeichnet, dass das feuchte, zu trocknende Material aufwärts zu dem Einlass in dem horizontalen Boden mittels Schaufelrädern oder Vorschubschrauben (18) bereitgestellt wird.
     
    13. Verwendung einer Vorrichtung nach einem der Ansprüche 7 bis 12 zum Trocknen von feuchtem Material und vorzugsweise wärmeempfindlichen Material.
     


    Revendications

    1. Procédé pour séchage en lit fluidisé de matière humide dans une chambre de séchage (1) comprenant une partie supérieure (3) et une partie inférieure (2) (4), la partie supérieure ayant une sortie (5) pour la matière sèche et la partie inférieure comprenant une partie de fond sensiblement horizontale avec au moins une entrée (17) pour la matière humide et au moins une entrée (7) pour un courant de fluidisation et d'agent de séchage, ledit procédé comprenant les étapes de:

    i) amener la matière humide à sécher dans la chambre de séchage verticalement à travers une entrée (7) dans la partie de fond horizontale de ladite chambre de séchage,

    ii) exposer la matière sèche à un courant ascendant de fluidisation et d'agent de séchage introduit dans ladite chambre de séchage, ledit courant de fluidisation et d'agent de séchage étant de préférence introduit par des ouvertures entourant partiellement ou totalement ladite entrée pour la matière humide,

    iii) sécher la matière humide dans le courant ascendant de fluidisation et d'agent de séchage pour obtenir la matière sèche,

    iv) enlever la matière sèche de la partie supérieure de la chambre de séchage par la sortie (5),

       caractérisé en ce que l'on ajuste le temps de séjour de la matière à sécher dans la chambre de séchage en ajustant la taille de l'ouverture d'un orifice ajustable prévu dans la partie supérieure de la chambre de séchage.
     
    2. Procédé selon la revendication 1, caractérisé en ce que la matière humide se présente sous la forme de pâte ou de gâteau de filtration.
     
    3. Procédé selon l'une quelconque des revendications 1 et 2, caractérisé en ce que la matière humide est sensible à la chaleur.
     
    4. Procédé selon l'une quelconque des revendications 1-3, caractérisé en ce que la matière humide est agitée et/ou désintégrée par des moyens d'agitation et/ou de désintégration (13, 14, 15) dans la chambre de séchage.
     
    5. Procédé selon l'une quelconque des revendications 1-4, caractérisé en ce que la matière humide à sécher est amenée dans la partie de fond sensiblement horizontale de la chambre de séchage verticalement vers le haut, de préférence au moyen de palettes ou de vis de transport (18).
     
    6. Utilisation d'un procédé selon les revendications 1-5 pour sécher une matière humide, de préférence une matière sensible à la chaleur.
     
    7. Appareil pour mettre en oeuvre le procédé selon la revendication 1-5 avec une chambre de séchage (1) comprenant une partie supérieure (3) et une partie inférieure (2) (4), la partie supérieure ayant une sortie (5) pour une matière sèche et la partie inférieure comprenant une partie de fond sensiblement horizontale comprenant des moyens (9, 10, 16) pour fournir un courant ascendant de fluidisation et d'agent de séchage dans la chambre de séchage et une entrée (17) pour la matière humide à sécher, caractérisé en ce que ladite partie supérieure (3) de la chambre de séchage comprend des moyens (6) pour ajuster le courant ascendant de fluidisation et d'agent de séchage, lesdits moyens présentant un bord en saillie sensiblement horizontal avec un orifice ajustable.
     
    8. Appareil selon la revendication 7, caractérisé en ce que ledit moyen pour fournir un courant ascendant de fluidisation et d'agent de séchage est une fente dans la partie de fond sensiblement horizontale de ladite chambre de séchage, de préférence ladite fente étant annulaire et de préférence ladite fente annulaire (11) entourant partiellement ou totalement l'entrée pour la matière humide à sécher.
     
    9. Appareil selon l'une quelconque des revendications 7 et 8, caractérisé en ce que ladite chambre de séchage présente une partie cylindrique supérieure (2) et une partie conique inférieure (4) allant en s'amenuisant vers le bas, vers la partie de fond sensiblement horizontale.
     
    10. Appareil selon l'une quelconque des revendications 7-9, caractérisé en ce que ladite entrée pour la matière humide à sécher est placée sensiblement au centre de la partie de fond sensiblement horizontale de ladite chambre de séchage.
     
    11. Appareil selon l'une quelconque des revendications 7-10, caractérisé en ce que ladite chambre de séchage est dotée de moyens (13, 14, 15) pour agiter et/ou désintégrer, lesdits moyens d'agitation et/ou de désintégration étant de préférence un arbre en rotation coaxialement placé avec des ailettes.
     
    12. Appareil selon l'une quelconque des revendications 7-11, caractérisé en ce que la matière humide à sécher est amenée vers le haut à destination de l'entrée dans le fond horizontal au moyen de palettes ou de vis de transport (18).
     
    13. Utilisation d'un appareil selon l'une quelconque des revendications 7-12 pour sécher une matière humide, de préférence une matière sensible à la chaleur.
     




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