(19)
(11) EP 1 489 927 B1

(12) EUROPEAN PATENT SPECIFICATION

(45) Mention of the grant of the patent:
30.04.2014 Bulletin 2014/18

(21) Application number: 03745478.2

(22) Date of filing: 27.03.2003
(51) International Patent Classification (IPC): 
A24B 15/14(2006.01)
A24B 3/14(2006.01)
(86) International application number:
PCT/NL2003/000235
(87) International publication number:
WO 2003/082030 (09.10.2003 Gazette 2003/41)

(54)

METHOD FOR MANUFACTURING A TOP LOADED CIGARETTE FILLER

VERFAHREN ZUR HERSTELLUNG EINES ZIGARETTENFÜLLSTOFFS MIT OBERLADUNG

PROCÉDÉ DE FABRICATION D'UN MATÉRIAU DE REMPLISSAGE DE CIGARETTE AVEC UNE CHARGE DE SURFACE


(84) Designated Contracting States:
AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HU IE IT LI LU MC NL PT RO SE SI SK TR

(30) Priority: 29.03.2002 NL 1020285

(43) Date of publication of application:
29.12.2004 Bulletin 2004/53

(73) Proprietor: B.V. Deli-Htl Tabak Maatschappij
5642 JA Eindhoven (NL)

(72) Inventors:
  • WIJERS, Steven, Dirk
    NL-5582 DA Waalre (NL)
  • VAN TUYN, Josephus, Alexander, Petrus, Franciscus
    NL-5615 KG Eindhoven (NL)

(74) Representative: Algemeen Octrooi- en Merkenbureau B.V. 
P.O. Box 645
5600 AP Eindhoven
5600 AP Eindhoven (NL)


(56) References cited: : 
EP-A- 0 658 317
DE-A- 19 602 405
US-A- 3 076 729
US-A- 4 681 126
DE-A- 4 334 222
GB-A- 1 203 939
US-A- 4 306 578
   
       
    Note: Within nine months from the publication of the mention of the grant of the European patent, any person may give notice to the European Patent Office of opposition to the European patent granted. Notice of opposition shall be filed in a written reasoned statement. It shall not be deemed to have been filed until the opposition fee has been paid. (Art. 99(1) European Patent Convention).


    Description


    [0001] This invention relates to a method for manufacturing a tobacco sheet with a top layer of tobacco powder, also referred to as top loaded cigarette filler, wherein a base layer on a basis of a fine fraction of tobacco and cellulose fibres is composed, which base layer is provided on one side with a fraction of coarse tobacco, subsequently the total is submitted to a drying treatment. This invention further relates to a top loaded cigarette filler constituted of a base layer of a fraction of fine tobacco and cellulose fibres and a top load of a fraction of course tobacco.

    [0002] The method as referred to in the preamble concerning the manufacturing of the base layer is known from U.S. patent 4,306,578. According to the method known therefrom the base layer is obtained from a aqueous slurry with a high solid content, which aqueous slurry contains a fortification agent composed of unrefined short cellulose fibres with an average length of less than 2.0 mm. Such a unrefined short fibre pulp has a lower apparent viscosity than the commonly known soft wood pulp of the same fibre length allowing the use of the unrefined short fibre formulation at a higher solid content. This results in a need to evaporate less water and accordingly the process can be carried out more economically. The fibres applied in such a method have an average length of less than about 2 mm, preferably varying from 0.5 to about 1.5 mm and a width of 5 to 30 µm, and they are commonly obtained from essentialy hardwood species, like oak timber and poplar timber. The application of such wood cellulose fibres is mainly intended to improve the tensile or tear properties of the base layer.

    [0003] A drawback of the method described above is that the base layer ultimately used in smoking products contains cellulose having no tobacco origin. This drawback could be overcome by e.g. the use of large amounts of high quality binder during the preparation of the base layer. A disadvantage of such a messure is that the end product will contain a lower tobacco content and will furthermore lead to a deteriorated taste. Both effects are undesired. In addition the application of large amounts of high quality binder results in the increase of the price of the final product, which is also commercially undesired.

    [0004] A method for manufacturing a tobacco sheet is known from the German Offenlegungsschrift 19949983, wherein a aqueous slurry of tobacco stems is obtained by grinding uncooked stems in presence of guar as binder. Furthermore, a solution of particular chemicals is prepared, being guar as binder, humidifier, e.g. glycerol, preservative, e.g. sodium benzoate, additives, e.g. sugar syrup, said chemical solution being first mixed with tobacco powder en then the solution containing tobacco powder is admixed with the aqueous stem slurry. The resulting mixture is spread on a conveyer via a continuous process and dried to a sheet.

    [0005] GB 1 203 939 relates to a process of manufacturing a coherent tobacco product wherein a refined pulp of cellulosic fibers is combined with comminuted tobacco and a water-insoluble cellulose derivative.

    [0006] The first object of this invention is to provide a method for manufacturing a base layer wherein substantially no cellulose not originated from tobacco is incorporated.

    [0007] A second object of this invention is to provide a base layer wherein no large amounts of high quality binders are incorporated and in which the strength of the base layer is maintained and no deteriorated taste results.

    [0008] The method according to the present invention comprises the steps as disclosed in claim 1.

    [0009] By the use in the present base layer of cellulose fibres originated for at least 50% from tobacco a base layer is thus obtained which has a small amount of cellulose not originated from tobacco. In a particular embodiment it is preferred that for composing the base layer from a fine fraction of tobacco at least 70%, especially at least 90%, of cellulose fibres originating from tobacco is used. Such percentages of cellulose originating from tobacco provide a base layer which satisfies the desired mechanical properties and in which, in addition, the intended tobacco flavour is maintained. Furthermore large amounts of binders and additives, as used in German Offenlegungsschrift 19949983, can be omitted. It should however be understood that in particular embodiments a certain amount of cellulose fibres from another origin can be used but that the largest part of the cellulose fibres are obtained from tobacco.

    [0010] It is particularly preferred that the composing of the base layer comprises the steps:
    1. i) providing a fine fraction of tobacco,
    2. ii) subjecting tobacco leaf veins to a cooking treatment for forming a slurry of cellulose fibres obtained from tobacco,
    3. iii) combining and mixing the slurry from step ii) with the fine fraction of tobacco from step i), and
    4. iv) dosing the mixture from step iii) on a drying conveyor for forming the base layer.


    [0011] The tobacco fibres are obtained from fibre containing plant parts of the tobacco plant, especially from the middle veins of tobacco leaves which are released as residual material in the processing of tobacco leaves. Such middle veins are also called tobacco stems. By means of the cooking treatment used in step ii) a part of the natural binders, e.g. pectin and hemicellulose, goes into solution and the tobacco fibres are rendered lying free. Subsequently in step iii) the slurry subjected to a cooking treatment is admixed with a fraction of fine tobacco and then the thus resulting mixture is dosed on a drying conveyor which is essentially a endless band of steel and subsequently passes through a drying furnace whereby the top load being the fraction of coarse tobacco is spread over the base layer in a regular layer for obtaining the desired end product.

    [0012] In the present method it is preferred that in a step preceeding step ii) the tobacco leaves veins are crushed and humidified, which decreases the size of the tobacco leaf veins and which promotes the formation of the tobacco leaf veins into a slurry.

    [0013] The cooking treatment according to step ii) is especially carried out under high pressure, particularly at a temperature in the range of 120-200 °C, especially at a temperature of about 150 °C.

    [0014] The dry content of the slurry according to step ii) is especially between 4 and 12 %, preferably between 6 and 10 %.

    [0015] For obtaining optimal properties for the base layer one or more additives selected from the group of plasticizers, binders, diluting agent, fragrances, flavours, preservatives and pH-buffer agents are added to the slurry as obtained in step ii).

    [0016] For the cellulose fibres to impart a good strength to the ultimate base layer it is preferred that the slurry as obtained in step ii) after the cooking treatment is subjected to a grinding treatment. By thus grinding the cellulose fibres in a refiner under wet conditions the fibres are reduced and fibrils are formed on the fibres. Such fibrils insure the cellulose fibres to entangle whereby the desired fortifying performance is optimally imparted.

    [0017] To obtain a sufficient strong base layer it is preferred that the cellulose fibre content in the slurry as obtained from step ii) is at least 15 %, calculated on dry material.

    [0018] As discussed before it is preferred to maintain the amount of cellulose not originated from tobacco in the final base layer at a low level. As appropriate starting material for the present invention a combination of tobacco material can be mentioned. This are generally residual materials from the cigarette industry. Such residual materials are preferably choosen from the group of middle veins of tobacco leaves, tobacco stems, veins with parts of tobacco leaves, tobacco leaf parts and fine dust. The middle veins of tobacco leaves are removed from the leaf in stripperies of tobacco companies to obtain the pure tobacco leaf. This material is often referred to as "tobacco stems". The thus stripped tobaccos are cut in a additional treatment wherein small veins with parts of tobacco leaves are formed which are however not suitable for a direct incorporation into the cigarette. Such small veins with parts of tobacco leaves, also referred to as winnovers, are gravimetrically separated. Furthermore during the overall production process of cigarettes an amount of fine dust is formed, which material is therefore not suitable for direct incorporation into the cigarettes but is suitable however to be used in the present method. The residual materials described above are grinded and screened into two separate fractions being a fine fraction and a coarse fraction whereby the fine fraction is admixed with a slurry of cellulose fibres obtained from tobacco, especially tobacco leaves veins, and dosed on a drying conveyor, additionally provided with a top load of the fraction of course tobacco and subsequently dried for obtaining the desired end product.

    [0019] The present invention further relates to a top loaded cigarette filler constituted of a base layer of a fraction of fine tobacco and cellulose fibres and a top load of a fraction of coarse tobacco obtained according the method according to the present invention wherein, the cellulose fibres in the base layer are for at least 50 %, preferably at least 75%, especially at least 90 %, originated from tobacco, especially tobacco leaf veins wherein the cellulose fibres are obtained by a slurry method, especially as described above.

    [0020] The essence of the present invention is the preparation of a base layer wherein substantially no cellulose not originating from tobacco is incorporated as is commonly used according to the prior art. The present invention especially ensures that in the base layer cellulose fibres originating from tobacco, especially from tobacco leaf veins, are used whereby a base layer is thus obtained which comprises a fine fraction of tobacco and cellulose fibres originating from tobacco.


    Claims

    1. A method for manufacturing a top loaded cigarette filler, the method comprising the steps of dosing a slurry composed on a basis of a fraction of fine tobacco and cellulose fibres on a drying conveyor for forming a base layer, spreading over said base layer a fraction of coarse tobacco for forming a top load on said base layer and subsequently subjecting the total to a drying treatment, wherein said cellulose fibres to be used for manufacturing said base layer are for at least 50 % of cellulose fibres originating from tobacco.
     
    2. A method according to claim 1, characterized in that said cellulose fibres to be used for manufacturing said base layer are for at least 70 %, especially at least 90 %, of cellulose fibres originating from tobacco.
     
    3. A method according to the claims 1-2, characterized in that composing the base layer comprises the steps of: i) providing a fine fraction of tobacco, ii) subjecting tobacco leaf veins to a cooking treatment for forming a slurry of cellulose fibres obtained from tobacco, m) combining and mixing the slurry from step ii) and the fine fraction of tobacco from step i), and iv) dosing the mixture from step iii) on a drying conveyer for forming of the base layer.
     
    4. A method according to claim 3, characterized in that the tobacco leaf veins are crushed and humidified in a step preceeding step ii).
     
    5. A method according to any one of the claims 3-4, characterized in that the cooking treatment according to step ii) is carried out under high pressure.
     
    6. A method according to any one of claims 3-5, characterized in that the cooking treatment according to step ii) is carried out at a temperature in the range of 120-200°C.
     
    7. A method according to any one of claims 3-6, characterized in that the dry content of the slurry according to step ii) is between 4 and 12 %, especially between 6 and 10 %.
     
    8. A method according to any one of the claims 3-7, characterized in that one or more additives are added to the slurry as obtained according to step ii) selected from the group of plasticizers, binders, diluting agents, fragrances, flavours, preservatives and pH-buffer agents.
     
    9. A method according to any one of the preceeding claims 3-8, characterized in that the slurry obtained in step ii) is subjected to a grinding treatment after the cooking treatment.
     
    10. A method according to any one of the preceeding claims 3-9, characterized in that the cellulose fibre content in the slurry from step ii) is at least 15 %, calculated on dry material.
     
    11. A method according to any of the preceeding claims, characterized in that both the fraction of coarse tobacco and the fraction of fine tobacco are originating from residual materials which are obtained by the manufacturing of smoking products.
     
    12. A method according to claim 11, characterized in that the residual materials are selected from the group of middle veins of tobacco leafs, tobacco stems, veins with parts tobacco leaf, tobacco leaf parts and fine dust.
     
    13. A top loaded cigarette filler constituted of a base layer of a fraction of fine tobacco and cellulose. fibres and a top load of a fraction of coarse tobacco obtained according to the method as described in any of the claims 1-12, wherein the cellulose fibres in the base layer are for at least 50 % originated from tobacco.
     
    14. A top loaded cigarette filler according to claim 13, characterized in that said cellulose fibres in the base layer are for at least 70 %, especially for at least 90 %, originated from tobacco.
     
    15. A top loaded cigarette filler according to claims 13-14, characterized in that said cellulose fibres originate from tobacco leaf veins.
     


    Ansprüche

    1. Verfahren zur Herstellung eines Zigarettenfüllstoffs mit Oberladung, wobei das Verfahren die folgenden Schritte umfasst: Dosieren einer Aufschlämmung, die auf Basis eines Anteils von Feintabak und Zellulosefasern zusammengesetzt ist, auf einen Trocknungsförderer zur Ausbildung einer Basisschicht; Verteilen eines Anteils von Grobtabak über der Basisschicht zur Ausbildung einer Oberladung auf der Basisschicht; und anschließendes Trocknen des Ganzen, wobei die zur Herstellung der Basisschicht verwendeten Zellulosefasern wenigstens zu 50% aus Zellulosefasern sind, die von Tabak stammen.
     
    2. Verfahren nach Anspruch 1, dadurch gekennzeichnet, dass die zur Herstellung der Basisschicht verwendeten Zellulosefasern wenigstens zu 70%, insbesondere wenigstens zu 90%, aus Zellulosefasern sind, die von Tabak stammen.
     
    3. Verfahren nach den Ansprüchen 1 bis 2, dadurch gekennzeichnet, dass das Zusammensetzen der Basisschicht die folgenden Schritte umfasst:

    i) Bereitstellen eines Anteils von Feintabak,

    ii) Kochen von Tabakblattrippen zur Ausbildung einer Aufschlämmung von aus Tabak erhaltenen Zellulosefasern,

    iii) Kombinieren und Mischen der Aufschlämmung aus Schritt ii) und des Anteils von Feintabak aus Schritt i), und

    iv) Dosieren der Mischung aus Schritt iii) auf einen Trocknungsförderer zur Ausbildung der Basisschicht.


     
    4. Verfahren nach Anspruch 3, dadurch gekennzeichnet, dass die Tabakblattrippen in einem Schritt ii) vorhergehenden Schritt gebrochen und befeuchtet werden.
     
    5. Verfahren nach einem der Ansprüche 3 bis 4, dadurch gekennzeichnet, dass das Kochen gemäß Schritt ii) unter hohem Druck durchgeführt wird.
     
    6. Verfahren nach einem der Ansprüche 3 bis 5, dadurch gekennzeichnet, dass das Kochen gemäß Schritt ii) bei einer Temperatur im Bereich von 120-220°C durchgeführt wird.
     
    7. Verfahren nach einem der Ansprüche 3 bis 6, dadurch gekennzeichnet, dass der Trockengehalt der Aufschlämmung gemäß Schritt ii) zwischen 4 und 12% beträgt, insbesondere zwischen 6 und 10%.
     
    8. Verfahren nach einem der Ansprüche 3 bis 7, dadurch gekennzeichnet, dass ein oder mehrere Zusätze zu der gemäß Schritt ii) erhaltenen Aufschlämmung hinzugefügt werden, die aus der aus Weichmachern, Bindemitteln, Verdünnungsmitteln, Duftstoffen, Geschmacksstoffen, Konservierungsstoffen und pH-Puffermitteln bestehenden Gruppe ausgewählt werden.
     
    9. Verfahren nach einem der vorhergehenden Ansprüche 3 bis 8, dadurch gekennzeichnet, dass die aus Schritt ii) erhaltene Aufschlämmung nach dem Kochen gemahlen wird.
     
    10. Verfahren nach einem der vorhergehenden Ansprüche 3 bis 9, dadurch gekennzeichnet, dass der auf den Trockengehalt berechnete Zellulosefaseranteil in der Aufschlämmung aus Schritt ii) wenigstens 15% beträgt.
     
    11. Verfahren nach einem der vorhergehenden Ansprüche, dadurch gekennzeichnet, dass sowohl der Anteil an Grobtabak als auch der Anteil an Feintabak von Reststoffen stammen, die beim Herstellen von Tabakprodukten gewonnen wurden.
     
    12. Verfahren nach Anspruch 11, dadurch gekennzeichnet, dass die Reststoffe aus der aus Mittelrippen von Tabakblättern, Tabakstämmen, Rippen mit Teiltabakblatt, Tabakblattteilen und Feinstaub bestehenden Gruppe ausgewählt werden.
     
    13. Zigarettenfüllstoff mit Oberladung, der aus einer Basisschicht eines Anteils von Feintabak und Zellulosefasern und einer Oberladung eines Anteils von Grobtabak gebildet ist, der gemäß dem in einem der Ansprüche 1 bis 12 beschriebenen Verfahren erhalten worden ist, wobei die Zellulosefasern in der Basisschicht wenigstens zu 50% von Tabak stammen.
     
    14. Zigarettenfüllstoff mit Oberladung nach Anspruch 13, dadurch gekennzeichnet, dass die Zellulosefasern in der Basisschicht wenigstens zu 70%, insbesondere wenigstens zu 90%, von Tabak stammen.
     
    15. Zigarettenfüllstoff mit Oberladung nach den Ansprüchen 13 bis 14, dadurch gekennzeichnet, dass die Zellulosefasern von Tabakblattrippen stammen.
     


    Revendications

    1. Procédé de fabrication d'une matière de remplissage de cigarette à charge en surface, le procédé comprenant les étapes de dosage d'une suspension composée sur la base d'une fraction de tabac fin et de fibres de cellulose sur un convoyeur de séchage pour former une couche de base, d'étalement sur ladite couche de base d'une fraction de tabac grossier pour former une charge en surface sur ladite couche de base, puis de soumission de l'ensemble à un traitement de séchage, dans lequel lesdites fibres de cellulose à utiliser pour fabriquer ladite couche de base sont composées à au moins 50 % de fibres de cellulose provenant de tabac.
     
    2. Procédé selon la revendication 1, caractérisé en ce que lesdites fibres de cellulose à utiliser pour fabriquer ladite couche de base sont composées à au moins 70 %, en particulier à au moins 90 %, de fibres de cellulose provenant de tabac.
     
    3. Procédé selon les revendications 1 et 2, caractérisé en ce que la composition de la couche de base comprend les étapes suivantes : i) la mise à disposition d'une fraction fine de tabac, ii) la soumission des veines de feuilles de tabac à un traitement de cuisson pour former une suspension de fibres de cellulose obtenues à partir du tabac, iii) la combinaison et le mélange de la suspension de l'étape ii) et de la fraction fine de tabac de l'étape i), et iv) le dosage du mélange de l'étape iii) sur un convoyeur de séchage pour former la couche de base.
     
    4. Procédé selon la revendication 3, caractérisé en ce que les nervures de feuilles de tabac sont broyées et humidifiées dans une étape antérieure à l'étape ii).
     
    5. Procédé selon l'une quelconque des revendications 3 et 4, caractérisé en ce que le traitement de cuisson selon l'étape ii) est réalisé sous une pression élevée.
     
    6. Procédé selon l'une quelconque des revendications 3 à 5, caractérisé en ce que le traitement de cuisson selon l'étape ii) est réalisé à une température située dans la plage allant de 120 °C à 200 °C.
     
    7. Procédé selon l'une quelconque des revendications 3 à 6, caractérisé en ce que la teneur en matière sèche de la suspension selon l'étape ii) est située entre 4 % et 12 %, en particulier entre 6 % et 10 %.
     
    8. Procédé selon l'une quelconque des revendications 3 à 7, caractérisé en ce qu'un ou plusieurs additifs sont ajoutés à la suspension telle qu'obtenue selon l'étape ii), choisis dans le groupe comprenant les plastifiants, les liants, les agents de dilution, les fragrances, les saveurs, les conservateurs et les agents tampons de pH.
     
    9. Procédé selon l'une quelconque des revendications 3 à 8 précédentes, caractérisé en ce que la suspension obtenue dans l'étape ii) est soumise à un traitement de broyage après le traitement de cuisson.
     
    10. Procédé selon l'une quelconque des revendications 3 à 9 précédentes, caractérisé en ce que la teneur en fibres de cellulose dans la suspension de l'étape ii) est au moins de 15 %, calculée sur la base de la matière sèche.
     
    11. Procédé selon l'une quelconque des revendications précédentes, caractérisé en ce que la fraction de tabac grossier et la fraction de tabac fin proviennent toutes les deux de matières résiduelles qui sont obtenues par la fabrication de produits à fumer.
     
    12. Procédé selon la revendication 11, caractérisé en ce que les matières résiduelles sont choisies dans le groupe comprenant les nervures médianes des feuilles de tabac, les tiges de tabac, les nervures avec des parties de feuille de tabac, les parties de feuille de tabac et les poussières fines.
     
    13. Matière de remplissage de cigarette à charge en surface, constituée d'une couche de base composée d'une fraction de tabac fin et de fibres de cellulose et d'une charge en surface composée d'une fraction de tabac grossier obtenue selon le procédé tel que décrit dans l'une quelconque des revendications 1 à 12, dans laquelle les fibres de cellulose dans la couche de base proviennent à au moins 50 % de tabac.
     
    14. Matière de remplissage de cigarette à charge en surface selon la revendication 13, caractérisée en ce que lesdites fibres de cellulose dans la couche de base proviennent à au moins 70 %, en particulier à au moins 90 %, de tabac.
     
    15. Matière de remplissage de cigarette à charge en surface selon les revendications 13 et 14, caractérisée en ce que lesdites fibres de cellulose proviennent de nervures de feuille de tabac.
     






    Cited references

    REFERENCES CITED IN THE DESCRIPTION



    This list of references cited by the applicant is for the reader's convenience only. It does not form part of the European patent document. Even though great care has been taken in compiling the references, errors or omissions cannot be excluded and the EPO disclaims all liability in this regard.

    Patent documents cited in the description