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EP 1 489 927 B1 |
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EUROPEAN PATENT SPECIFICATION |
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Mention of the grant of the patent: |
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30.04.2014 Bulletin 2014/18 |
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Date of filing: 27.03.2003 |
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International Patent Classification (IPC):
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International application number: |
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PCT/NL2003/000235 |
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International publication number: |
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WO 2003/082030 (09.10.2003 Gazette 2003/41) |
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METHOD FOR MANUFACTURING A TOP LOADED CIGARETTE FILLER
VERFAHREN ZUR HERSTELLUNG EINES ZIGARETTENFÜLLSTOFFS MIT OBERLADUNG
PROCÉDÉ DE FABRICATION D'UN MATÉRIAU DE REMPLISSAGE DE CIGARETTE AVEC UNE CHARGE DE
SURFACE
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Designated Contracting States: |
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AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HU IE IT LI LU MC NL PT RO SE SI SK TR |
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Priority: |
29.03.2002 NL 1020285
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Date of publication of application: |
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29.12.2004 Bulletin 2004/53 |
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Proprietor: B.V. Deli-Htl Tabak Maatschappij |
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5642 JA Eindhoven (NL) |
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Inventors: |
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- WIJERS, Steven, Dirk
NL-5582 DA Waalre (NL)
- VAN TUYN, Josephus, Alexander, Petrus, Franciscus
NL-5615 KG Eindhoven (NL)
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Representative: Algemeen Octrooi- en Merkenbureau B.V. |
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P.O. Box 645 5600 AP Eindhoven 5600 AP Eindhoven (NL) |
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References cited: :
EP-A- 0 658 317 DE-A- 19 602 405 US-A- 3 076 729 US-A- 4 681 126
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DE-A- 4 334 222 GB-A- 1 203 939 US-A- 4 306 578
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| Note: Within nine months from the publication of the mention of the grant of the European
patent, any person may give notice to the European Patent Office of opposition to
the European patent
granted. Notice of opposition shall be filed in a written reasoned statement. It shall
not be deemed to
have been filed until the opposition fee has been paid. (Art. 99(1) European Patent
Convention).
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[0001] This invention relates to a method for manufacturing a tobacco sheet with a top layer
of tobacco powder, also referred to as top loaded cigarette filler, wherein a base
layer on a basis of a fine fraction of tobacco and cellulose fibres is composed, which
base layer is provided on one side with a fraction of coarse tobacco, subsequently
the total is submitted to a drying treatment. This invention further relates to a
top loaded cigarette filler constituted of a base layer of a fraction of fine tobacco
and cellulose fibres and a top load of a fraction of course tobacco.
[0002] The method as referred to in the preamble concerning the manufacturing of the base
layer is known from
U.S. patent 4,306,578. According to the method known therefrom the base layer is obtained from a aqueous
slurry with a high solid content, which aqueous slurry contains a fortification agent
composed of unrefined short cellulose fibres with an average length of less than 2.0
mm. Such a unrefined short fibre pulp has a lower apparent viscosity than the commonly
known soft wood pulp of the same fibre length allowing the use of the unrefined short
fibre formulation at a higher solid content. This results in a need to evaporate less
water and accordingly the process can be carried out more economically. The fibres
applied in such a method have an average length of less than about 2 mm, preferably
varying from 0.5 to about 1.5 mm and a width of 5 to 30 µm, and they are commonly
obtained from essentialy hardwood species, like oak timber and poplar timber. The
application of such wood cellulose fibres is mainly intended to improve the tensile
or tear properties of the base layer.
[0003] A drawback of the method described above is that the base layer ultimately used in
smoking products contains cellulose having no tobacco origin. This drawback could
be overcome by e.g. the use of large amounts of high quality binder during the preparation
of the base layer. A disadvantage of such a messure is that the end product will contain
a lower tobacco content and will furthermore lead to a deteriorated taste. Both effects
are undesired. In addition the application of large amounts of high quality binder
results in the increase of the price of the final product, which is also commercially
undesired.
[0004] A method for manufacturing a tobacco sheet is known from the German Offenlegungsschrift
19949983, wherein a aqueous slurry of tobacco stems is obtained by grinding uncooked stems
in presence of guar as binder. Furthermore, a solution of particular chemicals is
prepared, being guar as binder, humidifier, e.g. glycerol, preservative, e.g. sodium
benzoate, additives, e.g. sugar syrup, said chemical solution being first mixed with
tobacco powder en then the solution containing tobacco powder is admixed with the
aqueous stem slurry. The resulting mixture is spread on a conveyer via a continuous
process and dried to a sheet.
[0005] GB 1 203 939 relates to a process of manufacturing a coherent tobacco product wherein a refined
pulp of cellulosic fibers is combined with comminuted tobacco and a water-insoluble
cellulose derivative.
[0006] The first object of this invention is to provide a method for manufacturing a base
layer wherein substantially no cellulose not originated from tobacco is incorporated.
[0007] A second object of this invention is to provide a base layer wherein no large amounts
of high quality binders are incorporated and in which the strength of the base layer
is maintained and no deteriorated taste results.
[0008] The method according to the present invention comprises the steps as disclosed in
claim 1.
[0009] By the use in the present base layer of cellulose fibres originated for at least
50% from tobacco a base layer is thus obtained which has a small amount of cellulose
not originated from tobacco. In a particular embodiment it is preferred that for composing
the base layer from a fine fraction of tobacco at least 70%, especially at least 90%,
of cellulose fibres originating from tobacco is used. Such percentages of cellulose
originating from tobacco provide a base layer which satisfies the desired mechanical
properties and in which, in addition, the intended tobacco flavour is maintained.
Furthermore large amounts of binders and additives, as used in German Offenlegungsschrift
19949983, can be omitted. It should however be understood that in particular embodiments a
certain amount of cellulose fibres from another origin can be used but that the largest
part of the cellulose fibres are obtained from tobacco.
[0010] It is particularly preferred that the composing of the base layer comprises the steps:
- i) providing a fine fraction of tobacco,
- ii) subjecting tobacco leaf veins to a cooking treatment for forming a slurry of cellulose
fibres obtained from tobacco,
- iii) combining and mixing the slurry from step ii) with the fine fraction of tobacco
from step i), and
- iv) dosing the mixture from step iii) on a drying conveyor for forming the base layer.
[0011] The tobacco fibres are obtained from fibre containing plant parts of the tobacco
plant, especially from the middle veins of tobacco leaves which are released as residual
material in the processing of tobacco leaves. Such middle veins are also called tobacco
stems. By means of the cooking treatment used in step ii) a part of the natural binders,
e.g. pectin and hemicellulose, goes into solution and the tobacco fibres are rendered
lying free. Subsequently in step iii) the slurry subjected to a cooking treatment
is admixed with a fraction of fine tobacco and then the thus resulting mixture is
dosed on a drying conveyor which is essentially a endless band of steel and subsequently
passes through a drying furnace whereby the top load being the fraction of coarse
tobacco is spread over the base layer in a regular layer for obtaining the desired
end product.
[0012] In the present method it is preferred that in a step preceeding step ii) the tobacco
leaves veins are crushed and humidified, which decreases the size of the tobacco leaf
veins and which promotes the formation of the tobacco leaf veins into a slurry.
[0013] The cooking treatment according to step ii) is especially carried out under high
pressure, particularly at a temperature in the range of 120-200 °C, especially at
a temperature of about 150 °C.
[0014] The dry content of the slurry according to step ii) is especially between 4 and 12
%, preferably between 6 and 10 %.
[0015] For obtaining optimal properties for the base layer one or more additives selected
from the group of plasticizers, binders, diluting agent, fragrances, flavours, preservatives
and pH-buffer agents are added to the slurry as obtained in step ii).
[0016] For the cellulose fibres to impart a good strength to the ultimate base layer it
is preferred that the slurry as obtained in step ii) after the cooking treatment is
subjected to a grinding treatment. By thus grinding the cellulose fibres in a refiner
under wet conditions the fibres are reduced and fibrils are formed on the fibres.
Such fibrils insure the cellulose fibres to entangle whereby the desired fortifying
performance is optimally imparted.
[0017] To obtain a sufficient strong base layer it is preferred that the cellulose fibre
content in the slurry as obtained from step ii) is at least 15 %, calculated on dry
material.
[0018] As discussed before it is preferred to maintain the amount of cellulose not originated
from tobacco in the final base layer at a low level. As appropriate starting material
for the present invention a combination of tobacco material can be mentioned. This
are generally residual materials from the cigarette industry. Such residual materials
are preferably choosen from the group of middle veins of tobacco leaves, tobacco stems,
veins with parts of tobacco leaves, tobacco leaf parts and fine dust. The middle veins
of tobacco leaves are removed from the leaf in stripperies of tobacco companies to
obtain the pure tobacco leaf. This material is often referred to as "tobacco stems".
The thus stripped tobaccos are cut in a additional treatment wherein small veins with
parts of tobacco leaves are formed which are however not suitable for a direct incorporation
into the cigarette. Such small veins with parts of tobacco leaves, also referred to
as winnovers, are gravimetrically separated. Furthermore during the overall production
process of cigarettes an amount of fine dust is formed, which material is therefore
not suitable for direct incorporation into the cigarettes but is suitable however
to be used in the present method. The residual materials described above are grinded
and screened into two separate fractions being a fine fraction and a coarse fraction
whereby the fine fraction is admixed with a slurry of cellulose fibres obtained from
tobacco, especially tobacco leaves veins, and dosed on a drying conveyor, additionally
provided with a top load of the fraction of course tobacco and subsequently dried
for obtaining the desired end product.
[0019] The present invention further relates to a top loaded cigarette filler constituted
of a base layer of a fraction of fine tobacco and cellulose fibres and a top load
of a fraction of coarse tobacco obtained according the method according to the present
invention wherein, the cellulose fibres in the base layer are for at least 50 %, preferably
at least 75%, especially at least 90 %, originated from tobacco, especially tobacco
leaf veins wherein the cellulose fibres are obtained by a slurry method, especially
as described above.
[0020] The essence of the present invention is the preparation of a base layer wherein substantially
no cellulose not originating from tobacco is incorporated as is commonly used according
to the prior art. The present invention especially ensures that in the base layer
cellulose fibres originating from tobacco, especially from tobacco leaf veins, are
used whereby a base layer is thus obtained which comprises a fine fraction of tobacco
and cellulose fibres originating from tobacco.
1. A method for manufacturing a top loaded cigarette filler, the method comprising the
steps of dosing a slurry composed on a basis of a fraction of fine tobacco and cellulose
fibres on a drying conveyor for forming a base layer, spreading over said base layer
a fraction of coarse tobacco for forming a top load on said base layer and subsequently
subjecting the total to a drying treatment, wherein said cellulose fibres to be used
for manufacturing said base layer are for at least 50 % of cellulose fibres originating
from tobacco.
2. A method according to claim 1, characterized in that said cellulose fibres to be used for manufacturing said base layer are for at least
70 %, especially at least 90 %, of cellulose fibres originating from tobacco.
3. A method according to the claims 1-2, characterized in that composing the base layer comprises the steps of: i) providing a fine fraction of
tobacco, ii) subjecting tobacco leaf veins to a cooking treatment for forming a slurry
of cellulose fibres obtained from tobacco, m) combining and mixing the slurry from
step ii) and the fine fraction of tobacco from step i), and iv) dosing the mixture
from step iii) on a drying conveyer for forming of the base layer.
4. A method according to claim 3, characterized in that the tobacco leaf veins are crushed and humidified in a step preceeding step ii).
5. A method according to any one of the claims 3-4, characterized in that the cooking treatment according to step ii) is carried out under high pressure.
6. A method according to any one of claims 3-5, characterized in that the cooking treatment according to step ii) is carried out at a temperature in the
range of 120-200°C.
7. A method according to any one of claims 3-6, characterized in that the dry content of the slurry according to step ii) is between 4 and 12 %, especially
between 6 and 10 %.
8. A method according to any one of the claims 3-7, characterized in that one or more additives are added to the slurry as obtained according to step ii) selected
from the group of plasticizers, binders, diluting agents, fragrances, flavours, preservatives
and pH-buffer agents.
9. A method according to any one of the preceeding claims 3-8, characterized in that the slurry obtained in step ii) is subjected to a grinding treatment after the cooking
treatment.
10. A method according to any one of the preceeding claims 3-9, characterized in that the cellulose fibre content in the slurry from step ii) is at least 15 %, calculated
on dry material.
11. A method according to any of the preceeding claims, characterized in that both the fraction of coarse tobacco and the fraction of fine tobacco are originating
from residual materials which are obtained by the manufacturing of smoking products.
12. A method according to claim 11, characterized in that the residual materials are selected from the group of middle veins of tobacco leafs,
tobacco stems, veins with parts tobacco leaf, tobacco leaf parts and fine dust.
13. A top loaded cigarette filler constituted of a base layer of a fraction of fine tobacco
and cellulose. fibres and a top load of a fraction of coarse tobacco obtained according
to the method as described in any of the claims 1-12, wherein the cellulose fibres
in the base layer are for at least 50 % originated from tobacco.
14. A top loaded cigarette filler according to claim 13, characterized in that said cellulose fibres in the base layer are for at least 70 %, especially for at
least 90 %, originated from tobacco.
15. A top loaded cigarette filler according to claims 13-14, characterized in that said cellulose fibres originate from tobacco leaf veins.
1. Verfahren zur Herstellung eines Zigarettenfüllstoffs mit Oberladung, wobei das Verfahren
die folgenden Schritte umfasst: Dosieren einer Aufschlämmung, die auf Basis eines
Anteils von Feintabak und Zellulosefasern zusammengesetzt ist, auf einen Trocknungsförderer
zur Ausbildung einer Basisschicht; Verteilen eines Anteils von Grobtabak über der
Basisschicht zur Ausbildung einer Oberladung auf der Basisschicht; und anschließendes
Trocknen des Ganzen, wobei die zur Herstellung der Basisschicht verwendeten Zellulosefasern
wenigstens zu 50% aus Zellulosefasern sind, die von Tabak stammen.
2. Verfahren nach Anspruch 1, dadurch gekennzeichnet, dass die zur Herstellung der Basisschicht verwendeten Zellulosefasern wenigstens zu 70%,
insbesondere wenigstens zu 90%, aus Zellulosefasern sind, die von Tabak stammen.
3. Verfahren nach den Ansprüchen 1 bis 2,
dadurch gekennzeichnet, dass das Zusammensetzen der Basisschicht die folgenden Schritte umfasst:
i) Bereitstellen eines Anteils von Feintabak,
ii) Kochen von Tabakblattrippen zur Ausbildung einer Aufschlämmung von aus Tabak erhaltenen
Zellulosefasern,
iii) Kombinieren und Mischen der Aufschlämmung aus Schritt ii) und des Anteils von
Feintabak aus Schritt i), und
iv) Dosieren der Mischung aus Schritt iii) auf einen Trocknungsförderer zur Ausbildung
der Basisschicht.
4. Verfahren nach Anspruch 3, dadurch gekennzeichnet, dass die Tabakblattrippen in einem Schritt ii) vorhergehenden Schritt gebrochen und befeuchtet
werden.
5. Verfahren nach einem der Ansprüche 3 bis 4, dadurch gekennzeichnet, dass das Kochen gemäß Schritt ii) unter hohem Druck durchgeführt wird.
6. Verfahren nach einem der Ansprüche 3 bis 5, dadurch gekennzeichnet, dass das Kochen gemäß Schritt ii) bei einer Temperatur im Bereich von 120-220°C durchgeführt
wird.
7. Verfahren nach einem der Ansprüche 3 bis 6, dadurch gekennzeichnet, dass der Trockengehalt der Aufschlämmung gemäß Schritt ii) zwischen 4 und 12% beträgt,
insbesondere zwischen 6 und 10%.
8. Verfahren nach einem der Ansprüche 3 bis 7, dadurch gekennzeichnet, dass ein oder mehrere Zusätze zu der gemäß Schritt ii) erhaltenen Aufschlämmung hinzugefügt
werden, die aus der aus Weichmachern, Bindemitteln, Verdünnungsmitteln, Duftstoffen,
Geschmacksstoffen, Konservierungsstoffen und pH-Puffermitteln bestehenden Gruppe ausgewählt
werden.
9. Verfahren nach einem der vorhergehenden Ansprüche 3 bis 8, dadurch gekennzeichnet, dass die aus Schritt ii) erhaltene Aufschlämmung nach dem Kochen gemahlen wird.
10. Verfahren nach einem der vorhergehenden Ansprüche 3 bis 9, dadurch gekennzeichnet, dass der auf den Trockengehalt berechnete Zellulosefaseranteil in der Aufschlämmung aus
Schritt ii) wenigstens 15% beträgt.
11. Verfahren nach einem der vorhergehenden Ansprüche, dadurch gekennzeichnet, dass sowohl der Anteil an Grobtabak als auch der Anteil an Feintabak von Reststoffen stammen,
die beim Herstellen von Tabakprodukten gewonnen wurden.
12. Verfahren nach Anspruch 11, dadurch gekennzeichnet, dass die Reststoffe aus der aus Mittelrippen von Tabakblättern, Tabakstämmen, Rippen mit
Teiltabakblatt, Tabakblattteilen und Feinstaub bestehenden Gruppe ausgewählt werden.
13. Zigarettenfüllstoff mit Oberladung, der aus einer Basisschicht eines Anteils von Feintabak
und Zellulosefasern und einer Oberladung eines Anteils von Grobtabak gebildet ist,
der gemäß dem in einem der Ansprüche 1 bis 12 beschriebenen Verfahren erhalten worden
ist, wobei die Zellulosefasern in der Basisschicht wenigstens zu 50% von Tabak stammen.
14. Zigarettenfüllstoff mit Oberladung nach Anspruch 13, dadurch gekennzeichnet, dass die Zellulosefasern in der Basisschicht wenigstens zu 70%, insbesondere wenigstens
zu 90%, von Tabak stammen.
15. Zigarettenfüllstoff mit Oberladung nach den Ansprüchen 13 bis 14, dadurch gekennzeichnet, dass die Zellulosefasern von Tabakblattrippen stammen.
1. Procédé de fabrication d'une matière de remplissage de cigarette à charge en surface,
le procédé comprenant les étapes de dosage d'une suspension composée sur la base d'une
fraction de tabac fin et de fibres de cellulose sur un convoyeur de séchage pour former
une couche de base, d'étalement sur ladite couche de base d'une fraction de tabac
grossier pour former une charge en surface sur ladite couche de base, puis de soumission
de l'ensemble à un traitement de séchage, dans lequel lesdites fibres de cellulose
à utiliser pour fabriquer ladite couche de base sont composées à au moins 50 % de
fibres de cellulose provenant de tabac.
2. Procédé selon la revendication 1, caractérisé en ce que lesdites fibres de cellulose à utiliser pour fabriquer ladite couche de base sont
composées à au moins 70 %, en particulier à au moins 90 %, de fibres de cellulose
provenant de tabac.
3. Procédé selon les revendications 1 et 2, caractérisé en ce que la composition de la couche de base comprend les étapes suivantes : i) la mise à
disposition d'une fraction fine de tabac, ii) la soumission des veines de feuilles
de tabac à un traitement de cuisson pour former une suspension de fibres de cellulose
obtenues à partir du tabac, iii) la combinaison et le mélange de la suspension de
l'étape ii) et de la fraction fine de tabac de l'étape i), et iv) le dosage du mélange
de l'étape iii) sur un convoyeur de séchage pour former la couche de base.
4. Procédé selon la revendication 3, caractérisé en ce que les nervures de feuilles de tabac sont broyées et humidifiées dans une étape antérieure
à l'étape ii).
5. Procédé selon l'une quelconque des revendications 3 et 4, caractérisé en ce que le traitement de cuisson selon l'étape ii) est réalisé sous une pression élevée.
6. Procédé selon l'une quelconque des revendications 3 à 5, caractérisé en ce que le traitement de cuisson selon l'étape ii) est réalisé à une température située dans
la plage allant de 120 °C à 200 °C.
7. Procédé selon l'une quelconque des revendications 3 à 6, caractérisé en ce que la teneur en matière sèche de la suspension selon l'étape ii) est située entre 4
% et 12 %, en particulier entre 6 % et 10 %.
8. Procédé selon l'une quelconque des revendications 3 à 7, caractérisé en ce qu'un ou plusieurs additifs sont ajoutés à la suspension telle qu'obtenue selon l'étape
ii), choisis dans le groupe comprenant les plastifiants, les liants, les agents de
dilution, les fragrances, les saveurs, les conservateurs et les agents tampons de
pH.
9. Procédé selon l'une quelconque des revendications 3 à 8 précédentes, caractérisé en ce que la suspension obtenue dans l'étape ii) est soumise à un traitement de broyage après
le traitement de cuisson.
10. Procédé selon l'une quelconque des revendications 3 à 9 précédentes, caractérisé en ce que la teneur en fibres de cellulose dans la suspension de l'étape ii) est au moins de
15 %, calculée sur la base de la matière sèche.
11. Procédé selon l'une quelconque des revendications précédentes, caractérisé en ce que la fraction de tabac grossier et la fraction de tabac fin proviennent toutes les
deux de matières résiduelles qui sont obtenues par la fabrication de produits à fumer.
12. Procédé selon la revendication 11, caractérisé en ce que les matières résiduelles sont choisies dans le groupe comprenant les nervures médianes
des feuilles de tabac, les tiges de tabac, les nervures avec des parties de feuille
de tabac, les parties de feuille de tabac et les poussières fines.
13. Matière de remplissage de cigarette à charge en surface, constituée d'une couche de
base composée d'une fraction de tabac fin et de fibres de cellulose et d'une charge
en surface composée d'une fraction de tabac grossier obtenue selon le procédé tel
que décrit dans l'une quelconque des revendications 1 à 12, dans laquelle les fibres
de cellulose dans la couche de base proviennent à au moins 50 % de tabac.
14. Matière de remplissage de cigarette à charge en surface selon la revendication 13,
caractérisée en ce que lesdites fibres de cellulose dans la couche de base proviennent à au moins 70 %,
en particulier à au moins 90 %, de tabac.
15. Matière de remplissage de cigarette à charge en surface selon les revendications 13
et 14, caractérisée en ce que lesdites fibres de cellulose proviennent de nervures de feuille de tabac.
REFERENCES CITED IN THE DESCRIPTION
This list of references cited by the applicant is for the reader's convenience only.
It does not form part of the European patent document. Even though great care has
been taken in compiling the references, errors or omissions cannot be excluded and
the EPO disclaims all liability in this regard.
Patent documents cited in the description