<?xml version="1.0" encoding="UTF-8"?>
<!DOCTYPE ep-patent-document PUBLIC "-//EPO//EP PATENT DOCUMENT 1.5//EN" "ep-patent-document-v1-5.dtd">
<ep-patent-document id="EP06789015B1" file="EP06789015NWB1.xml" lang="en" country="EP" doc-number="1919699" kind="B1" date-publ="20181121" status="n" dtd-version="ep-patent-document-v1-5">
<SDOBI lang="en"><B000><eptags><B001EP>ATBECHDEDKESFRGBGRITLILUNLSEMCPTIESILTLVFIRO..CY..TRBGCZEEHUPLSK....IS..............................</B001EP><B003EP>*</B003EP><B005EP>J</B005EP><B007EP>BDM Ver 0.1.63 (23 May 2017) -  2100000/0</B007EP></eptags></B000><B100><B110>1919699</B110><B120><B121>EUROPEAN PATENT SPECIFICATION</B121></B120><B130>B1</B130><B140><date>20181121</date></B140><B190>EP</B190></B100><B200><B210>06789015.2</B210><B220><date>20060801</date></B220><B240><B241><date>20080319</date></B241><B242><date>20171120</date></B242></B240><B250>en</B250><B251EP>en</B251EP><B260>en</B260></B200><B300><B310>210581</B310><B320><date>20050824</date></B320><B330><ctry>US</ctry></B330></B300><B400><B405><date>20181121</date><bnum>201847</bnum></B405><B430><date>20080514</date><bnum>200820</bnum></B430><B450><date>20181121</date><bnum>201847</bnum></B450><B452EP><date>20180704</date></B452EP></B400><B500><B510EP><classification-ipcr sequence="1"><text>B32B   3/26        20060101AFI20120531BHEP        </text></classification-ipcr><classification-ipcr sequence="2"><text>B32B   3/00        20060101ALI20120531BHEP        </text></classification-ipcr><classification-ipcr sequence="3"><text>B32B   3/10        20060101ALI20120531BHEP        </text></classification-ipcr><classification-ipcr sequence="4"><text>B32B   5/00        20060101ALI20120531BHEP        </text></classification-ipcr><classification-ipcr sequence="5"><text>B32B   7/12        20060101ALI20120531BHEP        </text></classification-ipcr><classification-ipcr sequence="6"><text>B32B  19/04        20060101ALI20120531BHEP        </text></classification-ipcr><classification-ipcr sequence="7"><text>B32B  23/02        20060101ALI20120531BHEP        </text></classification-ipcr><classification-ipcr sequence="8"><text>B32B  23/06        20060101ALI20120531BHEP        </text></classification-ipcr><classification-ipcr sequence="9"><text>B32B  27/10        20060101ALI20120531BHEP        </text></classification-ipcr><classification-ipcr sequence="10"><text>B32B  29/02        20060101ALI20120531BHEP        </text></classification-ipcr><classification-ipcr sequence="11"><text>B32B  29/04        20060101ALI20120531BHEP        </text></classification-ipcr><classification-ipcr sequence="12"><text>B32B  27/20        20060101ALI20120531BHEP        </text></classification-ipcr><classification-ipcr sequence="13"><text>B32B  29/00        20060101ALI20120531BHEP        </text></classification-ipcr></B510EP><B540><B541>de</B541><B542>LEICHTE PLATTE</B542><B541>en</B541><B542>LIGHTWEIGHT PANEL</B542><B541>fr</B541><B542>PANNEAU LÉGER</B542></B540><B560><B561><text>EP-A2- 0 697 382</text></B561><B561><text>GB-A- 2 084 624</text></B561><B561><text>US-A- 3 042 578</text></B561><B561><text>US-A- 4 548 676</text></B561><B561><text>US-A- 4 548 676</text></B561><B561><text>US-A- 4 959 272</text></B561><B561><text>US-A- 5 911 818</text></B561><B561><text>US-A- 5 911 818</text></B561><B561><text>US-A- 5 964 934</text></B561><B565EP><date>20120606</date></B565EP></B560></B500><B700><B720><B721><snm>BAIG, Mirza, A.</snm><adr><str>479 Nuthatch</str><city>Lindenhurst, IL 60046</city><ctry>US</ctry></adr></B721></B720><B730><B731><snm>USG Interiors, LLC</snm><iid>101306132</iid><irf>P/60448.EP01</irf><adr><str>550 West Adams Street</str><city>Chicago, IL 60661-3676</city><ctry>US</ctry></adr></B731></B730><B740><B741><snm>Findlay, Alice Rosemary</snm><iid>101251662</iid><adr><str>Reddie &amp; Grose LLP 
The White Chapel Building 
10 Whitechapel High Street</str><city>London E1 8QS</city><ctry>GB</ctry></adr></B741></B740></B700><B800><B840><ctry>AT</ctry><ctry>BE</ctry><ctry>BG</ctry><ctry>CH</ctry><ctry>CY</ctry><ctry>CZ</ctry><ctry>DE</ctry><ctry>DK</ctry><ctry>EE</ctry><ctry>ES</ctry><ctry>FI</ctry><ctry>FR</ctry><ctry>GB</ctry><ctry>GR</ctry><ctry>HU</ctry><ctry>IE</ctry><ctry>IS</ctry><ctry>IT</ctry><ctry>LI</ctry><ctry>LT</ctry><ctry>LU</ctry><ctry>LV</ctry><ctry>MC</ctry><ctry>NL</ctry><ctry>PL</ctry><ctry>PT</ctry><ctry>RO</ctry><ctry>SE</ctry><ctry>SI</ctry><ctry>SK</ctry><ctry>TR</ctry></B840><B860><B861><dnum><anum>US2006029790</anum></dnum><date>20060801</date></B861><B862>en</B862></B860><B870><B871><dnum><pnum>WO2007024421</pnum></dnum><date>20070301</date><bnum>200709</bnum></B871></B870></B800></SDOBI>
<description id="desc" lang="en"><!-- EPO <DP n="1"> -->
<p id="p0001" num="0001">The invention relates to a composite board useful in constructing static structures and, in particular, walls, suspended ceilings, and the like.</p>
<heading id="h0001"><u>PRIOR ART</u></heading>
<p id="p0002" num="0002">Conventional wallboard, sometimes called drywall, is used extensively throughout the world, particularly in the construction of interior walls. The formulation of this product ordinarily includes a large proportion of gypsum that, consequently, is reflected in the weight of a board. Typically, conventional boards have a density of about 40 lbs. per cubic foot (pcf). Air may be entrained or trapped in the board composition to afford compressibility and to reduce weight. However, the gypsum content normally is maintained at a relatively high level so that adequate "nail pull" strength is assured. The weight of conventional wallboard is a significant disadvantage because it adds to shipping and handling costs in its distribution and labor costs including the effects of fatigue and/or strain, in its site delivery and installation.</p>
<p id="p0003" num="0003">Tile for suspended ceilings is produced with various formulations, calipers, face patterns, and coatings. A long standing and frequent problem with conventional ceiling tile is its tendency, after being installed, to sag, particularly in humid and/or high temperature environments resulting in an unsightly and, therefore, unsatisfactory condition. It has been noted that the inclusion of perlite in ceiling tile formulations can have a tendency to increase the susceptibility of tile to sag.</p>
<p id="p0004" num="0004"><patcit id="pcit0001" dnum="US3042578A"><text>US 3042578</text></patcit> discloses an insulating product comprising expanded perlite held together by a network of fiber.</p>
<p id="p0005" num="0005"><patcit id="pcit0002" dnum="EP0697382A"><text>EP 0697382</text></patcit> discloses an acoustical tile composition based on a gypsum/cellulosic fiber composition which can replace all or a portion of the mineral wool normally present in acoustical ceiling tiles. The gypsum/cellulosic fiber composition is combined with a lightweight aggregate material and a binder to form a composition which is used in a water-felting process to manufacture acoustical ceiling tiles and panels. The preferred source of the cellulosic fiber is a composite gypsum/cellulose fiber material which is prepared by mixing the gypsum and cellulosic fiber material with sufficient water to form a dilute slurry which is then heated under pressure to calcine the gypsum, converting it to an alpha calcium sulphate hemihydrate. The resulting composite material comprises cellulosic fibers physically interlocked with calcium sulphate crystals. Another source of both gypsum and cellulosic fibers is waste (scrap) gypsum wallboard. Expanded perlite is the preferred lightweight aggregate material.<!-- EPO <DP n="2"> --></p>
<heading id="h0002"><u>SUMMARY OF THE INVENTION</u></heading>
<p id="p0006" num="0006">The invention which is defined by the claims provides a relatively lightweight composite board useful, inter alia, for wall construction and suspended ceiling tile. The invention combines the use of expanded perlite as a lightweight medium in the core of the board and paper as a high tensile material in a cladding for the core to produce a board that is surprisingly both light and strong. The formulation of a suitable board core contains, by way of example, on a weight basis, approximately 15% to 40% perlite, approximately 10% to 30% cellulose fiber,<br/>
<!-- EPO <DP n="3"> -->a binding agent such as starch of approximately 5% to 15%, approximately 0% to 50% mineral wool and approximately 0% to 25% of filler such as gypsum. Paper stock is laminated to at least one side of this board core to work as a tensile structural element.</p>
<p id="p0007" num="0007">It has been found that the expanded perlite, in the disclosed composite board, works like a structural foam so that despite its low density, a relatively high compressive strength is obtained. The high compressive strength, more specifically, can apparently be attributed to the structural integrity of the core where the expanded perlite, cellulose fiber, and binder function together as a structural foam. This compressive strength is reflected in a surprisingly high nail pull capacity enabling the product to be successfully used as wallboard. The performance of the board, with a core formulated as disclosed and clad with a laminated paper runs contrary to ordinary experience where the density of wallboard has heretofore out of necessity been maintained at a relatively high level to achieve an adequate nail pull value.</p>
<p id="p0008" num="0008">The lightweight board construction of the invention allows the board to be successfully used for ceiling tile applications. A paper layer laminated at the face or room side of the tile, in addition to providing a uniform base for finish painting or the like, serves to significantly enhance the sag resistance of the tile in an economically, environmentally positive manner.</p>
<heading id="h0003"><u>DESCRIPTION OF THE PREFERRED EMBODIMENT</u></heading>
<p id="p0009" num="0009">A composite board embodying the invention includes a planar core and at least one paper facer sheet laminated to one side of the core. The board, when intended to be used as wallboard can typically be manufactured in nominal 4' x 8', 10', and 12' (10.16 × 20.32, 25.4 and 30.48 cm) dimensions. The board can, of course, be manufactured in other sizes or can be cut to other sizes at the factory or in the field. Since the board is lighter in weight than conventional wallboard, it can be manufactured in a greater width that is standard, for example, 5 foot and still be manually handled. The core is manufactured by conventional water felting processes typically used in ceiling tile manufacture, for example. The formulation of the core can vary considerably, but the basic or primary constituents are perlite, cellulose fiber, and binder. These constituents and<!-- EPO <DP n="4"> --> other optional constituents are uniformly mixed in a water slurry of about 5% solids, dewatered on a screen to form a mat, and then dried to form the core.</p>
<p id="p0010" num="0010">To the extent practical, the constituents remain uniformly distributed in the core as it is completed. It is preferable that the mat thickness be controlled by appropriate pressing techniques, known in the art, with sufficient exactness to produce a core of specified thickness preferably without supplemental grinding or sanding operations.</p>
<p id="p0011" num="0011">A discussion of the primary constituents and some optional constituents follows:</p>
<heading id="h0004"><b><u>Perlite</u></b></heading>
<p id="p0012" num="0012">Expanded perlite can be visualized as popped popcorn. After expansion to a particular density, the perlite particles have included voids or holes. After mixing with the constituent materials in a water slurry, the perlite particles contain water which must be subsequently removed during drying of the core mat. While a high perlite content can produce good bulking of the core, increases in perlite content may reduce board forming speed because of increased water content and can lessen noise reduction and sag resistance in ceiling tile applications.</p>
<heading id="h0005"><b><u>Cellulose Fiber</u></b></heading>
<p id="p0013" num="0013">Cellulose fiber provides wet strength during formation of the core. Cellulose fiber encapsulates the perlite and other fine particle size materials such as starch and fillers during the mat formation. Without cellulose fiber in the core formulation, the perlite would float to the surface of the slurry and formation of the core would become difficult. Excessive amounts of cellulose fiber in ceiling tile applications adversely affect the cut-ability of the tile with a hand-held board knife, commonly used by installers to cut tiles. An economical source of suitable cellulose fiber is recycled paper, but other sources of such fiber, such as wood, are practical.</p>
<heading id="h0006"><b><u>Binder</u></b></heading>
<p id="p0014" num="0014">Starch and latex are binders that provide a cohesive bond between the primary core ingredients after the core is dried. Normally, uncooked starch is used in a typical core formulation. The uncooked starch does not provide any<!-- EPO <DP n="5"> --> strength until it is cooked so that cellulose fiber is relied upon to provide green/wet strength before the core is dried. Once the starch is cooked, the core becomes crispy and can be cut easily with a hand-held board knife. Higher amounts of starch provide better crispiness. Increased organic content including starch and cellulose fiber has a negative impact on ceiling tile sag resistance under high humidity conditions.</p>
<heading id="h0007"><b><u>Mineral Wool</u></b></heading>
<p id="p0015" num="0015">Mineral wool in the core formulation of a board used for ceiling tile increases the sound absorption (NRC) of the board. In general, the higher the amount of mineral wool the better the sound absorption. Mineral wool also advantageously gives bulking to the slurry during formation of the core.</p>
<heading id="h0008"><b><u>Fillers</u></b></heading>
<p id="p0016" num="0016">Clay is important in fire-rated ceiling tile. During a fire, the clay can sinter and provide exceptional fire resistance to the ceiling tile. However, high clay content in the core formulation slows down the production line speed due to its affinity for water.</p>
<p id="p0017" num="0017">Calcium carbonate is a typical filler that has no significant value in the board properties except that it may give some hardness to the product but it can lower the cost of the product. Other commonly used low cost fillers are calcium sulfate and fly ash.</p>
<p id="p0018" num="0018">Gypsum, due to a limited solubility in water, acts as a flocculating vehicle. The function of flocculent in the core slurry is to retain and uniformly distribute the fine particles (inorganic clay, organic starch, etc.) in the mat during the processing (dewatering, vacuum and wet pressing). The lack of a flocculating vehicle in the formulation adversely affects the drainage because of migration of fine and high density particles to the bottom of the mat during the processing. Gypsum can produce a mat thickness higher than that produced by other inorganic fillers, clays and calcium carbonate. A higher mat thickness (loft) prior to wet pressing is beneficial in removing excess water. Gypsum can avoid the need for another flocculent, a coagulant and/or a surfactant. Gypsum can improve the hardness in the board. Gypsum can act as a dispersant to de-agglomerate mineral fiber and/or cellulose fiber and thereby permit higher slurry consistency (solids %) to increase the production<!-- EPO <DP n="6"> --> rate. Gypsum does not significantly "spring-back" or swell after pressing and drying of the core mat so that the need to sand the core to control core thickness is reduced.</p>
<p id="p0019" num="0019">From the foregoing discussion of the primary and potential constituent materials it will be seen that the selection of materials and their proportions can depend on the intended use of the composite board and its requisite physical properties.</p>
<p id="p0020" num="0020">Of the main components, perlite, cellulose fiber and binder, perlite occupies the majority of the volume of the core. The density of the perlite is about 3 to about 15 pounds per cubic foot (48·056 to 240·278 kg/m<sup>3</sup>) and, more preferably, between about 6 and about 10 pounds per cubic foot (96·111 to 160·185 kg/m<sup>3</sup>) and, most preferably, about 8 pounds per cubic foot (128·148 kg/m<sup>3</sup>). Regardless of the actual density of the expanded perlite that is used in constructing the core, it is important on a bulk basis, the perlite occupies a majority of the volume of the core and, preferably, occupies substantially all of the volume of the core. One way of assuring that the core is adequate in its perlite content, is to slightly overcharge the mix in the slurry with perlite so that when the mat forming the core is pressed to a specified size, a limited amount of the perlite expanded particles, e.g. about 5% is crushed.</p>
<p id="p0021" num="0021">A paper facer is laminated to at least one side of the core. The paper facer can be any one of a variety of forms, such as kraft paper, depending on the ultimate use of the composite board. Where the composite board is intended to be used as wallboard, regular wallboard paper (i.e. paper on the face or rear of drywall) can be laminated to the core. An example of such paper has a thickness of between about 11 mills and about 13 mills (225·94 and 267·02µm) Such paper commonly will exhibit a tensile strength of about 140 pounds (63·504 kg) in the machine direction and 45 pounds (20·412 kg) in the cross direction when a sample size of 2 inches (5·18 cm) wide is clamped and pulled in a standard test fixture (TAPPI test standard). Also, where the composite board is intended to be used for wallboard, its overall caliper or thickness will be, for example, nominally 3/8", 1/2", or 5/8"(9·525, 12·7, 12·7 or 15·875 cm). The core is sized in thickness to make up this nominal thickness when combined with either a paper facer on only one side or a separate paper<!-- EPO <DP n="7"> --> facer on each opposite side of the core. Typically, the paper facer or facers are laminated to the core simultaneously on the production line as the core is being made after being cut to size or before. The paper facer or facers are adhered to the core by a suitable commercially available water-based adhesive, preferably a latex. The adhesive may be sprayed, roll-coated or otherwise distributed across the full surface of one or both the core and paper facer by conventional known techniques. As the mat is dried and the core completed in factory production, it typically has a very low moisture content of about 2% or less. This low moisture content enables the water based adhesive to cure quickly when the paper facer or facers is/are laminated to the core in factory production of the composite board.</p>
<p id="p0022" num="0022">Ideally, the resultant composite board should have a density of about 30 pounds per cubic foot. This density or weight can afford significant benefits over standard wallboard weights. Savings in shipping, handling, and installation costs are potentially immense. The invention, by employing a lightweight core, departs from the conventional practice of maintaining at least a minimum density of about 40 pounds per cubic foot (640·74 kg/m<sup>3</sup>) for gypsum-based wallboard. In current practice, when the density of conventional wallboard is reduced below this value, the strength of the wallboard suffers and typically nail-pull performance becomes unacceptable. Nail-pull is detailed in ASTM Standard C473 and is used by the industry to measure the performance of wallboard or panel construction with industry standards.</p>
<p id="p0023" num="0023">The invention involves the use of expanded perlite cells or particles in a homogeneous mix of cellulose (paper) fiber and binder. A practical form of binder is starch derived from, for example, corn, potato and/or wheat stock. The starch may be precooked before it is introduced into the slurry from which the mat of the core is formed. The cellulose fiber and binder form a matrix in the interstices between the perlite particles. The binder immobilizes the cellulose fibers relative to one another and the fibers relative to the perlite particles. The cellulose fibers contribute a major portion of the tensile strength of the core. Preferably, the combined weight of the perlite and cellulose fiber is at least 25% of the total weight of the core.<!-- EPO <DP n="8"> --></p>
<p id="p0024" num="0024">Composite boards made by the disclosed process and disclosed formulation exhibit a surprisingly high nail-pull performance, particularly when compared against standard gypsum-based wallboard and lightweight gypsum-based wallboard. As best understood, and depending in part on the actual formulation, it is theorized that the perlite component of the core mixture, combined with the stabilizing function of the paper fiber and binder enables the perlite grains to act collectively as a structural foam, yielding a high strength in compression while being relatively light in weight. The strength of the core, not only in compression, but also in tension, offers the unique ability of the composite board to be clad with only one paper facing and still provide high levels of nail-pull performance. That is to say, a second paper facer need not necessarily be used to obtain adequate nail pull strength where the face of the panel against which the head of a nail or screw is driven is the sole paper clad side.</p>
<p id="p0025" num="0025">In addition to the basic constituents of the core, as mentioned, other materials may be used in the core formulation. These additional materials can include mineral wool, gypsum and filler such as clay, fly ash, and dolomite. Below is a table showing potential components of a core mixture and potential relative percentages on the basis of weight. The core of the composite board has a formulation within the following parameters:
<tables id="tabl0001" num="0001">
<table frame="all">
<tgroup cols="4">
<colspec colnum="1" colname="col1" colwidth="26mm"/>
<colspec colnum="2" colname="col2" colwidth="19mm"/>
<colspec colnum="3" colname="col3" colwidth="20mm"/>
<colspec colnum="4" colname="col4" colwidth="38mm"/>
<thead>
<row>
<entry valign="top"/>
<entry align="center" valign="top">Minimum</entry>
<entry align="center" valign="top">Maximum</entry>
<entry align="center" valign="top">Exemplar Formulation 1</entry></row></thead>
<tbody>
<row>
<entry>Perlite</entry>
<entry align="center">15</entry>
<entry align="center">50</entry>
<entry align="center">30</entry></row>
<row>
<entry>Cellulose Fiber</entry>
<entry align="center">10</entry>
<entry align="center">30</entry>
<entry align="center">19</entry></row>
<row>
<entry>Binder</entry>
<entry align="center">5</entry>
<entry align="center">15</entry>
<entry align="center">12</entry></row>
<row>
<entry>Mineral Wool</entry>
<entry align="center">0</entry>
<entry align="center">50</entry>
<entry align="center">35</entry></row>
<row>
<entry>Filler</entry>
<entry align="center">0</entry>
<entry align="center">20</entry>
<entry align="center">4</entry></row>
<row>
<entry namest="col1" nameend="col2" colsep="0" align="left">TOTAL</entry>
<entry colsep="0" align="center">100</entry>
<entry align="center"/></row></tbody></tgroup>
</table>
</tables></p>
<p id="p0026" num="0026">Composite boards having either one or two faces laminated with a standard wallboard paper and having the exemplar core formula set out in the foregoing table exhibited the following performance:<!-- EPO <DP n="9"> -->
<tables id="tabl0002" num="0002">
<table frame="all">
<tgroup cols="7">
<colspec colnum="1" colname="col1" colwidth="19mm"/>
<colspec colnum="2" colname="col2" colwidth="28mm"/>
<colspec colnum="3" colname="col3" colwidth="25mm"/>
<colspec colnum="4" colname="col4" colwidth="22mm"/>
<colspec colnum="5" colname="col5" colwidth="28mm" colsep="0"/>
<colspec colnum="6" colname="col6" colwidth="18mm"/>
<colspec colnum="7" colname="col7" colwidth="28mm"/>
<thead>
<row>
<entry namest="col1" nameend="col7" align="left" valign="top"><b>Paper 1-side, 3/8" caliper core</b></entry></row>
<row>
<entry valign="top"><b>Sample #</b></entry>
<entry valign="top"><b>Paper Direction</b></entry>
<entry valign="top"><b>Thickness in</b></entry>
<entry valign="top"><b>Density pcf</b></entry>
<entry valign="top"><b>Break Load, LB</b></entry>
<entry valign="top"><b>MOR psi</b></entry>
<entry valign="top"><b>Weight LB /MSF</b></entry></row></thead>
<tbody>
<row>
<entry>Avg.</entry>
<entry>FU, MD</entry>
<entry>0.403</entry>
<entry>30.8</entry>
<entry>13.63</entry>
<entry>336</entry>
<entry>1034</entry></row>
<row>
<entry>Avg.</entry>
<entry>FD, MD</entry>
<entry>0.404</entry>
<entry>31.0</entry>
<entry>28.52</entry>
<entry>700</entry>
<entry>1042</entry></row>
<row>
<entry>Avg.</entry>
<entry>FU, CD</entry>
<entry>0.404</entry>
<entry>30.6</entry>
<entry>13.82</entry>
<entry>340</entry>
<entry>1030</entry></row>
<row>
<entry>Avg.</entry>
<entry>FD, CD</entry>
<entry>0.404</entry>
<entry>30.3</entry>
<entry>17.18</entry>
<entry>420</entry>
<entry>1021</entry></row>
<row>
<entry/>
<entry/>
<entry/>
<entry/>
<entry/>
<entry/>
<entry/></row></tbody></tgroup>
<tgroup cols="7">
<colspec colnum="1" colname="col1" colwidth="19mm"/>
<colspec colnum="2" colname="col2" colwidth="28mm"/>
<colspec colnum="3" colname="col3" colwidth="25mm"/>
<colspec colnum="4" colname="col4" colwidth="22mm"/>
<colspec colnum="5" colname="col5" colwidth="28mm"/>
<colspec colnum="6" colname="col6" colwidth="18mm"/>
<colspec colnum="7" colname="col7" colwidth="28mm"/>
<thead>
<row>
<entry namest="col1" nameend="col7" align="left" valign="top"><b>Paper 2-Side, 3/8" caliper core</b></entry></row></thead>
<tbody>
<row>
<entry>Avg.</entry>
<entry>FU, MD</entry>
<entry>0.414</entry>
<entry>31.8</entry>
<entry colsep="0">33.34</entry>
<entry>781</entry>
<entry>1097</entry></row>
<row>
<entry>Avg.</entry>
<entry>FD, MD</entry>
<entry>0.416</entry>
<entry>31.8</entry>
<entry colsep="0">34.56</entry>
<entry>799</entry>
<entry>1102</entry></row>
<row>
<entry>Avg.</entry>
<entry>FU, CD</entry>
<entry>0.421</entry>
<entry>31.7</entry>
<entry colsep="0">20.90</entry>
<entry>473</entry>
<entry>1112</entry></row>
<row>
<entry>Avg.</entry>
<entry>FD, CD</entry>
<entry>0.420</entry>
<entry>31.8</entry>
<entry colsep="0">20.82</entry>
<entry>473</entry>
<entry>1111</entry></row></tbody></tgroup>
<tgroup cols="7">
<colspec colnum="1" colname="col1" colwidth="19mm"/>
<colspec colnum="2" colname="col2" colwidth="28mm"/>
<colspec colnum="3" colname="col3" colwidth="25mm"/>
<colspec colnum="4" colname="col4" colwidth="22mm"/>
<colspec colnum="5" colname="col5" colwidth="28mm" colsep="0"/>
<colspec colnum="6" colname="col6" colwidth="18mm"/>
<colspec colnum="7" colname="col7" colwidth="28mm"/>
<thead>
<row>
<entry namest="col1" nameend="col7" align="left" valign="top"><b>Paper 1-side, ½" caliper core</b></entry></row></thead>
<tbody>
<row>
<entry>Avg.</entry>
<entry>FU, MD</entry>
<entry>0.520</entry>
<entry>29.8</entry>
<entry>29.57</entry>
<entry>437</entry>
<entry>1293</entry></row>
<row>
<entry>Avg.</entry>
<entry>FD, MD</entry>
<entry>0.523</entry>
<entry>29.8</entry>
<entry>49.84</entry>
<entry>730</entry>
<entry>2397</entry></row>
<row>
<entry>Avg.</entry>
<entry>FU, CD</entry>
<entry>0.518</entry>
<entry>30.3</entry>
<entry>24.45</entry>
<entry>364</entry>
<entry>1310</entry></row>
<row>
<entry>Avg.</entry>
<entry>FD, CD</entry>
<entry>0.520</entry>
<entry>30.2</entry>
<entry>31.48</entry>
<entry>466</entry>
<entry>1307</entry></row></tbody></tgroup><!-- EPO <DP n="10"> -->
<tgroup cols="7">
<colspec colnum="1" colname="col1" colwidth="19mm"/>
<colspec colnum="2" colname="col2" colwidth="28mm"/>
<colspec colnum="3" colname="col3" colwidth="25mm"/>
<colspec colnum="4" colname="col4" colwidth="22mm"/>
<colspec colnum="5" colname="col5" colwidth="28mm" colsep="0"/>
<colspec colnum="6" colname="col6" colwidth="18mm"/>
<colspec colnum="7" colname="col7" colwidth="28mm"/>
<thead>
<row>
<entry namest="col1" nameend="col7" align="left" valign="top"><b>Paper 2-Side, ½" caliper core</b></entry></row></thead>
<tbody>
<row>
<entry>Avg.</entry>
<entry>FU, MD</entry>
<entry>0.534</entry>
<entry>30.3</entry>
<entry>55.80</entry>
<entry>784</entry>
<entry>1347</entry></row>
<row>
<entry>Avg.</entry>
<entry>FD, MD</entry>
<entry>0.538</entry>
<entry>30.3</entry>
<entry>57.53</entry>
<entry>795</entry>
<entry>1361</entry></row>
<row>
<entry>Avg.</entry>
<entry>FU, CD</entry>
<entry>0.538</entry>
<entry>30.3</entry>
<entry>36.08</entry>
<entry>500</entry>
<entry>1357</entry></row>
<row>
<entry>Avg.</entry>
<entry>FD, CD</entry>
<entry>0.535</entry>
<entry>30.7</entry>
<entry>35.02</entry>
<entry>489</entry>
<entry>1368</entry></row></tbody></tgroup>
<tgroup cols="7" rowsep="0">
<colspec colnum="1" colname="col1" colwidth="19mm"/>
<colspec colnum="2" colname="col2" colwidth="28mm"/>
<colspec colnum="3" colname="col3" colwidth="25mm"/>
<colspec colnum="4" colname="col4" colwidth="22mm"/>
<colspec colnum="5" colname="col5" colwidth="28mm"/>
<colspec colnum="6" colname="col6" colwidth="18mm"/>
<colspec colnum="7" colname="col7" colwidth="28mm"/>
<tbody>
<row>
<entry namest="col1" nameend="col7" align="justify">inch = 25.4 mm<br/>
LB = 0.4536 kg<br/>
psi = 6.8947 kN/m<sup>2</sup><br/>
pcf = 16.0185 kg/m<sup>3</sup><br/>
LB MSF = 0.2046 g/m<sup>2</sup><br/>
During the testing: FU = Face Up, FD = Face Down<br/>
MD = sample tested paper in Machine Direction<br/>
CD = sample tested paper in Machine Cross Direction</entry></row></tbody></tgroup>
</table>
</tables>
\</p>
<p id="p0027" num="0027">MOR (modulus of rupture) is a measure of bending strength given by the following equation (ASTM D1037): <maths id="math0001" num=""><math display="block"><mi>MOR</mi><mo>=</mo><mfrac><mrow><mn>3</mn><mo>×</mo><mi>Load</mi><mfenced><mi>LB</mi></mfenced><mo>×</mo><mi>Span</mi><mfenced><mi>inches</mi></mfenced></mrow><mrow><mn>2</mn><mo>×</mo><mi>Sample width</mi><mfenced><mi>inches</mi></mfenced><mo>×</mo><msup><mi>Thickness</mi><mn>2</mn></msup><mfenced><msup><mi>inches</mi><mn>2</mn></msup></mfenced></mrow></mfrac></math><img id="ib0001" file="imgb0001.tif" wi="107" he="13" img-content="math" img-format="tif"/></maths></p>
<p id="p0028" num="0028">Based on the foregoing, one skilled in the art may formulate a 6,000 lb. solids water slurry batch to obtain the estimated results:
<tables id="tabl0003" num="0003">
<table frame="all">
<tgroup cols="9">
<colspec colnum="1" colname="col1" colwidth="23mm"/>
<colspec colnum="2" colname="col2" colwidth="13mm" colsep="0"/>
<colspec colnum="3" colname="col3" colwidth="15mm"/>
<colspec colnum="4" colname="col4" colwidth="13mm" colsep="0"/>
<colspec colnum="5" colname="col5" colwidth="15mm"/>
<colspec colnum="6" colname="col6" colwidth="13mm" colsep="0"/>
<colspec colnum="7" colname="col7" colwidth="15mm"/>
<colspec colnum="8" colname="col8" colwidth="13mm" colsep="0"/>
<colspec colnum="9" colname="col9" colwidth="15mm"/>
<thead>
<row>
<entry valign="top"/>
<entry namest="col2" nameend="col9" align="left" valign="top">Formulations with different amounts of perlite and weight - <b>1/2" Board</b></entry></row>
<row>
<entry valign="top"/>
<entry namest="col2" nameend="col3" align="center" valign="top">2</entry>
<entry namest="col4" nameend="col5" align="center" valign="top">3</entry>
<entry namest="col6" nameend="col7" align="center" valign="top">4</entry>
<entry namest="col8" nameend="col9" align="center" valign="top">5</entry></row>
<row>
<entry valign="top"/>
<entry align="center" valign="top">%</entry>
<entry align="center" valign="top">wt., LB</entry>
<entry align="center" valign="top">%</entry>
<entry align="center" valign="top">wt., LB</entry>
<entry align="center" valign="top">%</entry>
<entry align="center" valign="top">wt., LB</entry>
<entry align="center" valign="top">%</entry>
<entry align="center" valign="top">wt., LB</entry></row></thead>
<tbody>
<row rowsep="0">
<entry>Wool %</entry>
<entry align="center">0</entry>
<entry align="center">0</entry>
<entry align="center">20</entry>
<entry align="center">1200</entry>
<entry align="center">5</entry>
<entry align="center">300</entry>
<entry align="center">23</entry>
<entry align="center">1380</entry></row>
<row rowsep="0">
<entry>Perlite %</entry>
<entry align="center">35</entry>
<entry align="center">2100</entry>
<entry align="center">15</entry>
<entry align="center">900</entry>
<entry align="center">50</entry>
<entry align="center">3000</entry>
<entry align="center">40</entry>
<entry align="center">2400</entry></row>
<row rowsep="0">
<entry>Fiber %</entry>
<entry align="center">30</entry>
<entry align="center">1800</entry>
<entry align="center">30</entry>
<entry align="center">1800</entry>
<entry align="center">20</entry>
<entry align="center">1200</entry>
<entry align="center">25</entry>
<entry align="center">1500</entry></row>
<row rowsep="0">
<entry>Starch %</entry>
<entry align="center">15</entry>
<entry align="center">900</entry>
<entry align="center">10</entry>
<entry align="center">600</entry>
<entry align="center">11</entry>
<entry align="center">600</entry>
<entry align="center">12</entry>
<entry align="center">720</entry></row>
<row>
<entry>Filler %</entry>
<entry align="center">20</entry>
<entry align="center">1200</entry>
<entry align="center">25</entry>
<entry align="center">1500</entry>
<entry align="center">14</entry>
<entry align="center">840</entry>
<entry align="center">0</entry>
<entry align="center">0</entry></row>
<row>
<entry>TOTAL</entry>
<entry align="center">100</entry>
<entry align="center">6000</entry>
<entry align="center">100</entry>
<entry align="center">6000</entry>
<entry align="center">100</entry>
<entry align="center">6000</entry>
<entry align="center">100</entry>
<entry align="center">6000</entry></row>
<row>
<entry colsep="0"><b>Nail-Pull LB</b></entry>
<entry namest="col2" nameend="col3" colsep="0" align="center"><b>Estimated 110</b></entry>
<entry namest="col4" nameend="col5" colsep="0" align="center"><b>Estimated 100</b></entry>
<entry namest="col6" nameend="col7" colsep="0" align="center"><b>Estimated 95</b></entry>
<entry namest="col8" nameend="col9" align="center"><b>Estimated 110</b></entry></row></tbody></tgroup>
</table>
</tables></p>
<p id="p0029" num="0029">As a general rule, the higher the amount of cellulose fiber, the lower the density of the board will be. As previously indicated, the low density boards of the invention can readily exceed industry nail pull standards for equivalent board thicknesses.<!-- EPO <DP n="11"> --></p>
<p id="p0030" num="0030">Industry standards establish accepted nail pull values of 5 lb. (25.402 kg) for 3/8" (9.525 mm) wallboard and 77 lb. (34.927 kg) for 1/2" (12.7 mm) wallboard. The foregoing table shows that the lightweight core of the exemplar formulation combined with standard drywall paper laminated on one or both sides can exceed these industry standards. It is evident from this data that the density of the core and/or the strength of the paper facer or facers can be reduced from the recorded lightweight construction while still achieving satisfactory nail pull performance was of at least the industry standards.</p>
<p id="p0031" num="0031">It should be evident that this disclosure is by way of example and that various changes may be made by adding, modifying or eliminating details.</p>
</description>
<claims id="claims01" lang="en"><!-- EPO <DP n="12"> -->
<claim id="c-en-01-0001" num="0001">
<claim-text>A composite board comprising a core and a paper facer sheet adhesively laminated to one face of the core, the core including a mixture of perlite, binder, and cellulose fiber, the core being formed as a water slurry with said perlite, binder and cellulose fiber being uniformly distributed therein, the perlite being in an expanded state such that its particles include internal voids and exhibit a density of 5 to 15 pounds per cubic foot (80.093 to 240.278 kg/m<sup>3</sup>) and being present in sufficient quantity to occupy in bulk at least 50% of the volume of the core, on a weight basis, the perlite and cellulose fiber combined forming at least 25% of the weight of the core, the cellulose fiber and binder forming a matrix in the interstices between the perlite particles, the binder immobilizing the cellulose fibers relative to one another and the fibers relative to the perlite particles, the cellulose fibers contributing a major portion of the tensile strength of the core, the paper facer being laminated to the core with a water-based adhesive applied across substantially the full area of the facer, both the compressive strength of the perlite and tensile strength of the cellulose fiber being utilized by operation of the binder such that a relatively high nail-pull capacity as detailed in ASTM Standard C473 in comparison to the weight of the composite board is achieved.</claim-text></claim>
<claim id="c-en-01-0002" num="0002">
<claim-text>A composite panel as set forth in claim 1, wherein the original bulk volume of the perlite is at least as great as the volume of the core.</claim-text></claim>
<claim id="c-en-01-0003" num="0003">
<claim-text>A composite board as set forth in claim 1 , wherein the perlite, cellulose fiber, and binder combined, comprise at least 30% of the weight of the core.</claim-text></claim>
<claim id="c-en-01-0004" num="0004">
<claim-text>A composite board as set forth in claim 1, wherein the paper facer is laminated to the core as the core is being finished at the factory.</claim-text></claim>
<claim id="c-en-01-0005" num="0005">
<claim-text>A composite board comprising as components, a core and paper facer sheet material adhesively laminated to at least one face of the core, the core including a substantially uniform mixture of perlite, binder and cellulose fiber, the core being formed as a water slurry, the perlite being in an expanded state such that its particles include internal voids and exhibit a density of 3 to 15 pounds per cubic foot (80.093 to 240.278 kg/m<sup>3</sup>), the perlite comprising between 15% to 40% of the weight of the core, the cellulose fiber comprising between 10% to 30% of the weight of the core, the binder comprising between 5% to 15% of the weight of the core, the cellulose fiber and binder forming a matrix in the interstices between the perlite particles, the binder adhering the cellulose fibers to one another and adhering the cellulose fibers to the perlite particles, the paper facer material being laminated to the core with a water based adhesive applied across substantially the full area of the facer material, the<!-- EPO <DP n="13"> --> formulation of the perlite, cellulose fiber, binder and other constituents of the core and paper facer material being selected to produce a composite board density of 30 pounds per cubic foot (480.555 kg/m<sup>3</sup>) or less and a nail pull as detailed in ASTM Standard C473 of at least 56 pounds (25.402 kg) when the composite board caliper is nominally 3/8" (9.525 mm) and at least 77 pounds (34.927 kg) when the composite board caliper is nominally 1/2" (12.7 mm).</claim-text></claim>
<claim id="c-en-01-0006" num="0006">
<claim-text>A composite board as set forth in claim 5, wherein said paper facer sheet material is laminated on opposite sides of said core.</claim-text></claim>
</claims>
<claims id="claims02" lang="de"><!-- EPO <DP n="14"> -->
<claim id="c-de-01-0001" num="0001">
<claim-text>Verbundplatte, umfassend einen Kern und einen Papierdeckschichtbogen, der adhäsiv auf der einen Seite des Kerns laminiert ist, wobei der Kern eine Mischung aus Perlit, Bindemittel und Cellulosefaser enthält, wobei der Kern als eine wässrige Aufschlämmung mit dem Perlit, Bindemittel und Cellulosefaser gebildet wird, die darin gleichförmig verteilt sind, wobei der Perlit in einem geschäumten Zustand vorliegt, so dass seine Partikel innere Hohlräume einschliessen, und eine Dichte von 5 bis 15 Pfund pro Kubikfuß (80,093 bis 240,278 kg/m<sup>3</sup>) zeigt und in einer ausreichenden Menge vorhanden ist, um im losen Zustand bezogen auf das Gewicht mindestens 50% des Volumens des Kerns einzunehmen, wobei der Perlit und die Cellulosefaser zusammen mindestens 25% des Gewichts des Kerns bilden, wobei die Cellulosefaser und das Bindemittel in den Zwischenräumen zwischen den Perlitpartikeln eine Matrix bilden, wobei das Bindemittel die Cellulosefasern relativ zueinander und die Fasern relativ zu den Perlitpartikeln immobilisiert sind, wobei die Cellulosefasern einen Hauptteil der Zugfestigkeit des Kerns beitragen, wobei die Papierdeckschicht auf den Kern mit einem Klebemittel auf Wasserbasis laminiert wird, das im Wesentlichen über die gesamte Fläche der Deckschicht aufgebracht wird, wobei sowohl die Druckfestigkeit des Perlits als auch die Zugfestigkeit der Cellulosefaser durch die Funktion des Bindemittels derart genutzt werden, dass im Vergleich zu dem Gewicht der Verbundplatte eine relativ hohe Nagelziehfestigkeit erreicht wird, wie sie im ASTM-Standard C 473 detailliert ist.</claim-text></claim>
<claim id="c-de-01-0002" num="0002">
<claim-text>Verbundplatte nach Anspruch 1, wobei das ursprüngliche Schüttvolumen des Perlits mindestens so groß ist wie das Volumen des Kerns.</claim-text></claim>
<claim id="c-de-01-0003" num="0003">
<claim-text>Verbundplatte nach Anspruch 1, wobei der Perlit, die Cellulosefaser und das Bindemittel kombiniert mindestens etwa 30% des Gewichts des Kerns ausmachen.</claim-text></claim>
<claim id="c-de-01-0004" num="0004">
<claim-text>Verbundplatte nach Anspruch 1, wobei die Papierdeckschicht auf den Kern laminiert wird, wenn der Kern in der Fabrik ausgerüstet wird.</claim-text></claim>
<claim id="c-de-01-0005" num="0005">
<claim-text>Verbundplatte, als Komponenten umfassend ein Kern- und Papierdeckschichtmaterial, das adhäsiv auf mindestens eine Seite des Kerns laminiert ist, wobei der Kern eine im Wesentlichen gleichförmige Mischung aus Perlit, Bindemittel und Zellulosefaser enthält, wobei der Kern als eine wässrige Aufschlämmung gebildet wird, wobei der Perlit in einem geschäumten Zustand vorliegt, so dass seine Partikel innere Hohlräume einschliessen, und eine Dichte von 5 bis 15 Pfund pro Kubikfuß (80,093 bis 240,278 kg/m<sup>3</sup>) zeigt, wobei der Perlit zwischen etwa 15% bis etwa 40% des Kerngewichts umfasst, wobei die Cellulosefaser zwischen etwa 10% bis etwa 30% des Gewichts des Kerns umfasst, wobei das Bindemittel zwischen etwa 5% bis etwa 15% des Gewichts des Kerns umfasst, wobei die Cellulosefaser und das Bindemittel eine Matrix in den Zwischenräumen zwischen den Perlitpartikeln bilden, wobei das Bindemittel, das die Zellulosefasern miteinander verklebt und die Zellulosefasern mit den Perlitpartikeln verklebt, wobei das Papierdeckschichtmaterial auf den Kern mit einem Klebemittel auf<!-- EPO <DP n="15"> --> Wasserbasis laminiert wird, das im Wesentlichen über die gesamte Fläche des Deckschichtmaterials aufgebracht wird, wobei die Formulierung des Perlits, der Zellulosefaser, des Bindemittels und anderer Bestandteile des Kern- und Papierdeckschichtmaterials so ausgewählt werden, dass eine Dichte der Verbundplatte von 30 Pfund pro Kubikfuß (480,555 kg/m<sup>3</sup>) oder weniger und eine Nagelziehfestigkeit erzeugt wird, wie sie im ASTM-Standard C 473 detailliert ist, bei mindestens 56 Pfund (25,402 kg), wenn die Dicke der Verbundplatte nominell 3/8" (9,525 mm) beträgt und mindestens etwa 77 Pfund (34,927 kg), wenn die Dicke der Verbundplatte nominal 1/2" (12,7 mm) beträgt.</claim-text></claim>
<claim id="c-de-01-0006" num="0006">
<claim-text>Verbundplatte nach Anspruch 5, wobei das Papierdeckschichtmaterial auf gegenüberliegenden Seiten des Kerns laminiert ist.</claim-text></claim>
</claims>
<claims id="claims03" lang="fr"><!-- EPO <DP n="16"> -->
<claim id="c-fr-01-0001" num="0001">
<claim-text>Plaque composite comprenant un coeur et une feuille de face de papier laminée de façon adhésive sur une face du coeur, le coeur incluant un mélange de perlite, de liant et de fibre de cellulose, le coeur étant formé comme une suspension épaisse aqueuse avec lesdits perlite, liant et fibre de cellulose qui sont uniformément distribués dans celle-ci, la perlite étant dans un état expansé de sorte que ses particules incluent des vides internes et affichent une densité de 5 à 15 livres par pied cube (80,093 à 240,278 kg/m<sup>3</sup>) et étant présente dans une quantité suffisante pour occuper en vrac au moins 50% du volume du coeur, sur une base de poids, la perlite et la fibre de cellulose combinées formant au moins 25% du poids du coeur, la fibre de cellulose et le liant formant une matrice dans les interstices entre les particules de perlite, le liant immobilisant les fibres de cellulose les unes par rapport aux autres et les fibres par rapport aux particules de perlite, les fibres de cellulose contribuant à une portion majeure de la résistance à la traction du coeur, le revêtement de papier étant laminé sur le coeur avec un adhésif à base d'eau appliqué substantiellement sur toute la surface du revêtement, à la fois la résistance à la compression de la perlite et la résistance à traction de la fibre de cellulose étant utilisées par l'opération du liant de sorte qu'une capacité d'arrachage de clou relativement élevée telle que détaillée dans la norme ASTM C473 en comparaison au poids de la plaque composite est atteinte.</claim-text></claim>
<claim id="c-fr-01-0002" num="0002">
<claim-text>Panneau composite selon la revendication 1, dans lequel le volume en vrac d'origine de la perlite est au moins aussi grand que le volume du coeur.</claim-text></claim>
<claim id="c-fr-01-0003" num="0003">
<claim-text>Plaque composite selon la revendication 1, dans laquelle la perlite, la fibre de cellulose et le liant combinés comprennent au moins 30% du poids du coeur.</claim-text></claim>
<claim id="c-fr-01-0004" num="0004">
<claim-text>Plaque composite selon la revendication 1, dans laquelle le revêtement de papier est laminé sur le coeur lorsque le coeur est en finition à l'usine.</claim-text></claim>
<claim id="c-fr-01-0005" num="0005">
<claim-text>Plaque composite comprenant comme composants, un coeur et un matériau de revêtement de papier laminé de façon adhésive sur au moins une face du coeur, le coeur incluant un mélange substantiellement uniforme de perlite, de liant et de fibre de cellulose, le coeur étant formé comme une suspension épaisse aqueuse, la perlite étant dans un état expansé de sorte que ses particules incluent des vides internes et affichent une densité de 3 à 15 livres par pied cube (80,093 à 240,278 kg/m<sup>3</sup>), la perlite comprenant entre 15% et 40% du poids du coeur, la fibre de cellulose comprenant entre 10% et 30% du poids du coeur, le liant comprenant entre 5% et 15% du poids du coeur, la fibre de cellulose et le liant formant une matrice dans les interstices entre les particules de perlite, le liant adhérant les fibres de cellulose les unes aux autres et adhérant les fibres de cellulose aux particules de perlite, le matériau de feuille de face de papier étant laminé sur le coeur avec un adhésif à base d'eau appliqué substantiellement sur toute la surface du matériau de feuille de face, la formulation de la perlite, de la fibre de cellulose, du liant et d'autres constituants du coeur et du matériau de feuille de face de papier étant choisie pour<!-- EPO <DP n="17"> --> produire une densité de plaque composite de 30 livres par pied cube (480,555 kg/m<sup>3</sup>) ou moins et un arrachage de clou tel que détaillé dans la norme ASTM C473 d'au moins 56 livres (25,402 kg) lorsque l'épaisseur de la plaque composite est nominalement de 3/8" (9,525 mm) et d'au moins 77 livres (34,927 kg) lorsque l'épaisseur de la plaque composite est nominalement de 1/2" (12,7 mm).</claim-text></claim>
<claim id="c-fr-01-0006" num="0006">
<claim-text>Plaque composite selon la revendication 5, dans laquelle ledit matériau de revêtement de papier est laminé sur les côtés opposés dudit coeur.</claim-text></claim>
</claims>
<ep-reference-list id="ref-list">
<heading id="ref-h0001"><b>REFERENCES CITED IN THE DESCRIPTION</b></heading>
<p id="ref-p0001" num=""><i>This list of references cited by the applicant is for the reader's convenience only. It does not form part of the European patent document. Even though great care has been taken in compiling the references, errors or omissions cannot be excluded and the EPO disclaims all liability in this regard.</i></p>
<heading id="ref-h0002"><b>Patent documents cited in the description</b></heading>
<p id="ref-p0002" num="">
<ul id="ref-ul0001" list-style="bullet">
<li><patcit id="ref-pcit0001" dnum="US3042578A"><document-id><country>US</country><doc-number>3042578</doc-number><kind>A</kind></document-id></patcit><crossref idref="pcit0001">[0004]</crossref></li>
<li><patcit id="ref-pcit0002" dnum="EP0697382A"><document-id><country>EP</country><doc-number>0697382</doc-number><kind>A</kind></document-id></patcit><crossref idref="pcit0002">[0005]</crossref></li>
</ul></p>
</ep-reference-list>
</ep-patent-document>
