Filed of the Invention
[0001] The present invention relates to beverages, more precisely to shelf-stable liquid
base compositions useful for the preparation of acidified milk based beverages, especially
by means of beverage dispensing machines.
Background of the Invention
[0002] Acidified milk beverages are very popular today as they offer simultaneously sweetness
and freshness to consumers. These beverages further provide well known milk nutrients
like proteins or minerals and, when acidity is achieved by means of fruits juices,
the latter further bring flavours or vitamins in addition to the mere acidifying effect.
[0003] Most of the acidified milk based beverages are available today as "ready-to-drink"
beverages, which require storage at refrigerated conditions and, consequently, which
have a limited shelf life. Several attempts have been made in the past to increase
stability and storage period of said "ready-to-drink" beverages, e.g. by controlling
pH with suitable stabilizers, increasing sugar content or removal of undesired components
like certain milk or juice electrolytes (see e.g.
US 4,676,988).
[0004] US patent 3,800,052 discloses the preparation of a sour, "ready-to-drink" milk beverage having a good
whiteness and stability made by adding acid to skim milk to bring the pH of the beverage
within the range of 3.5 to 3.7. Acid is added to skim milk and water in predetermined
proportions, then sugar and the whole is subject to moderate heating (around 70° C),
refined and flavoured if necessary and eventually bottled as is for storage or for
direct consumption.
[0005] US patent 4,194,019 describes a method for preparing an acidified milk beverage which has milk protein
stably dispersed therein and which is "ready-to-drink" without dilution, when subjecting
an acidified skimmed milk having a milk solid-not-fat (SNF) content of 0.5 to 3.5
weight % and a pH value of 3.0 to 3.9 to heat treatment at ultra-high temperature.
Acidic pH is due to lactic fermentation and addition of sugar is optional.
[0006] US patent 4,192,901 eventually discloses a method for manufacturing a concentrate defined as "milk-containing
acid syrup" which is further used for preparing beverages by dilution with water.
In this case, the inventors have addressed a specific issue, i.e. the stabilization
of milk proteins by monitoring the casein / sugar ratio and subsequently subjecting
the acidified milk-sugar mixture to ultra-high temperature heating: inventors have
assumed that during said ultra-high temperature heat treatment, casein undergoes some
form of reaction with sugar and, hydrophilic property of the casein is significantly
enhanced.
[0007] Beverage dispensing machines or visual bowls are also quite popular in modem communities
so they are frequently used for dispensing various kinds of beverages in cans or even
as freshly prepared fruits juices or similar beverages. When refrigerated conditions
like those which should apply to "ready-to-drink" milk based beverages are necessary,
this is leading to use complex and expensive techniques or machines. Further, when
working with milk based beverages hygiene is a critical factor.
[0008] An approach would be to allow preparation of such acidified milk based beverages
immediately before consumption, for instance by storing separately sensitive or non
compatible components like e.g. milk and acid or fruit juice and then mix them on
demand. This way proved in fact unduly complex and expensive and, also, not suitable
for use in conventional beverage dispensing machines.
[0009] An other way to by-pass the above difficulties or drawbacks would be using stable
concentrated base compositions which would simply be diluted with water on demand,
i.e. just before consumption. The art, unfortunately, does not provide today any appropriate
solution to the skilled artisan.
[0010] The present invention offers an innovative and quite efficient solution to the skilled
artisan while providing him a storable, shelf-stable, concentrated base composition
which already comprises all the ingredients necessary for preparing an attractive,
acidified milk based beverage by mere dilution with water, namely by dilution in a
beverage dispensing or vending machine.
[0011] Further features or advantages of the present invention shall appear in the specification
here below.
Summary of the Invention
[0012] The present invention primarily refers to a shelf-stable liquid base composition
useful for preparing acidified milk based beverages, e.g. in beverage dispensers,
said liquid base composition comprising:
- a. from about 2 to about 10 weight % of denatured milk proteins expressed as solid-not-fat
(SNF) milk components;
- b. from about 15 to about 80 weight %, expressed as sugar equivalents, of a carbohydrate
based and/or non carbohydrate based sweetener;
- c. from about 0.35 to about 1.50 weight % of a carbohydrate based stabilizer; and
- d. an acidifying agent present in amounts necessary for achieving a pH of about 3.0
to about 3.8 of the said base composition.
[0013] The invention further refers to a method for preparing the said base composition,
which method comprises the sequence provided here below:
- heating a source of milk proteins at about 80 to about 120° C over a period of about
1 to about 20 minutes to achieve denaturising of the said milk proteins;
- mixing the source of denatured milk proteins with a carbohydrate based or non carbohydrate
based sweetener and with a carbohydrate based stabilizer;
- bringing the above mixture to a pH of about 3.0 to about 3.8 while mixing it with
an acidifying agent; and
- sterilizing or pasteurising the above acidified mixture and subsequently pouring it
into containers.
[0014] The invention also refers to another method for preparing the said liquid base composition,
which method comprises the sequence provided here below:
- heating a source of milk proteins at about 80 to about 120° C over a period of about
1 to about 20 minutes in presence of a carbohydrate based or non carbohydrate based
sweetener and of a carbohydrate based stabilizer;
- cooling down the heat treated mixture and bringing it to a pH of about 3.0 to about
3.8 while mixing it with an acidifying agent; and
- sterilizing or pasteurising the above acidified mixture and subsequently pouring it
aseptically into containers.
[0015] The invention, eventually, refers to a method for preparing acidified milk based
beverages by dilution of the relevant liquid base composition with an appropriate
amount of water and to the beverages so afforded as well.
[0016] In the acidified milk based beverage, the dilution of the liquid base composition
with an appropriate amount of water refers to diluting one part of said base composition
with 2 to 7 parts or water. Dilution can occur preferably in a beverage dispensing
machine under controlled dilution conditions. Controlled dilution conditions may require
the use of a pump for pumping the base composition at a certain flow rate and during
a controlled time and a pump for pumping the water at another flow rate and during
a controlled time and mixing said base composition and water in order to obtain the
desired ratio.
[0017] The acidified milk based beverage is preferably delivered with a protein content
of from 0.02 to 5% SNF and with sugar equivalent of from 7 to 10 weight %. The beverage
is also preferably delivered with a pH comprised between 3.6 and 4.2. A pH below 4.2
is preferred in order to guarantee a better machine hygiene. As a result of the base
composition as designed, the acidified milk based beverage experiences physical stability
for at least 1 hour after dispensing.
Detailed description of the Invention
[0018] One of the main characteristics of the invention consists in a well adjusted balance
of selected ingredients and their proportions in the base composition, more precisely
the milk proteins, a first class of carbohydrates such as sugars or sugar substitutes
acting as sweeteners, a second class of carbohydrates acting as stabilizers like gums,
pectins or the like acting as stabilizers and acid components. This adjusted balance
provides the conditions necessary for stabilizing the base composition and the "ready-to-drink"
beverage as well.
[0019] The use of this base composition represents another important feature of this invention.
This shelf-stable milk base is designed for application in beverage dispensers such
as e.g. visual bowls and juice dispensers. In both cases, the milk base offers convenience,
ease of handling over ready to drink beverages and less hygiene concerns. For machine
hygiene safety, the pH of the concentrate base composition and reconstituted beverage
is designed to stay below 4.2.
[0020] The specific heat treatment of selected ingredients like milk proteins represents
another feature of the invention as it is leading to denaturation of milk proteins
to such an extent that they remain stable when subjected to subsequent treatments
like acidifying, homogenising, pasteurising or the like and filling. Surprisingly,
the stability of the base composition so achieved is further reflected in the "ready-to-drink"
acidified milk base beverages, which are prepared by mere dilution with an appropriate
amount of water.
[0021] According to the invention the liquid base composition comprises from about 2.0 to
about 10 weight %, preferably from about 3.6 to about 6.0 weight % of denatured milk
protein. Within the frame of the invention, proportions of milk proteins of are preferably
expressed when referring to "solid-not-fat" or "SNF" milk components although simple
weight percent may also be used to that purpose. In such a case 2.0 to 10 weight %
(SNF) would be equivalent to 0.7 to 3.6 g of milk proteins in 100 grams of base composition.
Weight percent are expressed as referring to the total weight of the base composition,
i.e. the concentrate.
[0022] Suitable sources of milk proteins subjected to denaturing within the frame of this
invention are conveniently selected form fresh and powder whole or semi skimmed or
fully skimmed milk. Sodium caseinate, calcium caseinate, milk protein isolates, milk
protein concentrates or whey proteins can also be used.
[0023] According to the invention the milk proteins have been denatured by heat treatment.
Said treatment is generally performed by subjecting a liquid source of milk proteins
at temperatures comprised between about 80 to about 120° C, over a period of about
1 to 20 minutes depending on the manufacturing capabilities, preferably from 110 to
120° C to a period of 2 to 5 minutes. The selected temperature and time conditions
need to be addressed to achieve a degree of denaturation of at least 75%. The milk
protein denaturing heat treatment may also be carried out as part of the processing
for transforming liquid milk into heat milk powder. Therefore, high heat milk powder
can be used when heat treatment has already been applied to the milk proteins to denature
them. High heat milk powder refers to powder having a whey protein nitrogen index
below 1.5 mg N/g. The "whey protein nitrogen index" refers to the amount of still
denaturable serum protein left in the powder as described in literature, especially,
in "Walstra, P., J.T.M. Wouters, T.J. Geurts, Dairy Science and Technology, Second
ed, Boca Raton: CRC Taylor & Francis", page 530. A subsequent heat treatment can consequently
be reduced to 85°C for a few seconds or may even not be necessary.
[0024] The said heat treatment can be performed either in the presence of carbohydrates
such as those mentioned here below, or not.
[0025] Carbohydrates are also key ingredients within the frame of the present invention;
they comprise two groups each of them having a specific role to play:
- a first group of carbohydrates consisting of sugars which act, mainly, as sweeteners
in the "ready-to-drink" beverage. The term sugars is intended to cover ingredients
such as fructose, glucose, maltose, sucrose, lactose, dextrose, high fructose corn
syrup or sugar substitutes like e.g. sorbitol, mannitol, xylitol or combinations thereof.
These carbohydrates also offer the advantage of reducing the water activity of the
base composition and consequently, further reducing the risk of growth from bacteria,
yeasts or moulds;
- a second group of carbohydrates comprises polysaccharides acting as stabilizers in
both the base composition and the acidified milk base "ready-to-drink" beverage. Such
polysaccharides are preferably selected among gums, pectins or pectin derivatives,
cellulose derivatives like sodium carboxymethylcellulose, carrageenan or carrageenan
derivatives or mixtures of same. One of their main functions consists in controlling
the viscosity and the stability of the base composition, especially when the latter
is designed for beverage dispensing or vending machines.
[0026] Proportions of carbohydrate base sweeteners, when referred to within the frame of
the invention, are preferably expressed as "sugar equivalents" although simple weight
percent may also be used to that purpose. The terms "sugar equivalents" within the
frame of this invention, are meant to qualify ingredients such as non-carbohydrate
based, artificial, sweeteners that can replace sucrose. In terms of concentration
by weight, for example a milk base containing 40% wt sucrose is equivalent in terms
of sweetness to a milk base containing approximately 0.2% wt of aspartame.
[0027] Non-carbohydrate based sweeteners like e.g. Splenda®, Acesulfame K®, aspartame or
Stevia® are conveniently used within the frame of the present invention. For calculation
of sugar equivalents of artificial sweeteners and other carbohydrates based sweeteners,
relative sweetening powders compared to sucrose, the conversion factors were taken
from literature:
- "Birch, G. Ingredients handbook sweeteners, Second ed. Surrey: Leatherhead Publishing"
and,
- "Alexander, R. J. Sweeteners: nutritive, St. Paul: Eagan Press", page 40.
[0028] Sugar equivalent levels are usually comprised between about 15 to about 80 weight
%, preferably between about 30 and 60 wt% and most preferably between 40 and 55%.
[0029] It has been observed that, by setting the level of sucrose between 40 and 55 weight
%, good stability of the base composition could be achieved over a period running
up to 12 months at 20°C: the term "shelf-stable" or "storable" used throughout the
current specification qualifies these conditions, although shorter storage periods
or lower storage temperatures may be contemplated. No serum separation or precipitates
were observed in the said base composition. After dilution with water, a "ready-to-drink"
beverage was achieved which remained quite stable over 1 week of storage at refrigerated
conditions.
[0030] When the level of sucrose was set in the range of 30 to less than 40 %, good stability
of the corresponding base composition was also achieved over a period running up to
6 months at ambient conditions; minor serum separation but with some sedimentation,
however, have been observed in the base composition but this effect did not prevent
convenient dilution of the said base with water and no specific negative effect was
noticed in the "ready-to-drink" acidified beverage.
[0031] Polysaccharides stabilizers are useful for achieving the desired viscosity and density
and best results have been achieved in terms of viscosity range between 15 to 250
mPa.s, preferably, between 15 to 100 mPa.s of the base composition. It has been observed
that physical stability of the base composition is also closely related to the viscosity
value. In particular, when viscosity of the base composition is lower than 15 mPa.s,
the base composition is not stable and milk solid tends to separate from serum and
to settle at the bottom of container. Phase separation raises an important issue,
in particular, for delivering beverages in a beverage dispenser where no regular stirring
takes place and therefore quality of the final beverage can be dramatically affected
with high milk solid content variations in the final beverage.
[0032] One feature of the invention lies in selecting the most adequate polysaccharide to
be used as stabilizer. It has been surprisingly observed, however, that a level and
type of stabilizer that allowed having a stable base composition did not necessarily
provide a stable "ready-to-drink" beverage after dilution with water.
[0033] Therefore the goal of this invention is to provide stability for both the base composition
and the final beverage and, furthermore, to select a stabilizer that does not increase
the viscosity of the said base too much and that, at the same time, provides an acceptable
mouth feel in the final beverage. The advantage of not increasing the viscosity of
the composition too much is essentially that the composition can be pumped using conventional
dispenser equipment and can be diluted easily at cold or ambient temperature while
providing an homogeneously mixed beverage with water as a diluent, thus allowing to
use these base compositions even with very simple beverage dispensers. Further, the
amount of stabilizer used is dependent on the amount of milk proteins in the base;
within the frame of this invention, the most suitable proportions of the carbohydrate
based stabilizers (or polysaccharides) are comprised between about 0.35 to about 1.5
weight %, preferably from about 0.50 to about 1.00 weight %.
[0034] Eventually, the choice of the stabilizer is also directed by the pH of the base composition,
as the selected stabilizer needs to remain fairly active and stable at pH range below
4, preferably from 3.0 to about 3.8 during the whole processing and during storage
over prolonged periods.
[0035] Among the various polysaccharides mentioned here above, i.e. gums, pectin or pectin
derivatives, carrageenan or carrageenan derivatives or mixtures of same, guar gum,
locust bean and sodium carboxymethylcellulose represents preferred stabilizers. When
preparing a base composition having e.g. a SNF content of 3.6 weight %, of from 40
to 70 weight % of sugar equivalent concentration (which corresponds for example to
0.2 to 0.35 weight % of aspartame) and of high methyl ester pectin of about 0.4 and
0.7 weight % provide fairly stable base compositions; however, when the said base
is diluted with water, solid particles tend to settle at the bottom of the container
thus giving a beverage having an in-cup stability of max. 6 hours.
[0036] Best performances have been achieved by means of using high methyl ester pectin concentration
ranging from 0.7 to 1 weight % and both the base composition and the final beverages
exhibit the required stability and mouth feel.
[0037] Other polysaccharides such as acacia gum can be used at levels between 0.5 to 1 weight
percent, proteins do not coagulate after acidification and a homogenous product was
obtained.
[0038] Pectin or pectin derivatives like that mentioned above can also be combined with
other hydrocolloids such as K-carrageenan, sodium carboxymethylcellulose and acacia
gum: satisfying results have been obtained with both variants.
[0039] In particular, base compositions using non-sugar sweetener preferably require the
use of a combination of pectin or pectin derivatives and another stabilizer having
a thickening function in order to raise the viscosity of the base composition at or
above 15 mPa.s. If only pectin is used, viscosity may not so be reached and a stability
issue may be so appear. The additional stabilizer is preferably chosen in the group
of K-carrageenan, sodium carboxymethylcellulose and acacia gum, guar gum and locust
bean and combinations thereof.
[0040] Fat can also be present in the mixture subject to heat treatment mentioned here above.
In order to avoid fat stability in the composition by fat migrating and forming fat
globules at the surface of the liquid, it is also preferred that that fat is between
0.1 to 2 % weight of the base composition. By fat it is meant milk fat coming from
whole or semi skimmed milk used as source of proteins or, added fat like animal or
vegetable fat, when fully skimmed milk is used as source of proteins. Animal fat may
comprises e.g. butter oil or gee whereas vegetal fat may comprise e.g. palm kernel,
coconut, sunflower or soil oil.
[0041] Usually, fresh milk or milk powder is blended at 50°C with water, emulsifier, sugar
and melted fat if ever. Some of the sugar is used to dissolve the hydrocolloid (stabilizer)
in hot water (70-80°C) at high speed. The hydrocolloid solution is then added to the
milk base and the mixture is heat treated as mentioned here above. After heat treatment,
the milk and sugar concentrate is homogenized and cooled down to e.g. 4° C.
[0042] It has been observed that when working with "high heat milk powder" i.e., with whey
protein nitrogen index below 1.5 mg N/g, the pre heat treatment could be reduced to
85°C for a few seconds before cooling to 4°C or eliminated. If using low or medium
heat milk powders, the heat treatment should be adjusted accordingly. Low heat milk
powder refers to powder having whey protein nitrogen index above 6 mg N/g. Medium
heat milk powder refers to powder having whey nitrogen index between 1.5 and 6 mg
N/g.
Another advantage of using high heat milk powder is the higher viscosity that it brings
compared to low and medium heat powders.
[0043] According to the invention, dilution of the base composition with an appropriate
amount of water refers to diluting one part of said base composition with 2 to 7 parts
or water, e.g. in a beverage dispensing machine. Dilution of the concentrate leads
to a product with pH lower than 4.2, with a sugar content of from 5 to 10 g/100ml
and milk protein content of from 0.01 to 1.8 g/100ml.
[0044] According to the invention the mixture once subjected to the heat treatment leading
to denaturation of the milk proteins is then cooled to temperature below 10°C and
subsequently brought to the convenient pH range; said pH range is a further key feature
of the invention. Usually, from a mere stability point of view it is recommended to
decrease the pH of the concentrate base composition to below 3.7 in order to obtain
a stable isoelectric point of the milk proteins. However, such a low pH is not recommended
for the consumption of a "ready-to-drink" beverage due to taste issues and most of
the acidified beverages are usually consumed at a pH range of 4.0 to 4.4.
[0045] Thanks to the present invention this dilemma is conveniently solved by means of preparing
a base composition the pH range of which can be lowered to an optimal level for the
milk proteins, i.e. a pH of about 3.0 to about 3.5, without affecting the said milk
proteins and by diluting it subsequently with the appropriate amount of water and
so bringing the final beverage to pH between 3.6. and 4.2.
[0046] For applications with beverage dispensers and visual bowls, it is important that
the concentrates or final beverages are kept refrigerated after opening and the pH
of the product is below 4.2; therefore, below the pH range where pathogenic bacteria
can grow. For best results, the pH of the concentrates is designed so that the pH
of the final beverage is between 4.0 and 4.1.
[0047] Acidifying agents usable within the frame on the invention comprise edible organic
acids such as e.g. citric, malic, tartaric or lactic acid. The selected acids are
mixed with water in the ratio of about 30:70 and used to acidify the heated mixture
of sugars, stabilizer, milk proteins and fat. Acidification is generally performed
at 4°C and by adding the above mixture to the acid solution. This type of acidification
is preferred because the milk proteins pass quickly below the isoelectric point around
4.6 and then stay in a pH range of below 4.
[0048] Acidification can also be performed by means of fruit juices/concentrates like apple,
pear, lemon juice, orange juices, kiwi juice or exotic fruit juices to which acid
content has been adjusted accordingly. When doing so the acidification further brings
selected flavor components or vitamins. Of course artificial flavor components or
minerals or micronutrients can also be added to the whole mixture.
[0049] Flavors and colorants are usually added to the mixture before final heat treatment,
e.g. pasteurization. Nutrients like vitamins, minerals (Ca
++ and Mg
++) etc. can be added at this stage without flavor and insolubility issues. In all cases,
the dosage of these ingredients must be calculated based on the dilution factor to
achieve the proper final beverages.
[0050] The base composition is heat treated to e.g. 100° C for 10 sec using either direct
or indirect method, then aseptically homogenized, cooled to 30° C and eventually poured
into suitable containers aseptically, or by clean or hot filling.
[0051] The following examples shall only illustrate some of the embodiments of the invention.
Example 1
[0052] 40g sucrose and 45 g of partially skimmed milk were mixed at 50°C with added hydrated
solution of stabilizers such as K-carrageenan and pectin. The solution was heat treated
for 2 minutes at 120° C to denature the proteins, then homogenized and cooled down
to 4° C.
The pH of the solution was quickly adjusted to 3.5 with agitation by addition of 30
% citric acid solution. Colours and flavours are added at this stage. The acidified
product (with viscosity of 50 mPa.s) was mixed for 30 minutes and then pasteurized
and poured aseptically into storage containers.
[0053] The resulting base concentrate had 2.40 % weight of SNF and 40 % weight of sugar
equivalent.
[0054] Such a product will be consumed after dilution of 1 part of concentrate with 4 parts
of water giving acidified milk based beverage having a final pH of 4.0.
Example 2
[0055] 20g sucrose and 45 g of partially skimmed milk were mixed at 50°C with added hydrated
solution of stabilizers such as K-carrageenan and pectin. To increase the sweetness
level, 0.02 g of sucralose from Splenda® was added to the mixture. The solution was
heat treated for 1 minute at 100° C, then homogenized and cooled down to 4° C.
[0056] The pH of the solution was quickly adjusted to 3.5 with agitation by addition of
30 % citric acid solution. Colours and flavours are added at this stage. The acidified
product (with viscosity of 45 mPa.s) was mixed for 30 minutes and then sterilized
and poured aseptically into storage containers.
[0057] The resulting base concentrate had 2.40 % weight of SNF and 32 % weight of sugar
equivalent.
[0058] A final milk based beverage having a pH of 4.0 has been obtained by dilution of 1
part of the base composition with 4 parts of water.
Example 3
[0059] 46g sucrose and 33.4g of fresh whole milk and 1.5g of skimmed milk powder were mixed
at 50° C with added hydrated solution of pectin. The solution was heat-treated, then
homogenized and cooled down to 20° C.
[0060] The pH of the solution quickly adjusted to 3.3 with agitation by addition of 30%
citric acid solution. Colours and flavours are added at this stage. The acidified
product (with viscosity of 60 mPa.s) was mixed for 30 minutes, sterilized and poured
aseptically into storage containers.
[0061] The resulting base concentrate had 4.40 % weight of SNF and 46 % weight of sugar
equivalent.
[0062] A final acidified milk based beverage is prepared by dilution of 1 part of base composition
with 5 parts of water leading to final pH of 4.0.
Example 4
[0063] 28g sucrose and 36.2 g of fresh whole milk, 2 g of "milk powder high heat" and 0.09
g of Splenda® sweetener were mixed at 50° C with added hydrated solution of stabilizers
such as 0.5% weight of CMC (Carboxymethylcellulose) and pectin 0.7 weight %. The solution
was cooled down to 20° C.
[0064] The pH of the solution was quickly adjusted to 3.2 with agitation by addition of
30% malic acid solution. Colours (0.1g) and flavours (0.35 g) are added at this stage.
The product had viscosity of 100 mPa.s. The concentration of colours and flavours
is 7 times higher than in a corresponding "ready-to-drink" beverage. The acidified
product was mixed for 30 minutes, sterilized and aseptically filled.
[0065] The resulting base concentrate had 6.00 % weight of SNF and 54 % weight of sugar
equivalent.
[0066] A final acidified milk based beverage is prepared by dilution of 1 part of base composition
with 6 parts of water (pH 4.1).
Example 5
[0067] 0.14 grams of Splenda® sweetener and 6.1 g of "milk powder high heat" were mixed
at ambient conditions with added hydrated solution of stabilizers such as pectin and
carboxymethyl cellulose The solution was heat treated for few seconds at 85°C and
then cooled down to 4° C.
[0068] The pH of the solution was quickly adjusted to 3.2 with agitation by addition of
30% malic acid solution. Colours (0.1g) and flavours (0.35 g) are added at this stage.
The product had viscosity of 200 mPa.s The acidified product was mixed for 30 minutes,
pasteurised and then poured in a clean manner into storage containers.
[0069] The resulting base concentrate had 6.00 % weight of SNF and 46 % weight of sugar
equivalent.
[0070] A final acidified milk based beverage is prepared by dilution of 1 part of base composition
with 6 parts of water (pH 4.1).
1. A shelf-stable liquid base composition for preparing acidified milk based beverages
comprising:
e. from about 2 to about 10 weight % of denatured milk proteins expressed as solid-not-fat
(SNF) milk components;
f. from about 15 to about 80 weight %, expressed as sugar equivalents, of a carbohydrate
based and/or non carbohydrate based sweetener;
g. from about 0.35 to about 1.50 weight % of a carbohydrate based stabilizer; and
h. an acidifying agent present in amounts necessary for achieving a pH of about 3.0
to about 3.8 of the said base composition.
2. The base composition according to claim 1, wherein the viscosity ranges of from 15
to 250 mPa.s.
3. The liquid base composition according to claim 1 or 2, wherein the denatured milk
proteins are milk proteins subj ected to heat treatment.
4. The liquid base composition according to claims 1, 2 or 3, wherein the carbohydrate-based
sweetener is a mono- or polysaccharide selected from the group consisting of sugars,
sugar substitutes, sugar derivatives and mixtures of same.
5. The liquid base composition according to any one of claims 1 to 4, wherein the carbohydrate-based
stabilizer is a polysaccharide selected from the group consisting of gums, pectins
and pectin derivatives, cellulose derivatives, carrageenan and carrageenan derivatives
and mixtures of same.
6. The liquid base composition according to claim 5, wherein the sweetener is essentially
a non-carbohydrate based sweetener and the stabililizer comprises pectin and at least
a stabilizer having a thickening function.
7. The liquid base composition according to anyone of claims 1 to 6, wherein the acidifying
agent is a comestible acid or a source of comestible acid, e.g. fruit juice.
8. The liquid base composition according to anyone of claims 1 to 7, which further comprises
fats, colorants, flavours or micronutrients.
9. A method for preparing a shelf-stable liquid base composition according to any one
of claims 1 to 8, which comprises:
- heating a source of milk proteins at about 80 to about 120° C over a period of about
1 to about 20 minutes to achieve denaturing of the said milk proteins;
- mixing the source of denatured milk proteins with a carbohydrate based or non carbohydrate
based sweetener and with a carbohydrate based stabilizer;
- bringing the above mixture to a pH of about 3.0 to about 3.8 while mixing it with
an acidifying agent; and
- sterilizing or pasteurising the above acidified mixture and subsequently pouring
it into containers.
10. A method for preparing a liquid base composition according to any one of claims 1
to 8, which comprises:
- heating a source of milk proteins at about 80 to about 120° C over a period of about
1 to about 20 minutes in presence of a carbohydrate based or non carbohydrate based
sweetener and of a carbohydrate based stabilizer;
- cooling down the heat treated mixture and bringing it to a pH of about 3.0 to about
3.8 while mixing it with an acidifying agent; and
- sterilizing or pasteurising the above acidified mixture and subsequently pouring
it into containers.
11. The method according to claims 9 or 10, wherein the carbohydrate-based sweetener is
a mono- or polysaccharide selected from the group consisting of sugars, sugar substitutes,
sugar derivatives and mixtures of same.
12. The method according to claims 9 or 10, wherein the carbohydrate-based stabilizer
is a polysaccharide selected from the group consisting of gums, pectins and pectin
derivatives, cellulose derivatives, carrageenan and carrageenan derivatives and mixtures
of same.
13. The method according to anyone of claims 9 to 13, wherein the acidifying agent is
an edible acid or a source of edible acid, e.g. fruit juice.
14. The method according to anyone of claims 9 to 13, wherein the mixture subject to heat
treatment further comprises fat or a source of fat.
15. The method according to anyone claims 9 to 14, wherein flavours, colorants or micronutrients
are added to the acidified mixture prior to sterilisation or pasteurisation.
16. A method for preparing acidified milk based beverages, which comprises diluting one
part of the liquid base composition according to anyone of claims 1 to 5 with 2 to
7 parts of water.
17. A method according to claim 16, wherein the acidified milk based beverage has a protein
content of from 0.02 to 5% solid non fat (SNF), sugar equivalent of from 7 to 10 weight
% and pH comprised between 3.6 and 4.2.
18. The method according to claim 16 or 17 wherein the preparation of the acidified milk
based beverage is performed by means of a beverage-dispensing machine.
19. An acidified milk based beverage prepared according to the method according to anyone
of claims 16 to 18.