BACKGROUND OF THE INVENTION
1. Field of the Invention
[0001] The present invention relates to a method of forming a metal component from a powdered
feed material.
[0002] The present invention also relates to an apparatus for forming a metal component
from a powdered feed material.
2. Description of the Related Art
[0003] Powder metallurgy is a known method for forming a metal component, from a powdered
feed material. In a known hot isostatic pressing (HIP) process, powder is shaped in
a steel mould to which both pressure and temperature are applied. Typically, argon
gas is used to provide the isostatic pressure which may range from 50 megapascal to
300 megapascal. During this process, the temperature of the material is raised so
as to sinter the powder and cause the particles to fuse together. However, known powder
metallurgy is limited in terms of the size of products that can be produced and also
in terms of the complexity of their shape. Furthermore, it is a costly and time consuming
process. It is difficult to scale and often impossible to produce products having
the required size and complexity when competing against products produced by a more
conventional casting process.
[0004] European Patent No.
0 708 187 discloses a method and apparatus for directional solidification of a melt. Refractory
particulates are provided about at least one region of a casting mould and are heated
using an induction heating system and a susceptor element. Heat is then conducted
from the particles to the mould.
BRIEF SUMMARY OF THE INVENTION
[0005] According to a first aspect of the present invention, there is provided a method
of the aforesaid type for forming a metal component from a powdered feed material,
comprising the steps of: creating a negative mould of a component from a ceramics
material having a melting point that is higher than the melting point of said powdered
feed material; deploying said feed material of metal powder into said mould; locating
said mould in a vacuum chamber having an induction or microwave heating system, said
heating system comprising a source of electromagnetic energy and a granular susceptance
material; and heating said mould using said induction heating system to a temperature
higher than the melting point of the metal powder so as to melt the metal powder within
the mould; wherein said granular susceptance material absorbs the energy of the induction
field generated by said source of electromagnetic energy and radiates infra-red energy
towards the ceramic mould. In an embodiment, during the deployment of the feed material
into the mould, a degree of vibration may be introduced to facilitate the dispersal
of the feed material within the mould.
[0006] According to a second aspect of the present invention, there is provided an apparatus
for forming a metal component from a powdered feed material, comprising: a negative
mould of a component comprised of a ceramics material having a melting point higher
than the melting point of said powdered feed material contained therein; and a vacuum
chamber for receiving said mould, the vacuum chamber being having a microwave or induction
heating system comprising a source of electromagnetic energy and a granular susceptance
material; wherein said granular susceptance material configured to absorb the energy
of the induction field generated by said source of electromagnetic energy and radiate
infra-red energy towards the ceramic mould.
BRIEF DESCRIPTION OF THE DRAWINGS
[0007]
Figure 1 shows a method of forming a metal component;
Figure 2 shows procedures for the creation of a positive model;
Figure 3 shows the addition of layers to produce a mould;
Figure 4 shows the deployment of feed material;
Figure 5 shows apparatus for forming a metal component;
Figure 6 shows a cross section of a feeder section;
Figure 7 shows the mould of Figure 5 after being loaded with metal powder;
Figure 8 shows the mould of Figure 7 with liquid metal;
Figure 9 shows a partial cross section view of the mould;
Figure 10 shows the view of Figure 9 after further cooling;
Figure 11 shows a mould of an alternative configuration;
Figure 12 illustrates a heating system;
Figure 13 shows an alternative embodiment of the mould; and
Figure 14 shows a mould immersed in a granular susceptance material.
DETAILED DESCRIPTION OF EXAMPLE EMBODIMENTS
Figure 1
[0008] A method of forming a metal component from a powdered feed material is illustrated
in Figure 1. A feed material is initially in a powdered state (detailed in Figure
4) and a solid component is formed by the application of heat (detailed in Figure
12). At step
101 a sacrificial positive model
102 of a component is created. At step
103, a negative mould
104 is built around the positive model from a material having a melting point higher
than the melting point of the material from which the component is to be formed (as
detailed in Figure 3).
[0009] At step
105 the sacrificial positive model is removed so as to leave a void
106 within the negative mould.
[0010] At step
107 feed material of metal powder
108 is deployed into the mould. At step
109 heat 110 is applied to the mould to a temperature higher than the melting point of the metal
powder so as to cause the metal powder to melt within the mould, thereby establishing
molten metal
111 within the mould
104.
[0011] The metal powder
108 used herein to form a metal component is, in a first embodiment, a powder consisting
of particles of pure metal. However, in an alternative embodiment metal powder
108 is a powder comprising particles of an alloy. It should be appreciated therefore,
that metal components formed from the said metal powder may be comprised either of
a pure metal or an alloy compound.
[0012] Whereas metal powders need to be graded to specific size ranges for known powder
metallurgy techniques, such as HIPping, powder metallurgy, metal injection moulding,
etc, the method described herein is relatively insensitive to the size range of the
powder particles. The only requirement is that the metal powder flows readily into
the ceramic moulds. Where the mould defines sections having diameters as little as
0.5 millimetres, spherical powders produced by gas atomisation, for example, would
be more appropriate. With larger mould sections, even angular powders produced by
crushing and milling would enable the mould to be filled, especially when the flow
of powder is aided by vibration, as will be described with reference to Figure 4.
Figure 2
[0013] Procedures for the creation of the positive sacrificial model are illustrated in
Figure 2. Operations are performed upon a source material
201 in order to produce the positive model
102. In a first embodiment, it is possible to perform a machining operation
202 upon an appropriate material in order to define the shape of the positive model.
However, it should be appreciated that the material used must be of a type such that
it is possible to remove the sacrificial material in order to define the negative
mould.
[0014] As an alternative, it is possible to perform a wax injection process
203. Having created a mould around the wax positive, it is possible to remove the wax
by the application of heat. Such an approach is known in conventional casting systems
where the heating of the mould is also desirable prior to the application of molten
metal. However, in an embodiment, the mould would be allowed to cool and the particulates
would be added at room temperature.
[0015] As an alternative, it is also possible to produce the positive mould by a process
of additive manufacturing
204, with an appropriate rapid prototyping material for example. The material may be removed
by the application of heat and/or the application of an appropriate solvent.
Figure 3
[0016] In the embodiment, the negative mould, having a melting point higher than the melting
point of the metal from which the component is to be formed, is a ceramic shell that
is relatively porous to air. In an embodiment, the ceramic mould is produced by adding
a plurality of layers, as shown in Figure 3.
[0017] In the embodiment shown in Figure 3, layers are added as an alternating wet slurry
layer followed by a substantially dry stucco layer.
[0018] Slurry
301 is applied to the model
102. Dry stucco
302 is then applied that attaches itself to the wet slurry in order to build a layer.
[0019] This process is repeated, as shown generally at
303, resulting in the build up of a layer
304. Thus, further repetitions are made until the negative mould
104 has been built to the required thickness. Ceramic mould 104 should ideally have relatively
thin wall sections so as to allow the conduction of radiant heat from a radiant heating
system therein, to enable the metal powder to be melted. However, the wall sections
must be sufficiently thick to prevent cracks or fracturing during processing, and
therefore a compromise must be reached in creating a mould that has a high thermal
conductivity, but is sufficiently strong.
[0020] In an embodiment, a primary refractory slurry is applied that is inert to the metal
being used. A dry sand of similar or different material is then applied and further
slurries are applied, followed by sand, stucco and so on.
[0021] A number of suitable ceramic materials for forming the ceramic shell are known, such
as silica and alumina. It has been found during testing that a silica shell does not
have a sufficiently high thermal conductivity to allow the powder metal charge to
be melted in a suitable time-frame using a radiant heating system. Therefore, in a
preferred embodiment, a negative mould comprised of an alumina material having a high
thermal conductivity is used. Other types of shell material having a high thermal
conductivity may be used, however they must not be susceptible to dissolution in the
molten metal as can be experienced by graphite based moulds when used certain metals.
Figure 4
[0022] Step
107 for the deployment of feed material is detailed in Figure 4. The positive sacrificial
model
102 has been removed as illustrated by step
105. The negative mould
104 is placed upon a vibrating table
401, itself supported by a stable base
402. In this way, as the feed material
108 is deployed into the mould
104, or after deployment, a degree of vibration is introduced, as illustrated by arrows
403 and
404, to facilitate the dispersal of the feed material within the mould. High frequency
vibration, e.g. 40-60 hertz, with low amplitude displacement of, say, 0.10-0.15 millimetres
enables moulds for large and complex metal components to be filled easily.
[0023] Thus, the feed material is deployed within the mould and then heated, as illustrated
by step
109. In an embodiment, the heat is applied without pressure and the mould is heated to
a temperature that causes the feed material to melt. In this way, it is possible to
obtain close to 100 percent density using a process that has less overall complexity
compared to known systems. The heat is required not only to raise the temperature
of the metal, but also to melt the metal completely. Consequently, it is typically
heated to around 50 degrees Celsius above the melting point of the metal, in the case
of a pure metal, or above the liquidus temperature in the case of an alloy.
[0024] In some known systems, contamination is often introduced from containers and this
is a particular problem when using titanium. Processes using solid state diffusion
result in the container experiencing a similar environment to the material contained
inside. Thus, even after machining away, it is possible that a significant layer of
a material mixture will remain. Consequently, additional processing is required in
order to achieve the required result.
[0025] It has been recognised that the use of metal powder as a feed material may produce
products having desirable properties. There is a tendency for the microstructure to
be very uniform, which may improve strength and fatigue properties. Properties of
this type may be provided by forging operations but, as is known, forging results
in the production of significant levels of waste and therefore increases overall cost.
Similarly, a casting process yield is typically 50 percent; again increasing cost,
which becomes an important factor when expensive alloys are being used.
Figure 5
[0026] An apparatus for forming a metal component from a powdered feed material is illustrated
in Figures 5 through 12. As previously described, a sacrificial positive model is
created and a negative mould is built around the positive model from a material having
a melting point higher than the melting point of the metal from which the material
is formed. Thus, this results in the creation of a negative mould, preferably a ceramic
mould 501.
[0027] The sacrificial positive model is removed from the negative mould 501. The apparatus
further comprises a deploying device for deploying the feed material of metal powder
into the mould
501, and a heating system for heating the metal powder to a temperature higher than the
melting point of the metal powder so as to cause the metal powder to melt within the
mould.
[0028] An example of a mould
501 is illustrated in Figure 5 in cross-section. The mould
501 includes a component section
502 corresponding to the component to be produced and a feeder section
503. The feeder section
503 defines a generally cylindrical passageway
504, that may include an inwardly extending element as detailed in Figure 6. The feeder
section adjoins said component section at a first end and extends vertically upwards
towards a distal end that is open to allow insertion of feed materials up to a head
level.
[0029] The feeder section is provided because when metals cool from their molten liquid
state, their volume decreases as the temperature drops to the point where they are
solid. Thus, the feeder is used to provide additional liquefied metal to the mould
to compensate for the shrinkage cavities that would otherwise form at one or more
thermal centres in the interior of the casting as it cools. The volume of the feeder
is therefore determined by the requirement for sufficient liquid metal to be provided
in order to compensate for the volume reduction of the metal as it cools. Two factors
influence the efficiency of feeding; firstly, the metallostatic pressure in the feeder,
and secondly the pressure being applied to the liquid metal surface of the feeder
by the surrounding atmosphere. The metallostatic pressure head in the feeder assists
in forcing the molten metal into the mould section, as metal contained in the mould
section cools and decreases in volume.
[0030] The head of molten metal should remain molten at least until the metal in the component
section has solidified completely. To inhibit the conduction of thermal energy from
within the feeder section to outside the feeder section during cooling and to thereby
maintain the metal in the feeder in its molten state, the walls of the feeder section
should have a relatively lower thermal conductivity than the walls of the component
section. The feeder section may therefore be comprised of a different ceramic material
to said component section and may comprise insulating or exothermic ceramic powders.
Alternatively, the feeders may be wrapped in insulating material to ensure they solidify
later than the metal component and to ensure that the surface of the molten metal
in the feeder head remains molten so that any atmospheric pressure effects will assist
in feeding.
[0031] To maximise the metallostatic pressure, the feeder head should be raised as high
as is practically and economically feasible in order to maximise the metallostatic
pressure,
[0032] To further improve the degassing of molten metal in the component section and to
increase the pressure applied to the molten metal, one or more atmospheric cores may
be provided extending downwardly through the feeder section towards the component
section. These atmospheric cores may be pencil shaped ceramic tubes which are porous
to gasses and whose permeability allows atmospheric pressure to be applied to the
liquid metal in the thermal centre of the feeder section, and to allow gas trapped
within the liquefied metal to escape. A particular atmospheric core in the form of
an inwardly extending element is described further with reference to Figure 6.
[0033] In an embodiment, the ceramic mould is initially at room temperature, therefore it
is at a known and relatively constant temperature; compared to situations where the
mould may have been heated and the actual temperature of the mould, when material
may be added, may fall within a relatively wide range of possible temperatures. However,
in an embodiment where the temperature is known in terms of an initial temperature
and a melt temperature, it is possible to accurately calculate the volume of powder
required in the feeders. Thus, an optimum amount of material may be held in the feeders
so as to compensate for the 30-35 percent contraction in volume during the overall
process.
[0034] A cross-sectional view of the mould through horizontal plane
503 is illustrated in Figure 6.
Figure 6
[0035] The feeder section
503 defines a generally cylindrical passageway
504. The passageway
504 includes an atmospheric core, here provided by inwardly extending element
505 that is porous to gasses and extends inwardly from the generally cylindrical inside
surface
506 of the passageway
504 defined by the feeder towards the middle of the cylindrical passageway. In an embodiment,
the inwardly extending element
505 is substantially wedge-shaped, having faces arranged at an acute angle to each other,
to form a sharp edge
507 close to the middle of passageway
504 and is formed of the same porous material from which the feeder is formed.
[0036] In an embodiment the mould is located within the chamber of a vacuum furnace in order
to melt the metal powder within the mould. During this process, the inwardly extending
element provides a means for allowing the atmosphere in the chamber to access molten
metal in the feeder during cooling of the metal component, to allow gas trapped within
the molten material to be released. The inwardly extending element therefore functions
as an atmospheric core whose permeability allows pressure to be applied to the liquid
metal in a thermal centre of the feeder head and to allow gas to escape from the molten
metal in the component and feeder sections of the mould.
Figure 7
[0037] Mould
501 is shown in Figure 7, after being loaded with metal powder
108 during process
107. The metal powder has been poured into an open end
702 of the feeder
503 up to a head level, and vibrated (as described with reference to Figure 4) to compact
the metal powder
108. In an embodiment, the feeder is filled with metal powder to the top of said feeder.
The mould is then vibrated, resulting in the upper surface
703 of the metal powder in the feeder becoming lower, when compared to the level of the
powder before vibration.
[0038] In an embodiment, the metal powder is formed from substantially spherical particles.
Consequently, even after compaction by vibration, approximately 25-30 percent of the
volume taken up by the powder 108 comprises voids between the particles. In an alternative
embodiment, other shapes of particles may be deployed, either alone or in combination
with spherical partials. The inclusion of particles of this type may decrease the
volume taken up by voids within the powder.
Figure 8
[0039] Mould
501 is shown in Figure 8, after the metal powder
108 has melted to form a liquid metal
801. An upper surface
802 of the liquid metal has gone down the feeder when compared to the surface
703 of the powder. However, in this embodiment, the height of the molten metal
801 in the feeder is greater than twice the height of the section of the mould corresponding
to the metal object being produced. The height of the component section of the mould
corresponding to the component to be produced is indicated by arrow
803 and the height of the molten metal 801 in the feeder section
503 is indicated by arrow
804. Thus, in this embodiment, the height indicated by arrow
804 is more than twice the height of that indicated by arrow
803.
[0040] A pressure is created within the molten metal due to the weight of molten metal in
the feeder. By introducing a relatively high feeder of molten metal, sufficient pressure
may be produced in the molten metal within the mould to ensure that the molten metal
is forced into fine details of the mould surface.
Figure 9
[0041] A partial cross-sectional view of the mould
501 is illustrated in Figure 9. As the mould cools, heat is conducted from the molten
metal through the walls of the mould. Consequently, the outside of the molten metal
tends to solidify first, with the solidification process continuing in an inward direction.
[0042] In the example of Figure 9, region
901, adjacent to the walls of the mould, is in the process of crystallizing, whereas portions
of the metal away from the walls are still liquid. During solidification, the metal
contracts typically by about 7 percent by volume and consequently voids
902 form within the molten metal.
Figure 10
[0043] When voids are surrounded by molten metal, metal will tend to fall into the void
under gravity, resulting in voids appearing to rise up the mould.
[0044] In an embodiment, the feeder is arranged such that the voids rise into the feeder
and metal within the feeder falls into the mould to ensure that the mould is completely
filed.
[0045] In the example shown in Figure 10, voids
902 have coalesced to form a single void
1001 that has risen up to the feeder.
[0046] Generally, voids, such as void
1001, will define a volume of space containing a vacuum. However, these voids may contain
some gas that has become trapped by the molten metal within the mould. In an embodiment,
the inwardly extending element
505 provides a means for allowing gas trapped within the molten metal in the feeder to
escape. The inwardly extending element is able to do this because it is a relatively
good insulator of heat (compared to the metal itself) and it extends into the molten
core of the metal within the feeder. Furthermore, the element is porous to gases.
Figure 11
[0047] The mould described with reference to Figures 5 through 10 has a single feeder that
provides a means of receiving powder into the mould, while also providing a metallostatic
head for producing an elevated metallostatic pressure in the mould. However, in an
alternative embodiment, one or more additional feeders may be provided; separate from
the feeder providing the metallostatic head pressure.
[0048] An example is shown in Figure 11 in which a mould
1101 has a lower section
1102 corresponding to the metal object to be produced. In addition, the mould has a first
feeder
1103, a second feeder
1104 and a third feeder
1105.
[0049] The second feeder
1104 is substantially similar to the feeder
503 shown in Figure 5, having a height that is more than twice the height of section
1102 and providing an opening
1106 at its upper end for receiving powdered metal
1107.
[0050] The first feeder
1103 and the third feeder
1105 are similar to feeder
1104 but differ in that their heights are substantially less than the height of the second
feeder
1104. Furthermore, their upper ends have been capped such that said ends are completely
sealed.
[0051] The first feeder
1103 and the third feeder
1105 contain powdered metal for feeding section
1102. They also define a passageway, for receiving voids formed in the molten metal during
the cooling process. However, the metallostatic pressure is provided by the second
feeder
1104. Initially open feeders may be formed on moulds and subsequently sealed by a cap that
is cemented in place. Alternatively, the feeders may be formed during the manufacture
of the mould with a sealed upper end.
Figure 12
[0052] An embodiment of an apparatus for forming a metal component from a powdered feed
material is shown in Figure 12. In the embodiment, the induction heating system includes
a source of electromagnetic energy, such as coil
1207 for generating radio frequency energy from an electrical supply, along with a control
circuit for controlling the electrical supply in order to control temperature. The
apparatus further comprises a granular susceptor material, which is in this embodiment
contained with the walls of moulds
501.
[0053] A granular susceptor is a preferred form of susceptor material as it enables the
susceptor to be contoured to the shape of the mould to which heat is to be applied.
In an embodiment a refractory tube is formed of a ceramic material in a shape corresponding
to the shape of the mould it heats. The tube is then filled with a granular susceptance
material which acts to radiate heat to the adjacent mould. This provides a very versatile
susceptor element, which is not otherwise possible when using a solid susceptor ingot
which is hard to machine to an appropriate shape. In a specific embodiment, discussed
with reference to Figure 14, the granular susceptor material forms a loose bed into
which the mould is wholly immersed, thereby ensuring intimate contact between susceptor
and mould and an efficient transfer of thermal energy.
[0054] An embodiment of the invention further includes pressure reduction apparatus configured
to reduce the pressure of a chamber to a pressure below atmospheric pressure. An example
of this apparatus is shown in Figure 12. Pressure reduction is desirable in order
to reduce contamination from the surrounding atmosphere. However, although extremely
low pressures are possible, vapour pressure is required within the chamber in order
to prevent evaporation of the molten material.
[0055] The apparatus, indicated generally at
1201, has a vacuum furnace
1202. The vacuum furnace has a vacuum-tight vessel
1203, with a refractory lining
1204, defining a vacuum chamber
1205.
[0056] Vessel
1203 is provided with a door
1206, for the purpose of providing access to the chamber
1205, thereby allowing the chamber to be loaded and unloaded with moulds, such as mould
501.
[0057] In an embodiment, the vacuum furnace
1202 has a radio frequency coil 1207 connected to a suitable electrical power supply
1208. Typically, radio frequency coils are formed of molybdenum, but the full specification
of the vacuum furnace will depend upon the specific types of metals and alloys that
are being used in the process. Furthermore, the specification will also depend upon
the requirements of the metal objects that are being formed.
[0058] In an embodiment, the vacuum furnace, its radiation source and power supply are selected
such that the temperature of the chamber may be raised to a temperature in excess
of 2000 degrees Celsius. Furnaces with these capabilities are commercially available,
generally for the purpose of providing heat treatment operations.
[0059] Chamber
1205 is connected to a vacuum system
1209 for evacuating air from the chamber, such that pressures in the chamber may be reduced
to levels substantially below atmospheric pressure.
[0060] The chamber
1205 has an inlet port
1211 connected to a noble gas supply. In an embodiment, a tank
1212 of compressed helium may be provided in combination with a tank
1213 of compressed argon.
[0061] The apparatus
1201 also includes a fan
1214 having an inlet connected to outlet port
1210 of chamber
1205 and an outlet connected to the inlet port
1211. In an embodiment, helium gas is supplied to the chamber
1205 up to a predetermined pressure and the gas is circulated by the fan
1214 to provide a cooling draft over the moulds contained in the chamber.
[0062] Temperature sensors
1215 are located within the chamber and in preferred embodiments placed in contact with
the moulds so as to provide signals indicative of an actual temperature of the powdered
or molten metal in the moulds located within the chamber. The apparatus also includes
a vacuum pressure gauge
1216 configured to provide an indication of vacuum pressure within the chamber.
[0063] In an embodiment, the pressure gauge
1216 and the temperature sensor
1215 are arranged to provide signals to a controller
1217 indicative of the pressure and temperature of the chamber. The controller is arranged
to operate the power supply
1208 for the resistance heating element
1207 and the vacuum system
1209, in response to the signals received from gauge 1216 and sensor
1215. In an embodiment, controller
1217 is a programmed computer system or a microcontroller.
Figure 13
[0064] An alternative embodiment of the present invention is illustrated at
1301 in Figure 13. To form a metal component, a mould
1302 is filled with metal particles
1303. A source
1304 of electro-magnetic radiation is provided and a susceptance material is configured
to be heated in response to receiving electro-magnetic radiation and to thermally
heat the metal particles
1303. it has been determined that when heating a metal powder in a ceramic mould using
induction heating, the induction field couples too weakly with the powder metal itself
to melt it. The ceramic mould of the present invention, unlike a conventional metal
mould is relatively transparent to the induction field and is therefore not itself
heated. Therefore, when heating using an induction field, a radiant susceptor is preferred.
The susceptor is chosen to be of a material so that it absorbs the energy of the induction
field and radiates infra-red energy towards the ceramic mould. This causes the ceramic
mould to be heated, which in turn heats the metal powder contained within.
[0065] In an embodiment, the electro-magnetic radiation is microwave radiation and said
apparatus further comprises a source of microwave radiation, in the form of a microwave
generator. Microwave radiation is a preferred type of energy as it is efficiently
generated and easily guided. When using microwave energy a preferred susceptor material
is silicon carbide. Silicon carbide is less prone to thermal degradation than many
other susceptor materials and it can typically be heated to temperatures in excess
of 3000 degrees Celsius. In the embodiment shown at
1301, the granular susceptance material is included in the mould
1302 itself however, it is possible for a granular susceptor mass to be provided separately,
in a configuration substantially similar to that shown in Figure 14.
Figure 14
[0066] An alternative embodiment for forming a metal component is shown at
1401. A mould
1402 receives metal particles
1403. A source
1404 emits electro-magnetic radiation directed towards a container
1405. The container
1405 is substantially transparent to the radiation emitted by source
1404 and a susceptance material
1406 is included, within container
1405 that surrounds the mould
1402. In the illustrated embodiment, the susceptance material
1406 is a granular particulate material comprised of particles of silicon carbide. A granular
susceptance material is preferred in some applications as it allows suscepted heat
to be applied intimately to the mould. In the illustrated embodiment, container
1405 is filled with particles
1406 of the susceptance material and mould
1402 is placed in the container so as to be partially or wholly immersed in granular susceptance
material
1406. By immersing mould
1402 in susceptance material
1406 not only is thermal energy efficiently transferred from the susceptance material
1406 to the surface of mould
1402, but also mould
1402 is supported by susceptance material
1406, thereby reducing the risk of the mould fracturing when loaded with metal powder
1403.
1. A method of forming a metal component from a powdered feed material (108), comprising
the steps of:
creating a negative mould (104, 501) of a component from a ceramics material having
a melting point that is higher than the melting point of said powdered feed material;
deploying said feed material of metal powder into said mould;
locating said mould in a vacuum chamber (1205) having an induction or microwave heating
system, said heating system comprising a source of electromagnetic energy (1207, 1304,
1404) and a granular susceptance material; and
heating said mould using said heating system to a temperature higher than the melting
point of the metal powder so as to melt said metal powder within the mould; wherein
said granular susceptance material absorbs the energy of the field generated by said
source of electromagnetic energy and radiates infra-red energy towards the ceramic
mould.
2. The method of claim 1, wherein said negative mould is built about a sacrificial positive
model (102) of the component.
3. The method of claim 2, wherein said step of building said negative mould consists
of adding a plurality of layers (304) to the outside of said positive model.
4. The method of claim 1, wherein said step of heating said mould using said heating
system comprises the step of generating microwave energy.
5. The method of claim 1, wherein said granular susceptance material is comprised of
particles (1406) of silicon carbide.
6. The method of claim 3, wherein said plurality of layers comprises a primary refractory
slurry (301) that is inert to said powdered feed material.
7. The method of claim 3, wherein the plurality of layers are applied as an alternating
wet slurry layer (301) followed by a substantially dry stucco layer (302) and said
alternating slurry layers and stucco layers contain substantially similar ceramic
material.
8. The method of claim 1, further comprising the step of feeding additional liquefied
metal into said mould as said mould cools and the metal contained within said mould
contracts.
9. The method of claim 8, further comprising the step of feeding said additional liquefied
material into a feeder section (503) up to a head level to assist in forcing molten
metal into the mould during cooling.
10. The method of claim 9, further comprising the step of providing an atmospheric core
(505) to said feeder section and allowing gas trapped within said liquefied metal
to escape via said atmospheric core.
11. An apparatus for forming a metal component from a powdered feed material (108), comprising:
a negative mould (104, 501) of a component comprised of a ceramics material having
a melting point higher than the melting point of said powdered feed material contained
therein; and
a vacuum chamber (1205) for receiving said mould, the vacuum chamber having an induction
or microwave heating system, comprising a source of electromagnetic energy (1207,
1304, 1404) and a granular susceptance material, wherein
said granular susceptance material is configured to absorb the energy of the field
generated by said source of electromagnetic energy and radiate infra-red energy towards
the ceramic mould.
12. The apparatus of claim 11, further comprising a sacrificial positive model (102) of
the component to be formed about which said negative mould is built.
13. The apparatus of claim 11, wherein said granular susceptance material is comprised
of particles (1406) of silicon carbide.
14. The apparatus of claim 11, wherein said source of electromagnetic energy comprises
a source of microwave radiation.
15. The apparatus of claim 11, wherein said negative mould is comprised of an alumina
material having a high thermal conductivity.
16. The apparatus of claim 11, wherein the negative mould defines a component section
(502) corresponding to the metal component being produced and a feeder section (503)
for feeding additional liquefied metal into said component section as said mould cools
and the metal contained within contracts.
17. The apparatus of claim 16, wherein said feeder section extends vertically upwards
from said component section and comprises a head level, and the difference in height
between the top of said component section and said head level is more than twice the
height of said component section.
18. The apparatus of claim 16, wherein said feeder section has a first end adjoining said
component section and a distal end extending therefrom and open to allow insertion
of feed materials up to said head level.
19. The apparatus of claim 16, wherein said feeder section comprises an atmospheric core
(505) that is porous to gasses for allowing gas trapped within the liquefied metal
in said feeder section to escape.
1. Eine Methode, eine Metallkomponente aus einem pulverisierten Aufgabematerial (108)
zu formen, die die folgenden Schritte umfasst:
Erstellung einer Negativform (104, 501) einer Komponente aus einem Keramikmaterial,
dessen Schmelzpunkt höher liegt als der Schmelzpunkt des besagten pulverisierten Aufgabematerials;
Einbringung des besagten Aufgabematerials aus Metallpulver in besagte Form;
Platzierung besagter Form in einer Vakuumkammer (1205), die ein Induktions- oder Mikrowellenheizsystem
hat, wobei das besagte Heizsystem eine Quelle elektromagnetischer Energie (1207, 1304,
1404) und ein granulares Suszeptanzmaterial umfasst; und
Erhitzen besagter Form durch besagtes Heizsystem auf eine Temperatur, die höher als
der Schmelzpunkt des Metallpulvers liegt, um besagtes Metallpulver in der Form zu
schmelzen; wobei
besagtes granulares Suszeptanzmaterial die Energie des Feldes, das durch besagte Quelle
elektromagnetischer Energie generiert wird, aufnimmt, und Infrarotenergie in Richtung
der Keramikform ausstrahlt.
2. Die Methode aus Patentanspruch 1, wobei besagte Negativform um ein zerstörbares Positivmodell
(102) der Komponente herum gebaut wird.
3. Die Methode aus Patentanspruch 2, wobei besagter Schritt des Baus besagter Negativform
daraus besteht, der Außenseite des besagten Positivmodells eine Vielzahl an Schichten
(304) hinzuzufügen.
4. Die Methode aus Patentanspruch 1, wobei besagter Schritt des Erhitzens besagter Form
durch besagtes Heizsystem den Schritt der Generierung von Mikrowellenenergie umfasst.
5. Die Methode aus Patentanspruch 1, wobei besagtes granulares Suszeptanzmaterial aus
Partikeln (1406) von Siliziumkarbid besteht.
6. Die Methode aus Patentanspruch 3, wobei besagte Vielzahl an Schichten einen primären
feuerfesten Schlamm (301) umfasst, der gegenüber besagtem pulverisiertem Aufgabematerial
träge ist.
7. Die Methode aus Patentanspruch 3, wobei die Vielzahl an Schichten als eine abwechselnde
feuchte Schlammschicht (301), gefolgt von einer substantiell trockenen Stuckschicht
(302), aufgetragen werden, und besagte abwechselnde Schlamm- und Stuckschichten enthalten
substantiell ähnliches Keramikmaterial.
8. Die Methode aus Patentanspruch 1, die weiterhin den Schritt des Einbringens zusätzlichen
geschmolzenen Metalls in besagte Form umfasst, da die besagte Form abkühlt und das
Metall, das sich in besagter Form befindet, zusammenzieht.
9. Die Methode aus Patentanspruch 8, die weiterhin den Schritt des Einbringens besagten
zusätzlichen geschmolzenen Materials in ein Abgangsfeld (503) bis zu einer Kopfhöhe
umfasst, um dabei zu helfen, geschmolzenes Metall während des Abkühlens in die Form
zu zwingen.
10. Die Methode aus Patentanspruch 9, die weiterhin den Schritt der Zurverfügungstellung
eines atmosphärischen Kerns (505) für besagtes Abgangsfeld umfasst, und es in besagtem
geschmolzenem Metall eingeschlossenen Gas ermöglicht, über besagten atmosphärischen
Kern zu entweichen.
11. Ein Apparat zur Erstellung einer Metallkomponente aus einem pulverisierten Aufgabematerial
(108), der folgendes umfasst:
eine Negativform (104, 501) einer Komponente aus einem Keramikmaterial, dessen Schmelzpunkt
höher liegt als der Schmelzpunkt des besagten pulverisierten Aufgabematerials darin;
und
eine Vakuumkammer (1205) zur Aufnahme besagter Form, wobei die Vakuumkammer ein Induktions-
oder Mikrowellenheizsystem hat, das eine Quelle elektromagnetischer Energie (1207,
1304, 1404) und ein granulares Suszeptanzmaterial umfasst, wobei
besagtes granulares Suszeptanzmaterial so konfiguriert ist, die Energie des Feldes,
das durch besagte Quelle elektromagnetischer Energie generiert wird, aufnimmt, und
Infrarotenergie in Richtung der Keramikform ausstrahlt.
12. Der Apparat aus Patentanspruch 11, der weiterhin ein zerstörbares Positivmodell (102)
der zu formenden Komponente umfasst, um die besagte Negativform herum gebaut wird.
13. Der Apparat aus Patentanspruch 11, wobei besagtes granulares Suszeptanzmaterial aus
Partikeln (1406) von Siliziumkarbid besteht.
14. Der Apparat aus Patentanspruch 11, wobei besagte Quelle elektromagnetischer Energie
eine Quelle für Mikrowellenstrahlung umfasst.
15. Der Apparat aus Patentanspruch 11, wobei besagte Negativform aus einem Aluminiummaterial
besteht, das eine hohe thermische Leitfähigkeit besitzt.
16. Der Apparat aus Patentanspruch 11, wobei die Negativform einen Komponentenbereich
definiert (502), der mit der zu produzierenden Metallkomponente und einem Abgangsfeld
(503) zum Einbringen zusätzlichen geschmolzenen Metalls in besagten Komponentenbereich
übereinstimmt, da sich besagte Form abkühlt und das darin enthaltene Metall sich zusammenzieht.
17. Der Apparat aus Patentanspruch 16, wobei besagtes Abgangsfeld sich von besagtem Komponentenbereich
aus vertikal nach oben erstreckt und eine Kopfhöhe umfasst, und der Höhenunterschied
zwischen der Spitze des besagten Komponentenbereichs und der besagten Kopfhöhe ist
mehr als die doppelte Höhe des besagten Komponentenbereichs.
18. Der Apparat aus Patentanspruch 16, wobei besagtes Abgangsfeld ein erstes Ende hat,
das an besagten Komponentenbereich angrenzt, und ein distales Ende, das sich von dort
aus erstreckt und sich öffnet, um das Einbringen von Aufgabematerialien bis zur besagten
Kopfhöhe zu ermöglichen.
19. Der Apparat aus Patentanspruch 16, wobei besagtes Abgangsfeld einen atmosphärischen
Kern (505) umfasst, der für Gase durchlässig ist, um in geschmolzenem Metall in besagtem
Abgangsfeld eingeschlossenes Gas entweichen zu lassen.
1. Méthode de formation d'un composant métallique à partir d'une matière première pulvérulente
(108), comprenant les étapes suivantes :
création d'un moule négatif (104, 501) d'un composant, réalisé avec un matériau céramique
dont le point de fusion est supérieur au point de fusion de ladite matière première
pulvérulente ;
déploiement de ladite matière première de poudre métallique dans ledit moule ;
positionnement dudit moule dans une chambre à vide (1205) possédant un système de
chauffage à induction ou à microondes, ledit système de chauffage possédant une source
d'énergie électromagnétique (1207, 1304, 1404) et une matière de susceptance granulaire
; et
chauffage dudit moule à l'aide dudit système de chauffage à une température supérieure
au point de fusion de la poudre métallique, de façon à opérer la fusion de ladite
poudre métallique au sein du moule ;
ladite matière de susceptance granulaire absorbant l'énergie du champ généré par ladite
source d'énergie électromagnétique, et rayonnant de l'énergie infrarouge vers le moule
de céramique.
2. Méthode selon la revendication 1, ledit moule négatif étant réalisé autour d'une maquette
positive sacrificielle (102) du composant.
3. Méthode selon la revendication 2, ladite étape de réalisation dudit moule négatif
comportant l'adjonction d'une pluralité de couches (304) sur l'extérieur de ladite
maquette positive.
4. Méthode selon la revendication 1, ladite étape de chauffage dudit moule à l'aide dudit
système de chauffage comportant l'étape de génération d'énergie de microondes.
5. Méthode selon la revendication 1, ladite matière de susceptance granulaire étant composée
de particules (1406) de carbure de silicium.
6. Méthode selon la revendication 3, la pluralité de couches comprenant une boue réfractaire
primaire (301) inerte à ladite matière première pulvérulente.
7. Méthode selon la revendication 3, la pluralité de couches étant appliquées en alternant
une couche de boue humide (301) avec une couche de stuc substantiellement sèche (302),
et lesdites couches de boue humide s'alternant avec des couches de stuc contenant
une matière céramique substantiellement similaire.
8. Méthode selon la revendication 1, comprenant en outre l'étape d'introduction d'un
métal liquéfié additionnel dans ledit moule, au fur et à mesure que ledit moule se
refroidit et le métal contenu dans ledit moule se contracte.
9. Méthode selon la revendication 8, comprenant en outre l'étape d'introduction ledit
métal liquéfié additionnel dans une section d'alimentation (503) jusqu'à un niveau
de tête, afin de contribuer à l'introduction forcée de métal en fusion dans le moule
au cours du refroidissement.
10. Méthode selon la revendication 9, comprenant en outre l'étape de fourniture d'un noyau
atmosphérique (505) à ladite section d'alimentation et d'évacuation du gaz piégé dans
ledit métal liquéfié via ledit noyau atmosphérique.
11. Appareil pour la formation d'un composant métallique à partir d'une matière première
pulvérulente (108), comprenant :
un moule négatif (104, 501) d'un composant, réalisé avec un matériau céramique dont
le point de fusion est supérieur au point de fusion de ladite matière première pulvérulente
contenue dans celui-ci ; et
une chambre à vide (1205) pour la réception dudit moule, la chambre à vide possédant
un système de chauffage à induction ou à microondes, comprenant une source d'énergie
électromagnétique (1207, 1304, 1404) et une matière de susceptance granulaire, dans
laquelle
ladite matière de susceptance granulaire est configurée pour absorber l'énergie du
champ généré par ladite source d'énergie électromagnétique, et rayonner de l'énergie
infrarouge vers le moule de céramique.
12. Appareil selon la revendication 11, comprenant en outre une maquette positive sacrificielle
(102) du composant à former, autour de laquelle est réalisé ledit moule négatif.
13. Appareil selon la revendication 11, ladite matière de susceptance granulaire étant
composée de particules (1406) de carbure de silicium.
14. Appareil selon la revendication 11, ladite source d'énergie électromagnétique comprenant
une source de rayonnement microondes.
15. Appareil selon la revendication 11, ledit moule négatif étant composé d'un matériau
d'alumine présentant une conductivité thermique élevée.
16. Appareil selon la revendication 11, ledit moule négatif définissant une section du
composant (502) correspondant au composant métallique en cours de production, et une
section d'alimentation (503) pour l'introduction d'un métal liquéfié dans ladite section
du composant au fur et à mesure que ledit moule se refroidit et le métal contenu dans
ledit moule se contracte.
17. Appareil selon la revendication 16, ladite section d'alimentation s'étendant verticalement
vers le haut depuis ladite section du composant, et comprenant un niveau de tête,
et la différence de hauteur entre le dessus ladite section du composant et ledit niveau
de tête mesurant plus du double de la hauteur de ladite section du composant.
18. Appareil selon la revendication 16, ladite section d'alimentation comprenant un premier
bout contigu à ladite section du composant, et une extrémité distale s'étendant depuis
celle-ci, et ouverte pour permettre l'insertion de matières premières jusqu'audit
niveau de tête.
19. Appareil selon la revendication 16, ladite section d'alimentation comprenant un noyau
atmosphérique (505) poreux aux gaz, afin de permettre l'échappement du gaz piégé au
sein du métal liquéfié dans ladite section d'alimentation.