Technical Field
[0001] The invention relates to a steel for use in machine-construction, to be used in manufacturing
various machine-construction parts, including an automotive part, and a construction
machinery part, etc. and in particular, to a steel for use in machine-construction,
having excellent machinability such that a machined cut-surface roughness can be reduced.
Background Art
[0002] In general, the various parts for use in machine-construction, such as an automotive
part, and a construction machinery part, etc., are each finished in a final shape
by applying forging, and so forth to a steel for use in machine-construction to be
followed by a cutting operation. At the time of applying the cutting operation, a
steel for use in machine-construction, exhibiting excellent machinability, is required
from the viewpoint of part accuracy and manufacturing efficiency. With respect to
a steel material for use in a forming tool, in particular, requirements for machined
cut-surface roughness have become severe, so that there is a demand for a steel for
use in machine-construction, capable of securing the machined cut-surface roughness,
smaller in size. If the machined cut-surface roughness becomes larger (more rough),
this will raise needs for applying further finishing to a surface state by grinding,
and so forth, thereby creating a problem in that a manufacturing process becomes complicated.
[0003] With respect to the steel for use in machine-construction, exhibiting excellent machinability,
there have thus far been proposed a variety of techniques. For example, in Patent
Literature 1, there is shown one of these techniques, indicating that if the content
of an element, such as C, Mn, P, S, Pb, O, Si, Al, etc., in a leaded free-cutting
steel, low in respect of carbon and sulfur, is specified, while specifying an average
size of an MnS based inclusion, and a proportion of a sulfide not bonded with an oxide,
this will enable machinability to be improved. Furthermore, excellent machined cut-surface
roughness can also be obtained.
[0004] With this technique, lead (Pb), as a useful element for improvement of machinability,
is contained in the basic components. Lead is well known as the element for use in
improving machinability, however, harmful effects of Pb on the human body and environments
are pointed out, and it is lately required to exhibit excellent machinability without
addition of Pb.
[0005] Under such circumstances described as above, progress has since been made in the
development of a technique capable of exhibiting excellent machinability without positive
addition of Pb. For example, in Patent Literature 2, there is disclosed that excellent
machinability equivalent to that of a Pb-added steel can be obtained by composite
addition of S, Te, and Ca. Further, it is disclosed that machinability can be further
improved by addition of Bi or a rare-earth element (REM) in the case of this technique.
[0006] Unfortunately, since a machinability-enhancing element (a free-cutting element),
such as Te, Bi, and REM, etc., is expensive, and an increase in manufacturing cost
will pose a problem.
[0007] On the other hand, in Patent Literature 3, there is proposed a free-cutting steel
for use in machine-construction, exhibiting the respective characteristics of the
mechanical property of a steel material, and the chip-segmentation property thereof
by causing a predetermined content of Mg to be contained under the presence of a sulfide-based
inclusion. With this technique, Mg is added in order to control the sulfide-based
inclusion to be kept in a predetermined shape and dispersed state. However, Mg being
a strong deoxidizing element in addition to Mg being susceptible to evaporation because
of a low boiling point, the steel in its oxide form is susceptible to be separated
from a molten steel. For this reason, a yield becomes low, thereby resulting in a
situation where an increase in cost is unavoidable.
Citation List
Patent Literature
Summary of Invention
Technical Problem
[0009] The present invention has been developed under such circumstances described as above,
and it is an object of the invention to provide a steel for use in machine-construction,
capable of exhibiting excellent machinability, in spite of a normal chemical composition
thereof, without use of Pb having harmful effects on the human body, and an expensive
free-cutting element, the steel being excellent in machined cut-surface roughness,
in particular.
Solution to Problem
[0010] According to the present invention which can achieve the above object, a steel for
use in machine-construction has a mixed microstructure including a hard phase composed
of at least one species selected from the group consisting of pearlite, bainite, and
martensite, and a ferrite phase. The gist of the present invention lies in that an
average equivalent circle diameter of ferrite grains is 7 µm or less, and a [(ferrite
grain) - (ferrite grain) connection rate X], as expressed by an equation (1) described
hereunder, is 0.15 or less provided that [(ferrite grain) - (ferrite grain) connection
rate X] = [the number (A) of [(ferrite grain) - (ferrite grain) interface surfaces]]
/ [the number (B) of [(ferrite grain) - (hard phase) interface surfaces]] ... (1),
and [the number (A) of [(ferrite grain) - (ferrite grain) interface surfaces]], in
the equation, indicates the number of intersection points between a straight line
and [the (ferrite grain) - (ferrite grain) interfaces], at the time of drawing a predetermined
straight line across a photograph taken by use of a scanning electron microscope,
whereas the number (B) of [(ferrite grain) - (hard phase) interface surfaces] indicates
the number of intersection points between the straight line and the [(ferrite grain)
- (hard phase) interfaces], at the time of drawing a predetermined straight line in
the same way as described above.
[0011] By "average equivalent circle diameter" is meant an average value of the respective
diameters of ferrite crystal grains (equivalent circle diameters) if the ferrite crystal
grain is converted into a circle equivalent thereto in area.
[0012] With respect to the chemical component composition of the steel for use in machine-construction,
according to the present invention, there is no particular limitation thereto in the
case of a steel for use in machine-construction, however, a preferable chemical component
composition may include C: 0.2 to 1.2% (mass %, the same applies to chemical component
composition hereinafter), Si: 0.05 to 0.5%, Mn: 0.2 to 1.8%, P: 0.03% or less (excluding
0%), and S: 0.03% or less (excluding 0%), the balance being iron and unavoidable impurities.
[0013] The preferable chemical component composition may further include at least one species
of element selected from the group consisting of Cr: 0.5% or less (excluding 0%),
Cu: 0.5% or less (excluding 0%), Ni: 0.5% or less (excluding 0%), and Mo: 0.5% or
less (excluding 0%), as necessary, which is effective, and the characteristics of
the steel for use in machine-construction are further improved depending on the species
of the element contained.
[0014] According to the invention, there is provided a method for improving the machined-surface
characteristics, and a steel product whose machined-surface characteristics is improved
can be obtained by cutting the steel for use in machine-construction, described as
above.
[0015] According to the invention, there is provided a method for manufacturing a forming
tool, having excellent surface characteristics, whereby the forming tool can be efficiently
manufactured by cutting the steel for use in machine-construction, according to the
invention, without application of a finish processing, such as grinding, etc., thereto.
Advantageous Effects of Invention
[0016] With the present invention, it is possible to realize a steel for use in machine-construction,
having a mixed microstructure including a hard phase composed of at least one species
selected from the group consisting of pearlite, bainite, and martensite and a ferrite
phase, by specifying that an average equivalent circle diameter of ferrite grains
is 7 µm or less, and a [(ferrite grain) - (ferrite grain) connection rate X] is expressed
by a prescribed relational expression, thereby enabling the steel to exhibit superior
machinability, and excellent machined cut-surface roughness, in particular.
Brief Description of Drawings
[0017]
Fig. 1A is a schematic diagram for depicting a relationship between the microstructure
of a steel material and the machined cut-surface roughness thereof, being a view showing
the initial state of a cutting operation.
Fig. 1B is a schematic diagram for depicting a relationship between the microstructure
of the steel material and the machined cut-surface roughness thereof, being a view
showing a state of the cutting operation, halfway through thereof.
Fig. 1C is a schematic diagram for depicting a relationship between the microstructure
of the steel material and the machined cut-surface roughness thereof, being a view
showing a state of the cutting operation, after the completion thereof.
Fig. 2A is a drawing-substitute photograph, showing a procedure for finding a [(ferrite
grain)-(ferrite grain) connection rate X], being a view showing the case of X ≤ 0.15.
Fig. 2B is a drawing-substitute photograph, showing a procedure for finding a [(ferrite
grain)-(ferrite grain) connection rate X], being a view showing the case of X ≥ 0.15.
Description of Embodiments
[0018] In order to realize a steel for use in machine-construction, capable of obtaining
excellent machined cut-surface roughness, in spite of a normal chemical composition
thereof, the inventor of the present invention, et al, have continued studies on a
relation of the steel with a metal microstructure thereof, in particular. As a result,
they have come up with an idea that one of the causes of deterioration in the machined
cut-surface roughness at the time of a cutting operation is the presence of phases
differing in hardness from each other, in a mixed state, inside a microstructure.
This state is described hereunder with reference to the drawings.
[0019] Figs. 1A through 1C each are a schematic diagram for depicting a relationship between
the microstructure of a steel material and the machined cut-surface roughness thereof.
In the figure, reference numeral 1 denotes a ferrite phase, and reference numeral
2 denotes a hard phase (a hard phase composed of at least one species selected from
the group consisting of pearlite, bainite, and martensite), respectively. The steel
material is of a mixed-microstructure construction, in which these phases are present
in a mixed state. In the figure, a portion of the steel material, on the upper side
thereof, indicates the upper surface of the steel material to be cut. At the time
of a cutting operation, the ferrite phase 1 that is soft in the mixed-microstructure
construction undergoes deformation as if pushed out by the hard phase 2, as shown
in Fig. 1A. Subsequently, the ferrite phase 1, in a such state as to be pushed out,
is removed by a cutting edge (the tip) of a tool, as shown in Fig. 1B. On a surface
(a worked surface) where the cutting edge of the tool has passed through, the ferrite
phase 1 is deformed in such a way as to be retracted, by the agency of elastic recovery
of the hard phase 2, as shown in Fig. 1C, so that a recess 3 occurs to the ferrite
phase 1 on the worked surface, and thereby the worked the surface roughness of the
steel material will undergo deterioration due to the presence of this recess.
[0020] The inventor of the present invention, et al, have proceeded to make further studies
on the requirements for obtaining excellent machined cut-surface roughness, on the
basis of the idea described as above. As a result, they have found out that if the
average equivalent circle diameter of the ferrite grains is set in a predetermined
range, and each portion where the ferrite grains are connected to each other is reduced
in number, this will enable the steel for use in machine-construction, capable of
obtaining excellent machined cut-surface roughness to be realized, whereupon the present
invention has been completed.
[0021] Respective requirements specified by the present invention are described hereunder.
[0022] In order to inhibit formation of the recess on the worked surface, it is necessary
to cause the soft ferrite phases to be finely dispersed. With the microstructure in
which the ferrite phases are finely dispersed, the individual phases become smaller
in size, and therefore, the volume of one soft phase, when pushed out by a phase that
is harder (the hard phase), will be smaller, and the recess occurring on the worked
surface, as well, will be smaller. As a result, there is developed a state in which
minute asperities are dispersed, thereby improving the worked surface roughness.
[0023] In order to cause soft ferrite phases to be in a finely dispersed state, it is necessary
to render the size of a ferrite grain (the grain size) as small as possible. With
the steel for use in machine-construction, according to the invention, in order to
ensure a desired dispersed-state of ferrites, the size (the grain size) of a ferrite
grain need be 7 µm or less in terms of the average equivalent circle diameter. Further,
the average equivalent circle diameter of the ferrites (the ferrite grains) is preferably
6 µm or less, and more preferably 5 µm or less. Still further, a preferable lower
limit of the average equivalent circle diameter of the ferrites (the ferrite grains)
is not less than 2 µm.
[0024] However, just to specify only the size of the ferrite grain is insufficient to attain
the object of the present invention. The reason for this is because there is a possibility
of occurrence of a phenomenon in which the ferrite grains, each thereof being small
in grain size, are connected to each other. If such a phenomenon described as above
occurs, a plurality of the ferrite grains are gathered together to thereby indicate
a state as if those ferrite grains behave as a large chunk of aggregated ferrite grains,
so that the ferrite grains grouped together, as a whole, will be pushed out by the
phase (the hard phase) harder than the ferrite phase. This state appears as if there
had occurred a phenomenon equivalent to the phenomenon in which a ferrite grain large
in grain size exists (the phenomenon causing deterioration in the machined cut-surface
roughness).
[0025] In contrast, in the case where the ferrite grain small in grain size is surrounded
by the hard phases, the volume of the ferrite phase, pushed out at a site of the ferrite
grain, is reduced, thereby causing the recess formed after the cutting operation to
be miniaturized, so that the worked surface roughness is rendered excellent. Further,
in the strict sense, the pearlite indicates a microstructure having a construction
in which ferrite and cementite sheet-like in shape are alternately, and lamellarly
arranged, however, such a microstructure as described above is en bloc referred to
as "pearlite" herein. Further, the ferrite as the target of the present invention
is a phase appearing white in a scanning electron microscope image upon nital etching
being applied thereto, by disregarding the lamellar ferrite in the pearlite.
[0026] With the present invention, in order to determine whether or not the ferrite grain
small in grain size exists in such a state as to be surrounded by the hard phases,
a concept referred to as a [(ferrite grain) - (ferrite grain) connection rate X] is
specified to be used for assessment. The [(ferrite grain) - (ferrite grain) connection
rate X] is expressed by the following equation (1).

[0027] At the time of drawing a predetermined straight line across a photograph taken by
use of a scanning electron microscope, [the number (A) of (ferrite grain) - (ferrite
grain) interface surfaces], in the equation, indicates the number of intersection
points between the straight line and [the (ferrite grain) - (ferrite grain) interface
surfaces], whereas the number (B) of [(ferrite grain) - (hard phase) interface surfaces]
indicates the number of intersection points between the straight line and the [(ferrite
grain) - (hard phase) interface surfaces], at the time of drawing a predetermined
straight line in the same way as described above.
[0028] A procedure for finding the [(the ferrite grain) - (ferrite grain) connection rate
X] is described hereunder with reference to the drawings. First, a metal microstructure
is portrayed and subsequently, a microstructure observation is made by use of the
scanning electron microscope (SEM). Horizontal line-segments are drawn across an observation
surface at regular intervals of 5 µm such that the total length (lengths in total)
of the horizontal line-segments is not less than 1000 µm, as shown in each of Figs.
2A, 2B, (the drawing-substitute photographs), to thereby find the number of the intersection
points (surrounded by □) between each of the line-segments and an interface between
the ferrite grains adjacent to each other, and the number of the intersection points
[a part surrounded by ○ (white outlined)], that is, the number (B) of the [(ferrite
grain) - (hard phase) interfaces], respectively. Subsequently, [the (ferrite grain)
- (ferrite grain) connection rate X] is calculated on the basis of the equation (1).
An observation area at the time of conducting an observation is preferably not less
than 40,000 µm
2 from the viewpoint of ensuring higher accuracy. Further, the total length (lengths
in total) of the line-segments horizontally drawn at the equal intervals is preferably
not less than 1000 µm for the same reason described as above.
[0029] If the value of the [(ferrite grain) - (ferrite grain) connection rate X], specified
as above, is small, this indicates that a region where the ferrite grains successively
exist is less in number, in other words, this indicates that the ferrite grains do
not successively exist, and each of the ferrite grains is surrounded by a hard phase
to be thereby isolated from each other so as to be in a dispersed state. Conversely,
if the value of the [(ferrite grain) - (ferrite grain) connection rate X], is large,
this indicates that the region where the ferrite grains successively exist is more
in number, in other words, the ferrite grains are susceptible to form a large aggregated
phase.
[0030] Fig. 2A shows a working example in which the [(ferrite grain) - (ferrite grain) connection
rate X] was 0.15 or less, and Fig. 2B shows a working example in which the [(ferrite
grain) - (ferrite grain) connection rate X] exceeded 0.15.
[0031] In order to obtain excellent worked-surface roughness, the [(ferrite grain) - (ferrite
grain) connection rate X] need be 0.15 or less. The [(ferrite grain) - (ferrite grain)
connection rate X] is preferably 0.13 or less, and more preferably 0.10 or less.
[0032] With the steel for use in machine-construction, according to the present invention,
the object of the invention is attained by satisfying the requirements described as
above, and there is no limitation to a ferrite area percentage (a ferrite-area fraction
of the microstructure as a whole), however, an area % on the order of 30 through 80
is preferable from the viewpoint of an increase in ductility due to an increase in
the ferrite area percentage,.an increase in tool abrasion, due to an increase in the
hardness of the steel material, caused by lowering of the ferrite area percentage,
and so forth. The area % on the order of 40 through 70 is more preferable.
[0033] The invention has been developed assuming that a steel in use is the steel for use
in machine-construction, and as for the steel grade thereof, a steel grade of a normal
chemical component composition, for use in machine-construction may be used. With
respect to elements including C, Si, Mn, P, and S, it is recommendable to adjust the
content of each of the elements so as to fall within an appropriate range. The respective
appropriate ranges of these chemical components, and reasons for setting these ranges,
from such a point of view, are described as follows.
(C: 0.2 to 1.2%)
[0034] C is an element effective for securing the strength of a steel component manufactured
from the steel for use in machine-construction. If a C-content is excessively low,
it will be difficult to adjust a steel material such that the [(ferrite grain) - (ferrite
grain) connection rate X] falls within the specified range, whereas if the C-content
is excessively high, hardness will become excessively high, thereby deteriorating
machinability (for example, a tool life). For this reason, the C-content is preferably
set to not less than 0.2% (more preferably not less than 0.25%), and 1.2% or less
(more preferably, 1.1% or less).
(Si: 0.05 to 0.5%)
[0035] Si, as a deoxidizing element, is contained in the steel for use in machine-construction,
for the purpose of increasing the strength of a steel component, due to solid solution
hardening, and if an Si content is less than 0.05%, such an advantageous effect as
described cannot be effectively exhibited, whereas if Si in excess of 0.5% is contained,
this will cause hardness to excessively rise, thereby deteriorating machinability
(for example, the tool life). Further, a more preferable lower limit of the Si content
is not less than 0.1%, while a more preferable upper limit thereof is 0.4% or less.
(Mn: 0.2 to 1.8%)
[0036] Mn is effective as a deoxidizing and desulfurizing element, in molten steel, while
being an element effective for enhancing hardenability to thereby increase the strength
of a steel component. If an Mn content is less than 0.2%, these effects cannot be
exhibited, whereas if Mn in excess of 1.8% is contained, this will cause hardness
to excessively rise, thereby deteriorating cold workability. Further, a more preferable
lower limit of the Mn content is not less than 0.3%, and a more preferable upper limit
thereof is 1.5% or less.
(P: 0.03% or less) (excluding 0%)
[0037] P is an element unavoidably contained in steel to be segregated at a ferrite grain
boundary, thereby deteriorating cold workability. Accordingly, P is preferably lowered
as much as possible, however, an attempt to cause extreme reduction in P-content will
invite an increase in steel-making cost, so that it is difficult to lower the P-content
down to 0% from a manufacturing point of view. Therefore, the P-content is preferably
set to 0.03% or less (excluding 0%). An upper limit of the P-content is more preferably
0.025% or less.
(S: 0.03% or less) (excluding 0%)
[0038] S is an element unavoidably contained in steel, as in the case of P, being a detrimental
element that exists in steel, in the form of MnS, thereby deteriorating cold workability,
so that it is necessary to reduce S as much as possible. An S content is preferably
0.03% or less from such a point of view, (more preferably 0.025% or less). However,
S being an unavoidably contained impurity, it is industrially difficult to reduce
the S-content to 0%.
[0039] The basic component composition of the steel for use in machine-construction, according
to the present invention, is as described above, and the balance is practically iron.
Further, by "practically iron" is meant unavoidable impurities (for example, Al, N,
O, H, etc.), other than P and S, besides components (for example, Sb, Zn, etc.), each
thereof being in a trace amount, permissible to the extent that the characteristics
of the steel according to the present invention is not interfered with, other than
iron, can be contained. Still further, the following selective components may be contained
as necessary in the steel for use in machine-construction, according to the invention.
In the case where these components are contained, the reasons for limiting respective
component ranges are given as follows.
[0040] (At least one species selected from the group consisting of (Cr: 0.5% or less (excluding
0%), Cu: 0.5% or less (excluding 0%), Ni: 0.5% or less (excluding 0%), and Mo: 0.5%
or less (excluding 0%))
[0041] Any element selected from the group consisting of Cr, Cu, Ni, and Mo is an element
effective in increasing the strength of a final product by causing the hardenablity
of a steel material, and if necessary, one species of these elements is singly contained
or not less than two species thereof are contained. However, if these elements each
is excessive in content, the strength will become excessively high, thereby causing
deterioration in cold workability, and therefore, the preferable upper limit described
as above was set for the respective elements. A more preferable upper limit for any
one of these elements is 0.45% or less (still more preferably, 0.40% or less). Still
further, as the content of any one of these elements increases, so does the effect
thereof, however, a preferable lower limit of the content of any one among those elements
is not less than 0.015% (more preferably, not less than 0.020%).
[0042] At the time of manufacturing the steel for use in machine-construction, according
to the present invention, a steel satisfying the component composition described as
above is subjected to hot rolling under normal conditions to be turned into a hot-rolled
steel-plate material. Subsequently, the hot-rolled steel-plate material is heated
up to a temperature in a range of 800 to 950°C, and it need only be sufficient to
cool the hot-rolled steel-plate material to 500°C or lower at an average cooling rate
of not less than 2°C/sec after holding the same at that temperature for around 10
to 25 min (holding time). Further, the manufacturing conditions may be changed halfway
through an operation provided that such a change falls within the range of the manufacturing
conditions. These manufacturing conditions are described below
(Heating temperature: 800 to 950°C)
[0043] In order to control the [(ferrite grain) - (ferrite grain) connection rate X] at
0.15 or less, it is necessary to control a heating temperature (a heating temperature
after the hot rolling) in the range of 800 to 950°C. If the heating temperature at
this point in time exceeds 950°C, the total area of an austenite grain boundary, per
unit volume, will decrease due to coarsening of an austenite grain size at the time
of heating, thereby causing ferrite grains to be precipitated from the austenite grain
boundary to approach each other, so that it will become difficult to cause the ferrite
grains to be isolated from each other. Further, if the heating temperature is less
than 800°C, the ferrite grains existing in the hot-rolled steel-plate material prior
to the heat treatment will not be fully transformed into the austenite phase, so that
it will become difficult to control the [(ferrite grain) - (ferrite grain) connection
rate X] at 0.15 or less. A more preferable lower limit of the heating temperature
is not lower than 820°C (more preferably, not lower than 850°C), and a more preferable
upper limit thereof is not higher than 930°C (more preferably, not higher than 900°C).
(Holding time in the heating temperature range: 10 to 25 min)
[0044] Holding time in the heating temperature range is a factor having an influence exerted
on the [(ferrite grain) - (ferrite grain) connection rate X]. If the holding time
at this point in time is less than 10 min, a transformation from a ferrite phase before
the heat treatment to an austenite phase will not satisfactorily proceed, resulting
in a state where the ferrite phase is left out in the microstructure. Further, if
the holding time exceeds 25 min, an austenite grain will undergo coarsening, and the
total area of the austenite grain boundary, per unit volume, decreases, so that the
ferrite grains, precipitated from the austenite grain boundary, approach each other,
thereby rendering it difficult for the respective ferrite grains to be isolated from
each other. A more preferable lower limit of the holding time is not less than 15
min, and a more preferable upper limit thereof is 20 min or less.
(Cooling until 500°C or lower at an average cooling rate of not less than 2°C after
heated holding)
[0045] If an average cooling rate until 500°C or lower (a cooling-stop temperature) is less
than 2°C/sec, this will render it impossible for the average grain size of ferrites
to be 7 µm or less. There is the need for the average cooling rate being at not less
than 2°C/sec from such a point of view, described as above. The average cooling rate
is more preferably not less than 5°C/sec, and still more preferably not less than
7°C/sec. Further, with respect to the cooling at this point in time, a cooling form
capable of varying the cooling rate may be adopted provided that variation is made
within the range where the average cooling rate is not less than 2°C/sec.
(Cooling-stop temperature: 500°C or lower)
[0046] The cooling-stop temperature is preferably 500°C or lower. If the cooling-stop temperature
is higher than 500°C, the ferrite grain size will become susceptible to coarsen, thereby
rendering it difficult for the average grain size of the ferrite grains to be at 7
µm or less. On the other hand, if the cooling-stop temperature is lower, no influence
will be exerted on the microstructure of the material. Therefore, normal cooling (standing
to cool) is applied after completion of cooling until 500°C or lower, and lowering
of temperature, down to room temperature, will suffice.
[0047] The steel for use in machine-construction, according to the invention, excellent
in machinability, is thus obtained, and a steel product with improved machined-surface
characteristics (the worked-surface roughness) can be manufactured by applying a cutting
operation to the steel for use in machine-construction. Further, since excellent machined-surface
characteristics can be obtained by applying a cutting operation to the steel for use
in machine-construction, according to the invention, the steel for use in machine-construction
as it is can be used as a forming tool without applying a finish-machining, such as
grinding, etc., thereto.
[0048] The invention is more specifically described below with reference to examples of
the invention, however, it is to be pointed out that the invention be not limited
by the examples described below and that various changes and modifications may be
obviously possible in the invention without departing from the spirit and scope thereof,
those changes and modifications being incorporated in the technical range of the invention.
Examples
[0049] A hot-rolled steel material (a steel-plate material (plate thickness: 30 mm) was
prepared by hot rolling under a normal hot-rolling condition, using each of steel
grades A through D, having respective chemical component compositions shown in Table
1 given below. In Table 1, the steel grade A is an S55C equivalent steel (JISG 4051),
the steel grade B is an S60C equivalent steel (JISG 4051), the steel grade C is an
S50C equivalent steel (JISG 4051), and the steel grade D is an S45C equivalent steel
(JISG 4051).
[Table 1]
| Steel grade |
Chemical component composition *(mass%) |
| C |
Si |
Mn |
P |
S |
| A |
0.55 |
0.26 |
0.74 |
0.010 |
0.0024 |
| B |
0.60 |
0.22 |
0.76 |
0.018 |
0.0092 |
| C |
0.50 |
0.17 |
0.78 |
0.019 |
0.013 |
| D |
0.45 |
0.18 |
0.72 |
0.014 |
0.020 |
| * Balance: iron and unavoidable impurities, other than P and S |
[0050] Respective examples were prepared under manufacturing conditions (heating temperature,
holding time, an average cooling rate after heating, and a cooling method), shown
in Table 2 below, using the hot-rolled steel material obtained as above (Test Nos.
1 through 7). A steel of the steel grade A under Test No. 1 is the test sample obtained
by heating the hot-rolled steel material of the S55C equivalent steel (the steel grade
A) up to 850°C to be held at that temperature for 20 min to be subsequently air cooled
(at an average cooling rate: 3°C/sec) without air cooling by blowing with the use
of a blower. A steel of the steel grade B under Test No. 2 is the test sample obtained
by heating the hot-rolled steel material of the S60C equivalent steel (the steel grade
B) up to 850°C to be held at that temperature for 20 min to be subsequently furnace
cooled (at an average cooling rate: 0.8°C/sec). A steel of the steel grade C under
Test No. 3 is the test sample obtained by heating the hot-rolled steel material of
the S50C equivalent steel (the steel grade C) up to 900°C to be held at that temperature
for 20 min to be subsequently air cooled (at an average cooling rate: 6°C/sec) by
blowing with the use of a blower. A steel of the steel grade A under Test No. 4 is
the test sample obtained by heating the hot-rolled steel material of the S55C equivalent
steel (the steel grade A) up to 850°C to be held at that temperature for 20 min to
be subsequently air cooled (at an average cooling rate: 6°C/sec) by blowing with the
use of a blower, being further held for 1.5 min at a point in time, when the temperature
dropped to 750°C to be thereafter air cooled (the average cooling rate: 6°C/sec),
while blowing air to the hot-rolled steel material again with the use of the blower.
A steel of the steel grade A under Test No. 5 is the test sample obtained by heating
the hot-rolled steel material of the hot-rolled steel material of the S55C equivalent
steel (the steel grade A) up to 850°C to be held at that temperature for 20 min to
be subsequently furnace cooled (at the average cooling rate: 0.8°C/sec). A steel of
the steel grade A under Test No. 6 is the test sample obtained without heating the
hot-rolled steel material of the S55C equivalent steel (the steel grade A). A steel
of the steel grade D under Test No. 7 is the test sample obtained by heating the hot-rolled
steel material of the S45C equivalent steel (the steel grade D) up to 700°C to be
held at that temperature for 30 min to be subsequently air cooled (at the average
cooling rate: 3°C/sec) without air cooling by blowing with the use of a blower. With
respect to any of the test samples, the cooling-stop temperature was set to 500°C
or lower.
[Table 2]
| Test No. |
Steel grade |
Manufacturing condition |
| Heating temperature (°C) |
Holding time (min) |
Average cooling rate (°C/sec) |
Cooling method |
| 1 |
A |
850 |
20 |
3 |
Air cooled |
| 2 |
B |
850 |
20 |
0.8 |
Furnace cooled |
| 3 |
C |
900 |
20 |
6 |
Air cooled (blowing) |
| 4 |
A |
(1)850 |
20 |
6 |
Air cooled (blowing) |
| (2)750 |
1.5 |
6 |
Air cooled (blowing) |
| 5 |
A |
850 |
20 |
0.8 |
Furnace cooled |
| 6 |
A |
- |
- |
- |
- |
| 7 |
D |
700 |
30 |
3 |
Air cooled |
[0051] With respect to each of the test samples (Test Nos. 1 through 7), as obtained, a
measurement was made on the average equivalent circle diameter of ferrites, and a
[(ferrite grain)-(ferrite grain) connection rate X], by the following method.
(Measurement on the average equivalent circle diameter of ferrites)
[0052] The test samples each were specularly polished to be subsequently corroded by use
of a 3% nital solution to thereby expose a metal microstructure, and subsequently,
a microstructure observation was made on five visual fields, in a region of approximately
170 µm x 230 µm, by use of a scanning electron microscope (SEM) up to 400x magnification,
to take a photograph of the five visual fields. Based on these photographs, a white
part was determined as a ferrite grain from a contrast in an image to be marked, whereupon
an equivalent circle diameter of a ferrite grain was found by an image analysis, thereby
having found an average value of the respective equivalent circle diameters, in the
five visual fields.
(Measurement on a [(ferrite grain)-(ferrite grain) connection rate X]
[0053] The working examples each were specularly polished to be corroded with the use of
the 3% nital solution to expose a metal microstructure, and subsequently, a microstructure
observation was made in a region of 40000 µm
2 in area, using a scanning electron microscope (SEM) up to 400x magnification, having
thereby taken a photograph of the region. Thereafter, horizontal lines were drawn
at regular intervals across a photograph of the microstructure such that the total
length (lengths in total) of horizontal line-segments is not less than 1000 µm, having
thereby found a [(ferrite grain)-(ferrite grain) connection rate X] according to the
procedure described in the foregoing.
[0054] Still further, with respect to the respective test samples, a cutting test was conducted
under conditions shown in Table 3 depicted below, having thereby assessed the machined
cut-surface roughness of each of the test samples, after the cutting operation. In
this case, a cutting test was conducted by means of two-dimensional cutting (planing),
using a machining center. The machined cut-surface roughness, serving as a criterion
for decision on machinability, was measured by moving a stylus in a direction parallel
with the cutting direction, with the use of a contact-needle roughness meter. As to
the criterion for decision on machinability, if the machined cut-surface roughness
was less than 0.10 µm, in terms of calculated average roughness Ra, the surface characteristic
was assessed as excellent. In this connection, two-dimensional cutting was adopted
in the cutting test although a more-complex three-dimensional cutting was expected
in the case of a normal cutting. However, since the three-dimensional cutting can
be regarded as the case of integration of two-dimensional cuttings, the effect of
the three-dimensional cutting can be estimated on the basis of data obtained from
the two-dimensional cutting.
[Table 3]
| Processing style |
Two-dimensional cutting (planing) |
| Tool in use |
Protrusion-cutting process tool, Tool width: 6 mm, Face angle: 10°, P-grade cemented
carbide tip (non coat) without tip-breaker |
| Cutting depth |
5 µm |
| Cutting rate |
1 m / min |
| Cutting type |
Wet cutting (water-soluble cutting oil) |
| Cutting direction |
Direction perpendicular to the rolling direction (L direction) |
[0055] These results, as summarized, are shown in Table 4 depicted below.
[Table 4]
| Test No. |
Steel grade |
(Ferrite grain) - (Ferrite grain) connection rate X (-) |
Ferrite average equivalent circle diameter (µm) |
Machined cut-surface roughness (Ra) (µm) |
| 1 |
A |
0.09 |
5.6 |
0.03 |
| 2 |
B |
0.10 |
9.7 |
0.12 |
| 3 |
C |
0.12 |
5.1 |
0.05 |
| 4 |
A |
0.12 |
6.6 |
0.08 |
| 5 |
A |
0.13 |
8.3 |
0.11 |
| 6 |
A |
0.18 |
6.9 |
0.12 |
| 7 |
D |
0.26 |
4.9 |
0.14 |
[0056] On the basis of the result, described as above, observation can be made as follows.
It is evident that the example, as the object of each of Test Nos. 1, 3, and 4, is
an example satisfying all the requirements of the [(ferrite grain)-(ferrite grain)
connection rate X] and the average equivalent circle diameter of ferrite, specified
by the present invention, and the machined cut-surface roughness (Ra) thereof indicates
an excellent value. Further, it is evident that the example as the object of Test
No. 1, in particular, is an example in which the heating temperature and the holding
time are at a more preferable value, respectively, and the [(ferrite grain)-(ferrite
grain) connection rate X] as well is at a more preferable value, thus having the most
superior surface characteristics.
[0057] In contrast, the example as the object of each of Test Nos. 2, and 5 through 7 is
an example failing to satisfy any of the requirements specified by the present invention.
With any of those examples, the machined cut-surface roughness was found large in
value. More specifically, the examples under Test No.2, and Test No. 5, respectively,
represent an example in which the average cooling rate was at 0.8°C/sec, and the average
equivalent circle diameter of ferrites was found large, and the machined cut-surface
roughness (Ra) as well was found large.
[0058] The working example as the object of Test No. 6 is an example in which the heat treatment
was not applied after the hot rolling, the [(ferrite grain)-(ferrite grain) connection
rate X] of the ferrite grain was found large, and the machined cut-surface roughness
(Ra) as well was found large. The example as the object of Test No. 7 is an example
in which the heating temperature was low, the [(ferrite grain)-(ferrite grain) connection
rate X] of the ferrite grain was found large, and the machined cut-surface roughness
(Ra) as well was found large.
[0059] Although the present invention has been described in detail, while referring to specific
embodiments, it is believed obvious to those skilled in the art that variation and
modification may be made in the invention without departing from the spirit and scope
thereof.
Industrial Applicability
[0061] The steel for use in machine-construction, according to the invention, is useful
for various parts for use in machine-construction, including an automotive part and
a construction machinery part, etc., and this steel for use in machine-construction
is also suitable for application to a forming tool, in particular, because of excellent
machinability.
List of Reference Signs
[0062]
- 1: ferrite phase
- 2: hard phase
- 3: recess