[0001] The present application relates to heat treatment of high pressure die cast objects,
and more particularly to the solution heat treatment of high pressure die cast objects
with pressure. In particular, the present invention relates to a method of heat treating
a high pressure die cast aluminum alloy object with the features of the introductory
part of claim 1 or of claim 8.
[0002] High pressure die casting is a low cost, dimensionally accurate casting process for
high volume production of many cast objects, including, but not limited to marine
propellers, marine and automotive engine components, vehicle chassis, vehicle closures,
vehicle structural bodies, and advanced vehicle bodies. Approximately 70% of all cast
aluminum is cast using the high pressure die casting process, primarily using aluminum
alloys. In high volume, the high pressure die casting process delivers castings on
a cost per pound basis that are lower cost at higher dimensional accuracy than alternative
methods such as permanent mold casting or sand casting.
[0003] The disadvantage of the high pressure die casting process is that it results in cast
objects having comparatively lower strength than permanent mold or sand casting. This
lower strength is due to the fact that the high pressure die casting process moves
metal in a violent, turbulent fashion, entrapping air in the molten metal during the
casting process. This entrapped air becomes problematic because, in order to increase
the strength of a high pressure aluminum die cast object, it is preferable to heat
treat the cast object after casting. A typical heat treatment to strengthen aluminum
alloys is solution heat treatment and artificial aging to achieve the T6 treatment
condition. However, heat treatments above 700°F are not used for increasing the strength
and ductility of high pressure die cast objects because often the air entrained or
entrapped in the castings expands during the solution heat treatment at temperatures
above 700°F, creating blisters on and in the cast product. The blisters cause aesthetic
issues with surface finish and create large pores that reduce the mechanical properties
of the casting. Therefore, conventional high pressure die castings are used in the
"as cast" condition. For many low copper content alloys like Aluminum Association
alloys 367, 360, or 361 the associated yield strength is about 17 KSI, in the "as
cast" condition.
[0004] In traditional solution heat treatment, the cast object is placed in an air furnace,
fused salt bath, or fluidized sand bed and manipulated with heat to develop a wide
range of mechanical properties and achieve a combination of properties unattainable
by other means. The high pressure die cast object is heated to a specific temperature
to create a super-saturated solution of alloy elements, and the object is then soaked
at that temperature for a given time. Subsequently, the die cast object is rapidly
quenched and artificially aged at a lower temperature for a given period of time.
[0005] During the solution heat treatment portion of the T6 heat treating process, cast
objects may be subjected to temperatures up to 1000° for up to 12 hours. At 1000°F
a permanent mold or sand cast aluminum alloy cast object will dissolve any magnesium
present into solid solution for the given alloy, and will thermally modify the eutectic
silicon providing mechanical advantages. Again however, when high pressure die cast
objects are subjected to T6 heat treatment conditions, any entrained gas in the casting
will volumetrically expand at the increased temperature, increasing the pressure within
the pore or defect. This increase in pressure and the result of low mechanical properties
of the metal at that elevated temperature creates a situation where the metal plastically
deforms leaving a blister defect either internally or at the surface that creates
aesthetic and mechanical problems. Prior to the present application, blister defects
were prevented by heat treating high pressure die cast objects at very short solution
times (e.g. 15 minutes). This short solution time fails to allow for sufficient modification
of the eutectic and does not create the mechanical advantages that a longer (e.g.
2-12 hour) treatment creates.
[0006] It remains highly desirable to conduct heat treatment of high pressure die cast objects
because the heat treatment generally doubles the yield strength. For example, a T6
heat treatment of an aluminum alloy high pressure die cast object will increase from
17 KSI in the "as cast" condition to approximately 35 KSI in the T6 heat treated condition,
if no blistering defects arise to impair the mechanical properties. Moreover, this
dramatic increase in strength will allow a design engineer to redesign a part that
typically achieves a 30% reduction in the weight of the part when considering multiple
modes of loading and part geometries.
[0007] It is known in the art to apply pressure to objects cast using the sand casting or
permanent mold casting processes through hot isostatic pressing or HIP. The HIP process
involves healing of shrinkage porosity and subsequent improvements in tensile and
fatigue properties for sand cast or permanent mold cast aluminum castings. Internal
shrinkage porosity results from solidification shrinkage of the alloy and processing
variables such as the geometric effects of the mold, or the effects of casting parameters
including metal temperature, mold temperature, cooling rate, and pour rate. The HIP
procedure involves the use of uniform gas pressure applied at elevated temperatures
and subsequent slow cooling to room temperature. The parts are commonly solution heat
treated after cooling to room temperature. In the case of aluminum alloys, pressures
above 15 KSI and temperatures around 980°F can be used. The applied pressure causes
plastic flow in the material and the resulted healing of shrinkage porosities, however,
in the HIP process, it is well known that pressures of 10 KSI or less are inadequate
for full densification of the material within the time and temperature of limitations
for the HIP process. Accordingly, a pressure of 15 KSI or greater is generally required
to realize the advantages of the HIP process.
[0008] There are several problems with using the hot isostatic pressing process with high
pressure die cast objects. First, the high pressure die casting process requires high
pressures, above 15 KSI, and large, expensive pressure vessels to attain that pressure.
More significantly, the hot isostatic pressing process is incapable of fixing blistering
defects resulting from the high pressure die casting process. In other words, the
extensive amount of entrapped air in high pressure die cast aluminum alloy castings
cannot be fixed by the hot isostatic pressing process. This well-known lack of effectiveness
of HIP processing on high pressure die castings was verified by the inventors in an
experiment where a high pressure die cast propeller was subjected to 15 KSI pressure
at 1000°F for 4 hours of hot isostatic pressing and allowed to cool to room temperature.
The same propeller was then heat treated at 1000F for 4 hours at atmospheric conditions.
Blistering defects were still evident after the process showing that the internal
defects in the casting were not healed by the HIP process as shown in Figs. 9A and
9B.
[0009] Thus, it is known that the hot isostatic pressing (HIP) process is incapable of curing
blistering defects from subsequent solution heat treatment of cast objects, particularly
aluminum alloy cast objects. So it is the object of the present invention to provide
a method of heat treating a high pressure die cast aluminum alloy object that avoids
or at least reduces blistering effects.
[0010] The above-mentioned object is met with a method comprising the features of claim
1. Preferred improvements and modifications of the method according to claim 1 are
the subject matter of dependent claims 2 to 7.
[0011] The above-mentioned object is also met with a method comprising the features of claim
8. Preferred improvements and modifications on the method according to claim 8 are
the subject matter of dependent claims 9 to 14.
[0012] In accordance with the present application, it has been surprisingly found that the
application of pressure during the solution heat treatment process, at pressures below
conventional hot isostatic pressing (HIP) pressures, results in a beneficial pressure
equilibrium within an "as cast" high pressure die cast object where air entrained
in the casting due to the high pressure die casting process cannot expand and form
blistering defects. Accordingly, the present application discloses an application
of external pressure during solution heat treatment of a high pressure die cast object
to inhibit the problematic blistering defects that occur during a traditional heat
treatment of a high pressure die cast object. The present application discloses a
method of heat treating a high pressure die cast object. The method includes obtaining
a high pressure die cast object, and solution heat treating the high pressure die
cast object above 700°F for 0.5 to 12 hours at a pressure between 0.5 and 35 KSI.
Subsequently, the cast object may be quenched and artificially aged to create a high
pressure die cast object without blistering defects. The pressure applied during the
solution heat treatment step of one embodiment is between 0.5 and 15 KSI or at any
pressure or range of pressures therebetween. Another embodiment of the external pressure
applied during the solution heat treatment step is between 2.5 and 10 KSI or at any
pressure or range of pressures therebetween; while in another embodiment the pressure
applied is between 2.5 and 5 KSI or at any pressure or range of pressures therebetween.
The use of external pressure above 2.5 KSI creates a pressure balance during the heat
treatment of the high pressure die cast object such that air cannot expand to cause
the problematic blistering on the final heat treated object. The use of external pressure
between 0.5 and 3.5 KSI is sufficient to reduce and/or eliminate blistering defects.
[0013] In one embodiment, the step of solution heat treating comprises a T6 heat treatment
with the application of pressure between 0.5 and 15 KSI, 0.5 and 10 KSI or 2.5 to
5 KSI, or at any pressure or range of pressures between 0.5 and 15 KSI. In another
embodiment, the solution heat treatment temperature is between 700°F and 1200°F, or
at any temperature or range of temperatures therebetween. In another embodiment, the
temperature is between 800°F and 1000°F, or at any temperature or range of temperatures
therebetween. In another embodiment, the solution heat treatment temperature is at
1000°F. In one embodiment, the solution heat treatment step is 0.5 to 12 hours; in
another embodiment, the time is 2 to 8 hours; while in yet another embodiment, the
solution heat treatment time with pressure is 4 to 6 hours. It will be recognized
that such ranges are exemplary, and the range of time may be at any time within the
ranges noted.
[0014] The method of heat treating may further include the step of quenching the cast object.
The method of heat treating may also include a step of artificially aging the cast
object. The step of quenching will typically occur immediately after the cast object
is removed from the solution heat treatment pressure vessel. Allowing the cast object
to slowly cool to room temperature without cooling is not desirable since the beneficial
effects to the microstructure from solution heat treatment may be lost.
[0015] The present application also contemplates a method of heat treating a high pressure
die cast aluminum alloy object. This method includes casting an aluminum alloy object
with high pressure die cast equipment and removing the cast aluminum alloy object
from the high pressure die casting equipment. The cast aluminum alloy object is then
placed into a pressure vessel, the pressure vessel including a heating element. The
cast aluminum alloy object is solution heat treated above 700°F while applying pressure
between 0.5 and 35 KSI or 0.5 to 12 hours. The solution heat treated cast object is
removed from the pressure vessel. In this method, the step of solution heat treating
reduces blistering defects on the final cast of aluminum alloy object.
[0016] In a further embodiment, the step of solution heat treating comprises a T6 heat treatment
while applying pressure between 0.5 and 15 KSI or at any pressure or range of pressures
therebetween. In another embodiment, the step of solution heat treating comprises
solution heat treating the cast aluminum alloy object between 700°F and 1200°F or
at any temperature or range of temperatures therebetween. In yet another embodiment,
the step of solution heat treating comprises solution heat treating the cast aluminum
alloy object at 1000°F. In still another embodiment, the step of solution heat treating
comprises applying pressure between 0.5 and 15 KSI, or at any pressure or range of
pressures therebetween. In another embodiment, the step of solution heat treating
comprises applying pressure between 2.5 and 10 KSI or at any pressure or range of
pressures therebetween, wherein the step of solution heat treating eliminates blistering
defects on the final cast aluminum alloy object. In yet another embodiment, the step
of solution heat treating comprises applying pressure between 2.5 and 5 KSI or at
any pressure or range of pressures therebetween, and wherein the step of solution
heat treating eliminates blistering defects on the final cast aluminum alloy object.
[0017] The step of solution heat treating may comprise solution heat treating the cast aluminum
alloy object for 2-8 hours or for any time or range of times therebetween, including,
but not limited to 4-6 hours, and at 4 hours. The method of the present application
further contemplates an embodiment where a method of heat treating further comprises
the steps of quenching the cast aluminum alloy object and artificially aging the cast
aluminum alloy object.
[0018] By employing the solution heat treatment and pressure method of the present application,
it is contemplated that the yield strength of cast objects may increase by 50% to
100%. This translates into a 15-30% weight reduction on average for structural components.
This weight reduction has substantial economic and societal value in terms of energy
and CO2 footprint reduction in automotive and other transportation applications where
increasing fuel economy is paramount.
[0019] Further details for the present invention can be obtained from the following description
of preferred and non-limiting embodiments of the invention with reference to the drawings.
In the drawings:
- Fig. 1
- is a perspective view of an exemplary pressure chamber used for the disclosed method
of solution heat treating with pressure processing of the present application.
- Fig. 2
- is a photograph demonstrating blister defects on a solution heat treated high pressure
die cast aluminum alloy propeller blade subjected to solution heat treatment at 1000°F
with no pressure applied.
- Figs. 3a-3c
- are photographs of a solution heat treated high pressure die cast aluminum alloy propeller
blade demonstrating reduction of blistering defects when 0.5 KSI (500 psi) of pressure
is applied during solution heat treatment.
- Figs. 4a-4c
- are photographs of a solution heat treated high pressure die cast aluminum alloy propeller
blade demonstrating reduction of blistering defects when 2.0 KSI (2000 psi) of pressure
is applied during solution heat treatment.
- Figs. 5a - 5b
- are photographs of a solution heat treated high pressure die cast aluminum alloy propeller
blade demonstrating elimination of blistering defects when 3.5 KSI (3500 psi) of pressure
is applied during solution heat treatment.
- Figs. 6a - 6b
- are photographs demonstrating a solution heat treated high pressure die cast aluminum
alloy propeller blade where blistering defects are eliminated through the application
of 5.0 KSI (5000 psi) of pressure during solution heat treatment.
- Figs. 7a - 7b
- are photographs of a solution heat treated high pressure die cast aluminum alloy propeller
blade demonstrating elimination of blistering defects when 10.0 KSI (10,000 psi) of
pressure is applied during solution heat treatment.
- Figs. 8a - 8b
- are photographs of a solution heat treated high pressure die cast aluminum alloy propeller
blade demonstrating elimination of blistering defects when 15.0 KSI (15,000 psi) of
pressure is applied during solution heat treatment.
- Figs. 9a - 9b
- are photographs of a high pressure die cast aluminum alloy propeller blade treated
by hot isostatic processing (HIP) and subsequently solution heat treated with no pressure.
- Figs. 10a - 10
- are photographs of a high pressure die-cast aluminum alloy propeller blade treated
with 2.3 KSI of pressure during solution heat treatment.
[0020] The present application relates to a method of reducing and/or eliminating blistering
defects in high pressure die cast metal objects that typically occur during the solution
heat treatment of high pressure die cast objects. The present application contemplates
that applying between 0.5 and 35 KSI (500 psi-35,000 psi) will reduce and/or eliminate
blistering defects, and application of pressure between 2.5 and 35 KSI, or at any
pressure or range of pressures therebetween, will eliminate blistering defects. In
one embodiment, the application pressure is lower than the pressure applied during
hot isostatic pressing, and therefore is at or below 15 KSI. In another embodiment,
pressure applied that is between 2.5 and 10 KSI. In another embodiment, the pressure
applied is 5 KSI. The application of pressure creates a balance with any air that
may be entrained or entrapped in the high pressure die cast object due to the turbulent
nature of the high pressure die casting process. By the application of pressure, any
air entrained or entrapped in the casting cannot expand, and therefore blisters are
reduced and/or eliminated. Accordingly, the increasing internal pressure of entrained
air during solution heat treatment is offset as the casting is heated to elevated
temperatures with external pressure. If the external pressure and the inherent strength
of the material at elevated temperatures is greater than the internal pressure of
the entrapped air, blistering will not occur.
[0021] The present application contemplates a method of heat treating a high pressure die
cast object. In one embodiment, the high pressure die cast object is an aluminum alloy
high pressure die cast object, however, the present application may be used for heat
treating any high pressured die cast metal object wherein air becomes entrained during
the turbulent high pressure die casting process. The method contemplates first obtaining
a high pressure die cast object 2. In the embodiment shown in the Figs. 2-8, the high
pressure die cast object 2 is a marine propeller, however the present application
is applicable for any high pressure die cast object that may be formed using the high
pressure die casting method, including but not limited to, vehicle chassis, vehicle
closures, structural bodies, and advanced vehicle bodies.
[0022] Referring now to Fig. 1, once the high pressure die cast object is obtained, the
object is subjected to solution heat treatment with pressure. A pressure vessel 4
having an end closure 6, heating means such as heating elements 8 and workload support
10 may be used for the step of solution heat treating with pressure. However, the
pressure vessel 4 may be any certified pressure vessel capable of applying pressure
up to 35 KSI and heat up to 1200°F. In one embodiment, a certified pressure vessel
capable of applying pressure up to 15 KSI is acceptable, while in other embodiments,
certified vessels that have a maximum pressure of 10 KSI or 5 KSI are acceptable.
Acceptable pressure vessels for solution heat treatment with pressure in accordance
with the present application may be obtained from American Isostatic Presses, Inc.
of Columbus, Ohio. The pressure vessel 4 may further include insulation 12 to efficiently
solution heat treat the high pressure die cast object 2 at the requisite temperatures
and pressures. Additionally, a thermocouple feed through 14 and power feed through
16 may be present to provide for the measurement of heat and pressure. The pressure
vessel 4 is connected to a compressor (not shown) to create the necessary pressure
during the solution heat treatment process.
[0023] The high pressure die cast object 2 is placed within the pressure vessel 4, and the
pressure vessel 4 is sealed with end closure 6. The cast object is then solution heat
treated to above 700°F at a pressure between 0.5 and 35 KSI for 0.5 to 12 hours. In
one embodiment, the temperature is between 700 and 1200°F or at any temperature or
range of temperatures therebetween. In another embodiment, the temperature is between
800 and 1000°F, in yet another embodiment, the temperature is at 1000°F. Similarly,
the pressure may vary, with one embodiment applying pressure between 0.5 and 15 KSI
or at any pressure or range of pressures therebetween, another embodiment applying
pressure between 2.5 and 10 KSI, another embodiment applying pressure between 2.5
and 5 KSI, and an embodiment where pressure is applied at 5 KSI. In one embodiment,
the time and temperature comprises a T6 heat treatment at a pressure between 0.5 and
15 KSI. In yet another embodiment, the high pressure die cast object is solution heat
treated at 1000°F for 4 hours at 5 KSI to achieve a high pressure die cast object
devoid of blistering defects.
[0024] The gas used to apply pressure through the compressor may be atmospheric gas, an
inert gas, or any other gas sufficient to apply the required pressures during solution
heat treatment without combusting. In one embodiment, the gas is an inert gas. In
another embodiment, the gas used is argon. Once the high pressure die cast is solution
heat treated for the desired time, the die cast object is quenched and may optionally
be artificially aged. Quenching contemplates rapidly cooling the solution heat treated
object directly after removal from the solution heat treatment pressure vessel, and
not allowing the object to slowly cool to room temperature. In one embodiment, the
cast object is artificially aged for at least 2 hours. However, the length of time
and the temperature for artificial aging is generally dictated by the strength and
ductility levels desired, as is well-known by those of ordinary skill in the art.
[0025] The solution heat treatment with pressure provides for the ability to increase the
yield strength of high pressure die cast objects. For example, and without limitation,
the typical mechanical properties of high pressure die cast alloy A360.0 in the as
cast condition for temperatures up to 700°F are demonstrated in Table 1, below.
TABLE 1
[0026]
Table 1 Typical tensile properties for separately cast test bars of alloys 360.0-F
and A360.0-F at elevated temperature
Temperature |
Tensile strength |
Yield strength(s) |
Elongation(b) |
°C |
F° |
MPa |
ksi |
MPa |
ksi |
% |
360.0 aluminum |
24 |
75 |
325 |
47 |
170 |
25 |
3 |
100 |
212 |
305 |
44 |
170 |
25 |
2 |
150 |
300 |
240 |
35 |
165 |
24 |
4 |
205 |
400 |
150 |
22 |
95 |
14 |
8 |
250 |
500 |
85 |
12 |
50 |
7.5 |
20 |
315 |
600 |
50 |
7 |
30 |
4.5 |
35 |
370 |
700 |
30 |
4.5 |
20 |
3 |
40 |
A360.0 aluminum |
24 |
75 |
315 |
46 |
165 |
24 |
5 |
100 |
212 |
295 |
43 |
165 |
24 |
3 |
150 |
300 |
235 |
34 |
160 |
23 |
5 |
205 |
400 |
145 |
21 |
90 |
13 |
14 |
250 |
500 |
75 |
11 |
45 |
6.5 |
30 |
315 |
600 |
45 |
6.5 |
28 |
4 |
45 |
370 |
700 |
30 |
4 |
15 |
2.5 |
45 |
(a) 0.2% offset, (b) In 50 mm or 2 in. |
[0027] According to Table 1, at higher temperatures required for solution heat treatment,
i.e. above 700°F, the tensile strength will be less than 4 KSI and the yield strength
will be less than 2.5 KSI. Thus, at solution heat treatment temperatures, when the
yield strength of the die casting alloy is less than the pressure in the entrapped
air, the air will expand, creating blistering defects 20, as shown in Fig. 2. As shown
in Figs. 5-8, 10a and 10b, by applying an external gas pressure above 2.5 KSI to the
cast object, the internal trapped gas cannot expand, and therefore the blistering
of the high pressure die cast object can be eliminated. Even at lower pressures from
0.5 to 3.5 KSI, blistering defects can be reduced as shown in Figs. 3, 4, 10a and
10b. Since the blistering defects may be eliminated while obtaining the advantages
of the solution heat treatment process, the yield strength of the solution heat treated
high pressure die cast objects may increase by 50% to 100%. This translates into a
15-30% weight reduction on average for a redesigned component or a substantially higher
safety factor on the same geometry component. It is known in the art that a 10% increase
in yield strength of an aluminum casting can facilitate a designed weight reduction
of 3% on average for the cast object. This is highly important, particularly in vehicle
design (whether automobiles, trucks, or marine vehicles, because even a 10% total
vehicle weight reduction improves mileage by 5-7%. Accordingly, the present invention
provides a significant advance as weight reductions of 15-30% may be obtained.
EXAMPLES
EXAMPLE 1
[0028] High pressure die cast aluminum alloy marine propellers were selected as a test sample.
Fig. 2 demonstrates a high pressure die cast aluminum alloy marine propeller treated
at the T6 heat treatment of 1000°F for 4 hours with 0 KSI pressure applied. Numerous
blistering defects 20 are demonstrated.
[0029] Subsequently, high pressure die cast aluminum alloy marine propellers were subjected
to solution heat treatment with pressure. Eighteen (18) high pressure die cast aluminum
alloy propellers were solution heat treated with an externally applied gas pressure
of 15 KSI, 10 KSI and 5 KSI, respectfully (i.e. six (6) samples at each pressure).
Each solution heat treatment was at 1000°F for 4 hours. The externally applied gas
pressure was accomplished through placing the high pressure die cast aluminum alloy
marine propellers in a pressure vessel 4, and the pressure was applied using argon.
The results are shown in Figs. 6, 7 and 8, wherein an elimination of blister defects
20 was observed.
EXAMPLE 2
[0030] High pressure die cast aluminum alloy marine propellers were subjected to solution
heat treatment with pressure. Three (3) high pressure die cast aluminum alloy marine
propellers were each solution heat treated at 3.5 KSI, 2.0 KSI, and 0.5 KSI at 1000°F
for 4 hours. The three propellers solution heat treated at 3.5 KSI demonstrated an
elimination of blistering defects as shown in Fig. 5. The three high pressure die
cast aluminum alloy marine propellers solution heat treated at 0.5 KSI demonstrated
a reduction of blistering defects as shown in Fig. 3. The three high pressure die
cast aluminum alloy marine propellers solution heat treated at 2.0 KSI demonstrated
a significant reduction of blistering, with one small blister on only 1 of 3 propeller
blades, as shown in Fig. 4.
[0031] Accordingly, the experiments confirm solution heat treatment with pressures between
0.5 and 35.0 KSI result in reduction of blister defects on high pressure die cast
aluminum marine propellers, and pressures between 3.5 and 15.0 KSI demonstrate an
elimination of blistering defects in high pressure die cast aluminum alloy marine
propellers.
EXAMPLE 3
[0032] The lack of effectiveness of HIP processing on high pressure die castings was verified
by the inventors in an experiment where a high pressure die cast propeller was subjected
to 15 KSI pressure at 1000°F for 4 hours of hot isostatic pressing and allowed to
cool to room temperature. The same propeller was then heat treated at 1000F for 4
hours at atmospheric conditions. Blistering defects were still evident after the process
showing that the internal defects in the casting were not healed by the HIP process
as shown in Figs. 9A and 9B.
EXAMPLE 4
[0033] In an effort to more accurately define the lowest pressure at which blistering will
not occur, two (2) high pressure die cast aluminum alloy marine propellers each having
three (3) blades were each solution heat treated at 2.5 and 2.3 ksi at 1000F for 4
hours. The 3-blade propeller solution heat treated at 2.5 ksi demonstrated a total
elimination of blistering defects. In contrast, the 3-blade high pressure die cast
aluminum alloy marine propeller solution heat treated at 2.3 ksi also demonstrated
a significant reduction in blistering, bit did demonstrated one small blister at the
root of one of the propeller blades. The diameter of this blister is approximately
1mm in diameter, as shown in Figure 10a. The propeller was subjected to a drop weight
impact test to ascertain whether the blister reduced the mechanical ductility of the
propeller blade. As shown in Figure 2, the propeller processed at 2.3 ksi after a
drop weight impact test showing the very small blister did not substantially reduce
ductility or result in fracture of the blade. However, because one (1) very small
blister was detected on one (1) blade at 2.3 ksi, the lower pressure limit where the
invention can be expected to be reliably practiced without any blistering is 2.5 ksi.
[0034] The highest pressure limit where both blistering will not occur and the invention
has utility is not defined by the blistering mechanism itself. Pressures equal to
2.5 ksi and up to 35 ksi have been demonstrated to eliminate blistering. Instead,
the upper limit of pressure where the invention has practical utility is defined by
the increasing equipment cost of the pressure vessel and increasing process cycle
time that adds to the final product cost. As pressure increases, both the capital
cost of the pressure vessel itself increases and the process cycle time and associated
cost increases on a non-linear basis. When these capital and process cycle time costs
become excessive, it is not financially advantageous to use high pressure diecast
articles and the inventive processing method. Instead, other metalworking or casting
processes, such as but not limited to forging a wrought blank and machining or ablation
casting become more financially preferred. The upper pressure limit of 15 ksi is defined
by the capital equipment and process costs of today's modern pressure vessel technology.
[0035] In the above description, certain terms have been used for brevity, clearness and
understanding. No unnecessary limitations are to be implied therefrom beyond the requirement
of the prior art because such terms are used for descriptive purposes only and are
intended to be broadly construed. The different systems and methods described herein
may be used alone or in combination with other systems and methods. Various alternatives
and modifications are possible within the scope of the appended claims. While each
of the method claims includes a specific series of steps for accomplishing the claimed
method, the scope of this disclosure is not intended to be bound by the literal order
or literal content of steps described herein, and not substantial differences or changes
still fall within the scope of the disclosure.
1. A method of heat treating a high pressure die cast aluminum alloy object, the method
comprising: obtaining a high pressure die cast aluminum alloy object, solution heat
treating the high pressure die cast aluminum alloy object, and quenching the high
pressure die cast aluminum alloy object after said solution heat treating, characterized in that
the solution heat treating is effected in a solution heat treatment vessel at a temperature
above 700°F while applying pressure between 2.5 and 10 KSI for 2 to 8 hours, so that
the step of solution heat treating eliminates blistering defects on the high pressure
die cast object, and
quenching is effected after removing the die cast object from the solution heat treatment
vessel.
2. The method of claim 1, characterized in that
the step of solution heat treating comprises applying pressure between 2.5 and 5 KSI.
3. The method of claim 2, characterized in that
the method further comprises subsequently quenching the die cast object and artificially
aging the die cast object to effect a T6 heat treatment.
4. The method according to any one of the preceding claims, characterized in that
the step of solution heat treating comprises solution heat treating the die cast object
between 700°F and 1200°F.
5. The method of claim 4, characterized in that
the step of solution heat treating comprises solution heat treating the die cast object
at 1000°F.
6. The method according to any one of the preceding claims, characterized in that
the step of solution heat treating comprises solution heat treating the die cast object
for 4 to 6 hours.
7. The method according to any one of the preceding claims, characterized in that
the method of heat treating further comprises the step of artificially aging the die
cast object.
8. A method of heat treating a high pressure die cast aluminum alloy object, the method
comprising: casting an aluminum alloy object with high pressure die casting equipment,
removing the die cast aluminum alloy object from the high pressure die casting equipment,
solution heat treating the die cast aluminum alloy object, and quenching the die cast
aluminum alloy object,
characterized in that
after removing the die cast aluminum alloy object from the high pressure die casting
equipment said object is placed into a pressure vessel, said pressure vessel including
a heating element,
the die cast aluminum alloy object is solution heat treated in said pressure vessel
at a temperature of above 700°F while applying pressure between 2.5 and 10 KSI for
2 to 8 hours,
after said solution heat treating the die cast aluminum alloy object is removed from
the pressure vessel and after this removal from the pressure vessel the quenching
of the die cast aluminum alloy object is done,
wherein the step of solution heat treating reduces blistering defects on the die cast
aluminum alloy object.
9. The method of claim 8, characterized in that
the step of solution heat treating comprises applying pressure between 2.5 and 5 KSI.
10. The method of claim 9, characterized in that
the method further comprises subsequently quenching the die cast aluminum alloy object
and artificially aging the cast object to effect a T6 heat treatment.
11. The method according to any one of the preceding claims, characterized in that
the step of solution heat treating comprises solution heat treating the die cast aluminum
alloy object between 700°F and 1200°F.
12. The method according to claim 11, characterized in that
the step of solution heat treating comprises solution heat treating the die cast aluminum
alloy object at 1000°F.
13. The method according to any one of the preceding claims, characterized in that
the step of solution heat treating comprises solution heat treating the die cast aluminum
alloy object for 4 to 6 hours.
14. The method according to any one of the preceding claims, characterized in that
the method of heat treating further comprises the step of artificially aging the die
cast aluminum alloy object.