Technical Field
[0001] The present invention relates to a low-strength steel sheet for hot stamping, a hot
stamped member obtained using a low-strength steel sheet for hot stamping, and a method
for manufacturing the hot stamped member, especially to a low-strength steel sheet
for hot stamping having excellent safety at the time of collision and a high yield
ratio YR represented by a ratio (YS/TS) of yield stress YS to tensile strength TS
in a region where the tensile strength TS after a heat treatment is 500 to 800 MPa,
a hot stamped member obtained using such a low-strength steel sheet for hot stamping,
and a method for manufacturing the hot stamped member.
Background Art
[0002] From the viewpoint of reducing the weight of motor vehicles and securing safety at
the time of collision (hereinafter referred to as "collision safety"), steel sheets
having a high strength and a high yield ratio YR are required. Because of the deterioration
in cold press moldability due to the increased strength of steel sheets, a hot stamping
technology has been proposed in which a steel sheet is press-molded in a heated state
to achieve both moldability and high strength at the same time.
[0003] Hot stamped members manufactured by such a technology mainly have a tensile strength
TS of 1.5 GPa class or higher. However, in recent years, various hot stamped members
having a tensile strength TS of 1.5 GPa or less have been proposed, such as steel
members having a tensile strength TS of 500 MPa or more as presented in Patent Literature
1, high-strength members having a tensile strength TS of 600 to 1000 MPa class as
presented in Patent Literature 2, and steel members having a tensile strength TS of
700 to 1300 MPa class as presented in Patent Literature 3.
[0004] In all of the hot stamped members proposed so far, it is attempted to control the
microstructure by the hot stamping process and the tensile strength TS is controlled.
For these reasons, it is the actual situation that the tensile strength TS of hot
stamped members is greatly dependent on the hot stamping process. It is conceivable
to control the tensile strength TS of the steel sheet so as to increase by addition
of alloying elements so that the tensile strength TS is not dependent on the hot stamping
process.
[0005] In most of the technologies proposed so far, it is usually attempted to increase
the strength by containing a hard microstructure such as martensite. However, it is
impossible to increase the yield ratio YR by increasing the strength through such
microstructure control, and a heat treatment such as tempering is required in order
to increase the yield stress YS from the viewpoint of improving collision safety.
[0006] The present invention was made in view of circumstances as described above, and an
object thereof is to provide a low-strength steel sheet for hot stamping, from which
a hot stamped member having a yield ratio YR of 70% or more and a tensile strength
TS of 500 to 800 MPa can be manufactured without largely depending on the hot stamping
process, a hot stamped member obtained using such a low-strength steel sheet for hot
stamping, and a method for manufacturing the hot stamped member.
Citation List
Patent Literature
Summary of Invention
[0008] The present inventors diligently conducted studies from the viewpoint of realizing
a low-strength steel sheet for hot stamping, from which a hot stamped member can be
manufactured without largely depending on the hot stamping process. As a result, it
was found that the austenite fraction is lowered during a heat treatment such as hot
stamping and the following actions (1) and (2) are exerted when the Ac
3 point (°C) of a steel sheet is increased by appropriately adjusting the chemical
composition, the contents of elements that improve the hardenability are decreased,
and the steel sheet has a microstructure mainly composed of ferrite, and the present
invention was completed by further conducting studies based on such findings.
- (1) Obtaining a predetermined strength without largely depending on the hot stamping
process by diminishing the microstructural changes during the hot stamping process
as much as possible, and
- (2) Being able to improve the yield ratio YR by making it difficult for a martensite
structure to be generated in the microstructure after a heat treatment.
[0009] Namely, an aspect of the present invention is a low-strength steel sheet for hot
stamping, the steel sheet containing, in % by mass:
C: 0.005% to 0.12%,
Si: 0.50% to 2.0%,
Mn: 0.50% or less (not including 0%),
Al: 0.010% to 1.0%,
P: 0.1000% or less (not including 0%),
S: 0.0100% or less (not including 0%),
N: 0.0100% or less (not including 0%),
O: 0.0100% or less (not including 0%), and
iron and unavoidable impurities as a remainder,
in which an Ac3 point (°C) represented by the following Equation (1) is 890°C or more, and an area
ratio of ferrite at a depth to be 1/4 of a steel sheet thickness is 80% or more.

[0010] In Equation (1), [C], [Si], [Mn], [P], [Al], and [Ti] are values denoting percentage
contents of C, Si, Mn, P, Al, and Ti in terms of % by mass, respectively.
[0011] The objects, features and advantages of the present invention will be apparent from
the following detailed description and accompanying drawings.
Brief Description of Drawings
[0012]
FIG. 1 is a schematic diagram illustrating a heat treatment pattern assuming a hot
stamping process.
FIG. 2 is a graph illustrating a relation between a tensile strength TS and a yield
stress YS after a heat treatment.
Description of Embodiments
[0013] The inventors conducted studies from various angles in order to achieve the object.
As a result, it was found that the object is brilliantly achieved when the Ac
3 point (°C) of a steel sheet is increased by appropriately adjusting the chemical
composition and the steel sheet has a microstructure mainly composed of ferrite, whereby
the present invention was completed.
[0014] In the present invention, it is possible to realize a low-strength steel sheet for
hot stamping, from which a hot stamped member having a yield ratio YR of 70% or more
and a tensile strength TS of 500 to 800 MPa can be manufactured without largely depending
on the hot stamping process.
[0015] The reason why the chemical composition is set as described above in the low-strength
steel sheet for hot stamping of the present embodiment is as follows. Hereinafter,
% in the chemical composition means % by mass.
[0016] The low-strength steel sheet for hot stamping of the present embodiment satisfies
C: 0.005% to 0.12%, Si: 0.50% to 2.0%, Mn: 0.50% or less (not including 0%), Al: 0.010%
to 1.0%, P: 0.1000% or less (not including 0%), S: 0.0100 % or less (not including
0%), N: 0.0100% or less (not including 0%), and O: 0.0100% or less (not including
0%).
[C: 0.005% to 0.12%]
[0017] C is an element that secures the strength of steel sheets. C is also an element that
facilitates the generation of martensite in the microstructure after a heat treatment
by lowering the Ac
3 point and increases the strength of hot stamped members. When the amount of such
C becomes excessive, a decrease in the yield ratio YR of hot stamped members is caused,
and the upper limit of the amount of C is thus required to be set to 0.12% or less.
The amount of C is preferably 0.10% or less, more preferably 0.08% or less. On the
other hand, an excessive decrease in the amount of C leads to an increase in the manufacturing
cost, and thus the amount of C is set to 0.005% or more. The amount of C is preferably
0.007% or more, more preferably 0.010% or more.
[Si: 0.50% to 2.0%]
[0018] Si is an important element in order to raise the Ac
3 point, to decrease the austenite fraction during heat treatment, and to decrease
the hot stamping process dependence of hot stamped members. Si is also an element
that contributes to the strength securing of hot stamped members by the solid solution
strengthening of ferrite. In order to exert these effects, the amount of Si is set
to 0.50% or more. The amount of Si is preferably 0.70% or more, more preferably 1.0%
or more. However, when the amount of Si becomes excessive, deterioration in the pickling
property during steel sheet manufacture and deterioration in the plating property
are caused. The amount of Si is thus set to 2.0% or less. The amount of Si is preferably
1.8% or less, more preferably 1.6% or less.
[Mn: 0.50% or less (not including 0%)]
[0019] Mn lowers the Ac
3 point and is thus an unfavorable element in the present invention. Mn is also an
element that increases the austenite fraction during heat treatment and enhances the
hot stamping process dependence of hot stamped members. Furthermore, Mn enhances hardenability,
facilitates the generation of martensite in the microstructure of hot stamped members,
and lowers the yield ratio YR of hot stamped members. Hence, the amount of Mn is set
to 0.50% or less. The amount of Mn is preferably 0.40% or less, more preferably 0.30%
or less. On the other hand, an excessive decrease in the amount of Mn leads to an
increase in the manufacturing cost, and thus the amount of Mn is set to more than
0%. The lower limit of the amount of Mn is preferably 0.005% or more, more preferably
0.01% or more.
[Al: 0.010% to 1.0%]
[0020] Al is an element that acts as a deoxidizer. Al, as Si, is an element that raises
the Ac
3 point, decreases the austenite fraction during heat treatment, and decreases the
hot stamping process dependence of hot stamped members. Al is also an element that
is dissolved in ferrite to form a solid solution and contributes to the strength securing
of hot stamped members by the solid solution strengthening of ferrite. In order to
exert these effects, the amount of Al is set to 0.010% or more. The amount of Al is
preferably 0.020% or more, more preferably 0.025% or more. However, an excessive content
of Al leads to an increase in the manufacturing cost, and thus the amount of Al is
set to 1.0% or less. The amount of Al is preferably 0.80% or less, more preferably
0.70% or less.
[P: 0.1000% or less (not including 0%)]
[0021] P is an element that is unavoidably contained and is an element that deteriorates
the weldability of steel sheets. P is also an element having an effect of contributing
to the solid solution strengthening of ferrite phase. In order to exert such effects
and not to deteriorate the weldability of steel sheets, the amount of P is set to
0.1000% or less. The amount of P is preferably 0.0500% or less, more preferably 0.0200%
or less. P is an impurity that is unavoidably mixed into steel, and it is impossible
to decrease the amount of P to 0% in industrial production, and P is usually contained
at 0.0005% or more.
[S: 0.0100% or less (not including 0%)]
[0022] S is an element that is unavoidably contained and deteriorates the weldability of
steel sheets. The amount of S is thus set to 0.0100% or less. The amount of S is preferably
0.0080% or less, more preferably 0.0050% or less. It is more preferable that the amount
of S is as small as possible, and thus the lower limit of the amount of S is not particularly
limited. However, it is impossible to decrease the amount of S to 0% in industrial
production, and S is usually contained at 0.0001 % or more.
[N: 0.0100% or less (not including 0%)]
[0023] N is an element that is unavoidably contained, and N forms AlN and diminishes the
effect of solute Al when being contained in an excessive amount. The amount of N is
thus set to 0.0100% or less. The amount of N is preferably 0.0080% or less, more preferably
0.0050% or less. It is more preferable that the amount of N is as small as possible,
and thus the lower limit of the amount of N is not particularly limited. However,
it is impossible to decrease the amount of N to 0% in industrial production, and N
is usually contained at 0.0001% or more.
[O: 0.0100% or less (not including 0%)]
[0024] O is an element that is unavoidably contained, and O forms an oxide when being contained
in an excessive amount, and lowers the amount of solute Si to cause a decrease in
the strength of ferrite. The amount of O is thus set to 0.0100% or less. The amount
of O is preferably 0.0050% or less, more preferably 0.0030% or less. It is more preferable
that the amount of O is as small as possible, and thus the lower limit of the amount
of O is not particularly limited. However, it is impossible to decrease the amount
of O to 0% in industrial production, and O is usually contained at 0.0001% or more.
[0025] The basic components of the low-strength steel sheet for hot stamping of the present
embodiment are as described above, and the remainder is iron and unavoidable impurities
other than P, S, N, and O described above. As these unavoidable impurities, mixing
of tramp elements (Pb, Bi, Sb, Sn, and the like) introduced depending on the situations
of raw materials, materials, manufacturing equipment and the like is permitted as
long as the effects of the present invention are not impaired.
[0026] The low-strength steel sheet for hot stamping of the present embodiment may further
contain at least one of Ti and Nb as another element, and the properties of the steel
sheet are further improved by containing these elements.
[At least one of Ti: 0.10% or less (not including 0%) and Nb: 0.10% or less (not including
0%)]
[0027] Ti and Nb are carbide forming elements and are elements that contribute to the micronization
of the microstructure of steel sheets. As the microstructure of steel sheets is micronized,
reverse transformation during heat treatment is promoted, but the generation of ferrite
can be promoted during cooling in the hot stamping process, and the ferrite fraction
in the hot stamped member can be increased. Such an effect increases as the content
of Ti and Nb increases, but there is a disadvantage that the cold rollability deteriorates
when Ti and Nb are excessively contained. From this point of view, Ti and Nb are both
contained at 0.10% or less. The contents of Ti and Nb are preferably 0.07% or less,
more preferably 0.05% or less. One of Ti and Nb may be contained, or both of Ti and
Nb may be contained. The lower limits of the contents of Ti and Nb are not limited
since the effects are exerted when Ti and Nb are contained in small amounts, and Ti
and Nb are preferably contained at 0.005% or more in order to exert the effects more
effectively.
[0028] The low-strength steel sheet for hot stamping of the present embodiment has an Ac
3 point (°C) of 890°C or more as represented by the following Equation (1).

[0029] In Equation (1), [C], [Si], [Mn], [P], [Al], and [Ti] are values denoting percentage
contents of C, Si, Mn, P, Al, and Ti in terms of % by mass, respectively.
[0030] "
Leslie Steel Materials Science" (Maruzen Co., Ltd., May 31, 1985, p. 273) states that the Ac
3 point (°C) is calculated from the following Equation (2). Equation (1) is a simplified
equation of the following Equation (2) in consideration of the kinds of elements contained.
Namely, in the low-strength steel sheet for hot stamping of the present embodiment,
the attention is paid to Si and Al that increase the Ac
3 point (°C) and have less concern about deterioration in other properties, and the
amounts of C, Mn and the like that decrease the Ac
3 point (°C) are decreased.

[0031] In Equation (2), [C], [Ni], [Si], [V], [Mo], [W], [Mn], [Cr], [Cu], [P], [Al] and
[Ti] are values denoting the percentage contents of C, Ni, Si, V, Mo, W, Mn, Cr, Cu,
P, Al, As and Ti in terms of % by mass, respectively.
[0032] In the low-strength steel sheet for hot stamping of the present embodiment, it is
required that the area ratio of ferrite at a depth to be 1/4 of the steel sheet thickness
is 80% or more. The measurement point of the area ratio of ferrite is set to the depth
to be 1/4 of the steel sheet thickness because it is the point where the most typical
properties of the steel sheet are exhibited.
[0033] In the present embodiment, the area ratio of ferrite is a value measured by point
counting. This point counting is a method applied for calculation of the area percentage
between a mixed microstructure and ferrite crystal grains when a microstructure other
than ferrite is mixed, and is a method in which a photograph of the surface to be
inspected (a surface exposed to a depth to be 1/4 of the steel sheet thickness) is
taken, a prescribed grid line is placed on the taken photograph, and the number of
lattice point centers occupied by ferrite crystal grains is counted. In Examples described
later, the point counting was performed under the condition that the number of cells
(squares) partitioned by grid lines was 100. For the microstructure observation when
the area ratio of ferrite is determined, an optical microscope or a scanning microscope
is used properly (magnification: a range of 400 to 1000) depending on the size of
ferrite crystal grains, but the numerical values measured do not change.
[0034] By appropriately controlling the design of the chemical composition as described
above and increasing the area ratio of ferrite in the steel sheet, it is possible
to decrease the microstructure fraction containing C such as pearlite, bainite, and
martensite that are preferentially reverse transformed to austenite. By increasing
the ferrite area ratio in the steel sheet, the reverse transformation to austenite
can be delayed, the austenite fraction during heat treatment can be decreased, the
yield stress YS can be secured and the yield YR ratio can be increased without extremely
increasing the tensile strength TS of the steel sheet after the heat treatment.
[0035] It is required that the area ratio of ferrite in the low-strength steel sheet for
hot stamping of the present embodiment is 80% or more from this point of view. The
area ratio of ferrite is preferably 84% or more, more preferably 86% or more. Alternatively,
the area ratio of ferrite may be 100%. In the low-strength steel sheet for hot stamping
of the present embodiment, it is only required that the area ratio of ferrite is 80%
or more, and pearlite, bainite, and martensite mentioned above as microstructures
other than ferrite may be contained in small amounts. Alternatively, residual austenite
may be contained.
[0036] From the gist, it is preferable not to contain elements that may decrease the area
ratio of ferrite as much as possible. For example, B has an action of suppressing
the generation and growth of polygonal ferrite from the austenite grain boundaries,
and as a result, acts to decrease the area ratio of ferrite. It is preferable not
to contain elements, such as B, that decrease the ferrite area ratio, as much as possible.
However, it is permissible to contain elements that decrease the ferrite area ratio
in a range in which adverse effects as mentioned above are not exerted, for example,
at 0.0005% or less.
[0037] The low-strength steel sheet for hot stamping of the present embodiment includes
hot rolled steel sheets and cold rolled steel sheets, and these hot rolled steel sheets
and cold rolled steel sheets may have a hot dip-galvanized layer (GI: Hot Dip-Galvanized)
or a hot dip-galvannealed layer (GA: Alloyed Hot Dip-Galvanized), and the present
invention also includes hot dip-galvanized steel sheets (GI steel sheets) and hot
dip-galvannealed steel sheets (GA steel sheets).
[0038] The present specification discloses various aspects of a technology as described
above, but the main technology is summarized below.
[0039] The low-strength steel sheet for hot stamping of the present embodiment contains,
in % by mass, C: 0.005% to 0.12%, Si: 0.50% to 2.0%, Mn: 0.50% or less (not including
0%), Al: 0.010% to 1.0%, P: 0.1000% or less (not including 0%), S: 0.0100% or less
(not including 0%), N: 0.0100% or less (not including 0%), O: 0.0100% or less (not
including 0%), and iron and unavoidable impurities as the remainder, in which the
Ac
3 point (°C) represented by Equation (1) is 890°C or more and the area ratio of ferrite
at a depth to be 1/4 of the steel sheet thickness is 80% or more.
[0040] By adopting such a configuration, it is possible to realize a low-strength steel
sheet for hot stamping, from which a hot stamped member having a yield ratio of 70%
or more and a tensile strength of 500 to 800 MPa can be manufactured without largely
depending on the hot stamping process.
[0041] The low-strength steel sheet for hot stamping of the present embodiment can further
contain at least one of Ti: 0.10% or less (not including 0%) and Nb: 0.10% or less
(not including 0%), and the properties of the steel sheet are further improved depending
on the components contained.
[0042] The low-strength steel sheet for hot stamping of the present embodiment is useful
as a steel sheet for manufacturing a tailored blank member by combining with a steel
sheet having a tensile strength of 1000 MPa or more after a heat treatment. In a normal
hot stamping process, the heating temperature before press molding is set to the single-phase
temperature of austenite (namely, a temperature higher than the Ac
3 point). The steel sheet heated to the temperature region is then press-molded while
being cooled by the mold to be formed into a hot pressed member.
[0043] In a steel sheet having a tensile strength of 1000 MPa or more after a heat treatment,
the Ac
3 point of the steel sheet is usually set to a temperature lower than 860°C. Therefore,
when the low-strength steel sheet for hot stamping of the present embodiment is subjected
to tailored blank by combining with a steel sheet having a tensile strength of 1000
MPa or more after a heat treatment by welding or the like, then heating is performed
to a temperature range of 860°C or more and the Ac
3 point or less of the low-strength steel sheet for hot stamping, and then hot stamping
is performed, a tailored blank material having a region where the tensile strength
is 1000 MPa or more and a region where the tensile strength is 500 to 800 MPa is obtained.
[0044] Namely, in a steel sheet having a tensile strength of 1000 MPa or more after a heat
treatment, the heating temperature range described above becomes the austenite region
and martensite and bainite are generated during subsequent cooling to make the steel
sheet high-strength. In the low-strength steel sheet for hot stamping of the present
embodiment, the heating temperature range described above becomes the two-phase region
of austenite and ferrite, and the generation of martensite and bainite is suppressed
during subsequent cooling and the microstructure mainly composed of ferrite is formed
to make the steel sheet low-strength. As described above, in the hot stamping process,
the heating temperature before press molding is set to the single-phase temperature
of austenite, specifically in the temperature range of 900°C ± 50°C. However, in the
present invention, the heating temperature range during hot stamping may be appropriately
set within the temperature range of 900°C + 50°C depending on the Ac
3 point of each steel sheet to be subjected to tailored blank.
[0045] As is clear from the gist, by including heating the low-strength steel sheet for
hot stamping of the present embodiment to the Ac
3 point (°C) or less and subjecting the heated steel sheet to hot stamping, it is possible
to manufacture not only tailored blank materials but also hot stamped members exerting
desired properties. Namely, the hot stamped member obtained using the low-strength
steel sheet for hot stamping of the present embodiment is a hot stamped member exhibiting
properties that the yield ratio is 70% or more and the tensile strength is 500 to
800 MPa.
[0046] Hereinafter, the effects of the present invention will be specifically described
based on Examples, but the following Examples are not intended to limit the present
invention, and any design change according to the gist described above and to be described
below is included in the technical scope of the present invention.
Examples
[0047] Various steel materials having the chemical compositions (steel types A to H) presented
in Table 1 below were manufactured, and various steel sheets (Experiment Nos. 1 to
8) were fabricated under the hot rolling conditions presented in Table 2 below. The
steel types A to F presented in Table 1 below are examples prepared in a laboratory,
and steel types G and H are materials prepared by a real manufacturing equipment.
The Ac
3 points presented in Table 1 are the values calculated based on Equation (1). In Table
1, the column of [-] means that it is not added or it is less than the measurement
limit. P, S, N, and O are unavoidable impurities as described above, and the values
presented in the columns of P, S, N, and O mean amounts unavoidably contained. The
thickness of the GA steel sheet of Experiment No. 7 is the thickness after the surface
was ground by 0.2 mm and the alloyed hot dip-galvanized layer was removed. The thickness
of the hot rolled steel sheet of Experiment No. 8 is the thickness after the surface
was ground by 0.2 mm and the scale was removed.
[Table 1]
| Steel type |
Chemical composition (% by mass) |
Ac3 point (°C) |
Remark |
| C |
Si |
Mn |
Al |
P |
S |
N |
O |
Ti |
Nb |
B |
| A |
0.05 |
1.2 |
0.2 |
0.035 |
0.0100 |
0.0016 |
0.0031 |
0.0012 |
- |
- |
0.0002 |
933 |
Prepared in laboratory |
| B |
0.05 |
1.2 |
0.2 |
0.035 |
0.0100 |
0.0016 |
0.0031 |
0.0010 |
- |
0.05 |
- |
934 |
Prepared in laboratory |
| C |
0.09 |
1.2 |
0.2 |
0.037 |
0.0120 |
0.0016 |
0.0025 |
0.0008 |
- |
- |
- |
921 |
Prepared in laboratory |
| D |
0.05 |
1.2 |
0.2 |
0.487 |
0.0100 |
0.0014 |
0.0040 |
0.0011 |
- |
- |
- |
1116 |
Prepared in laboratory |
| E |
0.04 |
1.2 |
2.2 |
0.034 |
0.0110 |
0.0019 |
0.0032 |
0.0006 |
0.03 |
- |
0.0016 |
888 |
Prepared in laboratory |
| F |
0.06 |
0.02 |
1.5 |
0.035 |
0.0090 |
0.0020 |
0.0027 |
0.0015 |
0.07 |
0.05 |
0.0015 |
864 |
Prepared in laboratory |
| G |
0.07 |
0.01 |
2.1 |
0.040 |
0.0400 |
0.0400 |
0.0027 |
0.0016 |
- |
0.05 |
- |
838 |
Prepared by real equipment |
| H |
0.08 |
0.02 |
1.4 |
0.038 |
0.0380 |
0.0380 |
0.0042 |
0.0009 |
- |
0.03 |
- |
854 |
Prepared by real equipment |
[Table 2]
| Experiment No. |
Steel type |
Hot rolling conditions |
Steel sheet thickness (mm) |
Type of steel sheet |
| Finishing temperature (°C) |
Holding temperature corresponding to coiling temperature (°C) |
| 1 |
A |
900±20 |
650 |
1.4 |
Cold rolled steel sheet |
| 2 |
B |
| 3 |
C |
| 4 |
D |
| 5 |
E |
| 6 |
F |
| 7 |
G |
890 |
560 |
1.0 |
GA steel sheet |
| 8 |
H |
860 to 880 |
500 to 550 |
2.1 |
Hot rolled steel sheet |
[0048] With respect to the obtained various steel sheets, the area ratio of ferrite (hereinafter
referred to as "ferrite fraction") was measured by the point counting described above,
and a heat treatment assuming a hot stamping process was performed, and the tensile
properties of the steel sheets after the heat treatment were evaluated by the following
method. The heat treatment conditions at this time were performed by a heat treatment
simulator based on the following References 1 and 2. The heat treatment pattern assuming
a hot stamping process is schematically illustrated in FIG. 1. Reference 1:
Conference Proceedings of the Society of Automotive Engineers of Japan, No.72-07,
p.14
Reference 2:
Metal Forming, steel research int. 79 (2008), No. 2, p. 81
[0049] The heat treatment pattern illustrated in FIG. 1 indicates that the steel sheet is
heated to 890°C at a heating rate of 10°C/sec, held at that temperature for 300 seconds,
then cooled to 750°C at a cooling rate of 20°C/sec, cooled to 450°C at a cooling rate
of 40°C/sec, and then further cooled to room temperature (25°C) at a cooling rate
of about 5°C/sec.
[Measurement of tensile properties]
[0050] The tensile strength TS and yield stress YS were determined by collecting JIS No.
5 test pieces (sheet-shaped test pieces) and conducting a tensile test in conformity
with JIS Z 2241: 2011. At this time, with regard to the yield stress YS, the upper
yield point UYP was measured when a clear yield point appeared, and 0.2% proof stress
σ
0.2 was determined based on the JIS provision when the yield point did not appear. As
the acceptance criteria, a tensile strength TS in a range of 500 to 800 MPa and a
yield ratio YR of 70% or more were determined as acceptance.
[0051] The results of these are presented in Table 3 below together with the applied steel
types (steel types A to H).
[Table 3]
| Experiment No. |
Steel type |
Ferrite fraction (% by area) |
Tensile properties of steel sheet after heat treatment |
| Tensile strength TS (MPa) |
Upper yield point UYP or 0.2% proof stress σ0.2 (MPa) |
Yield ratio YR (%) |
| 1 |
A |
95 |
545 |
473 |
87 |
| 2 |
B |
99 |
532 |
480 |
90 |
| 3 |
C |
91 |
541 |
474 |
88 |
| 4 |
D |
97 |
646 |
515 |
80 |
| 5 |
E |
31 |
753 |
493 |
65 |
| 6 |
F |
20 |
598 |
360 |
60 |
| 7 |
G |
72 |
640 |
404 |
63 |
| 8 |
H |
64 |
546 |
368 |
67 |
[0052] From the results, it can be considered as follows. Experiment Nos. 1 to 4 are examples
of the present invention in which the chemical composition, the Ac
3 transformation point (°C) and the ferrite fraction are within the ranges prescribed
in the present invention, and it can be seen that a tensile strength TS of 500 to
800 MPa after a heat treatment and a yield ratio YR of 70% or more were secured in
Experiment Nos. 1 to 4.
[0053] In contrast, Experiment Nos. 5 to 8 are comparative examples that do not satisfy
any of the requirements prescribed in the present invention, and desired properties
was not obtained in Experiment Nos. 5 to 8. Specifically, Experiment No. 5 is an example
obtained using steel type E in which the amount of Mn is excessive (the amount of
B is also excessive), and is a steel sheet having an Ac
3 transformation point (°C) lower than 890°C and a low ferrite fraction, and the yield
ratio YR of the steel sheet after a heat treatment is less than 70%. Experiment No.
6 is an example obtained using steel type F in which the amount of Si is small and
the amount of Mn is excessive (the amount of B is also excessive), and is a steel
sheet having an Ac
3 transformation point (°C) lower than 890°C and a low ferrite fraction, and the yield
ratio YR of the steel sheet after a heat treatment is less than 70%.
[0054] Experiment No. 7 is an example applied to GA steel sheet, but is obtained using steel
type G in which the amount of Si is small and the amount of Mn is excessive, and is
a steel sheet having an Ac
3 transformation point (°C) lower than 890°C and a low ferrite fraction, and the yield
ratio YR of the steel sheet after a heat treatment is less than 70%. Experiment No.
8 is an example applied to a hot rolled steel sheet, but is obtained using steel type
H in which the amount of Si is small and the amount of Mn is excessive, and is a steel
sheet having an Ac
3 transformation point (°C) lower than 890°C and a low ferrite fraction, and the yield
ratio YR of the steel sheet after a heat treatment is less than 70%.
[0055] Based on these results, the relation between the tensile strength TS and the yield
stress YS after a heat treatment is illustrated in FIG. 2. In FIG. 2, the line L denotes
the boundary line where the yield ratio YR is 70%, the upper region including the
line L indicates that the yield ratio YR is 70% or more, and the region below the
line L indicates that the yield ratio YR is less than 70%. In FIG. 2, "Experiment
No." is abbreviated as "No.".
[0056] As is clear from the results, in the examples of the present invention (Nos. 1 to
4), it can be seen that hot stamped members (steel sheets after heat treatment) having
a yield ratio of 70% or more and a tensile strength TS of 500 to 800 MPa can be manufactured
without largely depending on the hot stamping process.
[0058] In order to express the present invention, the present invention has been described
above appropriately and sufficiently through the embodiments with reference to specific
examples and the like. However, it should be recognized by those skilled in the art
that changes and/or improvements of the above-described embodiments can be readily
made. Accordingly, changes or improvements made by those skilled in the art shall
be construed as being included in the scope of the claims unless otherwise the changes
or improvements are at the level which departs from the scope of the appended claims.
Industrial Applicability
[0059] The present invention has a wide range of industrial applicability in the technical
field related to steel sheets for hot stamping and hot stamped members.