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(11)

EP 4 150 382 A2

(12)

(88) Date of publication A3: 03.03.2022 (43) Date of publication: 22.03.2023 Bulletin 2023/12 (21) Application number: 21833473.8 (22) Date of filing: 01.07.2021

(51) International Patent Classification (IPC):  G01V 5/00(2006.01) G01V 13/00(2006.01) G01V 5/08(2006.01) (52) Cooperative Patent Classification (CPC): G01N 23/046; G01N 23/10 (86) International application number: PCT/US2021/040140 (87) International publication number: WO 2022/006429 (06.01.2022 Gazette 2022/01)

(84) Designated Contracting States: AL AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HR HU IE IS IT LI LT LU LV MC MK MT NL NO PL PT RO RS SE SI SK SM TR Designated Extension States: BA ME Designated Validation States: KH MA MD TN (30) Priority: 02.07.2020 US 202063047639 P (71) Applicant: Battelle Memorial Institute Columbus, OH 43201 (US)

(72) Inventors: COCHRAN, Joseph Matthew Egg Harbor Township, New Jersey 08234 (US) ADERHOLDT, Matthew Robert Vineland, New Jersey 08360 (US) BUXTON, Jesse Thomas Columbus, Ohio 43201 (US) AUME, Laura Lee Strang Circleville, Ohio 43113 (US) TATAROWICZ, John Blackwood, New Jersey 08012 (US) HALLGREN, Rodney Philadelphia, Pennsylvania 19130 (US) (74) Representative: Forresters IP LLP  Skygarden Erika-Mann-Straße 11 80636 München 80636 München (DE)