Technical Field
[0001] The present invention relates to a non-combustion-heating-type tobacco and an electric
heating tobacco product.
Background Art
[0002] Electric heating tobacco products that include a non-combustion-heating-type tobacco
which are inserted into an electric heating device when used have been developed as
an alternative to cigarettes (paper-wrapped tobaccos) (Patent Document 1). The non-combustion-heating-type
tobacco commonly includes a tobacco rod formed by a shredded tobacco, a material that
generates a flavor component, and the like being wrapped with a wrapping paper, a
mouthpiece used for inhaling components generated from the tobacco rod by heating,
and a tipping paper with which the above members are wrapped.
[0003] Commonly, in an electric heating tobacco product, the non-combustion-heating-type
tobacco is inserted into an electric heating device and, subsequently, a heater member
is caused to produce heat. As a result, the tobacco rod is heated from a portion of
the tobacco rod which is in contact with the heater member, and the components generated
by heating are delivered to the user
[0004] The delivery of components generated by heating has been considered as an important
characteristic for not only electric heating tobacco products but also cigarettes
and widely studied.
[0005] Patent Document 2 discloses a cigarette including a tobacco rod that includes a volatile
containing material included in a polysaccharide gel in order to increase the amount
of delivery of a volatile flavoring agent contained in smoke generated on the first
puff, to eliminate the possibility of the volatile flavoring agent bleeding out during
storage, and to maintain the intended amount of delivery of the volatile flavoring
agent during smoking subsequent to storage.
[0006] Patent Document 3 discloses a cigarette that includes an adsorbent or liquid absorber
added to a filter disposed downstream of a tobacco rod in order to reduce the amount
of unfavorable components generated by combustion and enables the delivery of a suitable
flavor.
Citation List
Patent Document
Summary of Invention
Technical Problem
[0008] In the techniques disclosed in Patent Documents 1 and 2 above, a specific material
is added to a tobacco rod or a filter in order to adjust the amount of volatile components
and achieve the delivery of intended components. Compared with the techniques of improving
the delivery of components generated by heating with attention being focused on the
materials included in tobacco, there have not been many studies of techniques of improving
the delivery of the above components with attention being focused on the structure
of the material constituting the filter. Thus, there is room for improvement.
[0009] An increase in the amount of components delivered through an electric heating tobacco
product has been particularly anticipated, because the temperatures at which electric
heating tobacco products are heated during use are low and the amount of components
generated by electric heating tobacco products is small compared with cigarettes,
which involve combustion.
[0010] Accordingly, an object of the present invention is to provide a non-combustion-heating-type
tobacco and an electric heating tobacco product that increase the amount of delivery
of the components generated by heating.
Solution to Problem
[0011] The inventors of the present invention conducted extensive studies and consequently
found that the above-described issues may be addressed by forming a filter element
included in the filter using a fiber having a specific shape and a specific size.
Thus, the inventors of the present invention conceived the present invention.
[0012] Specifically, the summary of the present invention is as follows.
- [1] A rod-shaped non-combustion-heating-type tobacco comprising a tobacco rod portion
and a mouthpiece portion,
wherein the mouthpiece portion includes a filter segment including a filter element,
the filter element being composed of a fiber, a cross section of the fiber taken in
a circumferential direction being Y-shaped, the fiber having a filament denier of
8 or more and 12 or less.
- [2] The non-combustion-heating-type tobacco according to [1], wherein the filter element
has a density of 0.09 g/cm3 or more and 0.14 g/cm3 or less.
- [3] The non-combustion-heating-type tobacco according to [1] or [2], wherein the filter
element has a compression change P of 88% or more and 95% or less, the compression
change P being represented by Formula (1),

P(%): a compression change
D1 (mm): a diameter of the filter element, the diameter being measured in a compressive
direction after the filter element has been compressed and deformed in a direction
perpendicular to an airflow direction at a compressive load of 3 N/mm per unit length
in a longitudinal direction for a compression time of 10 seconds
D2 (mm): an average diameter of the filter element before compression.
- [4] The non-combustion-heating-type tobacco according to any one of [1] to [3], wherein
a length of the filter element in a longitudinal direction is 5 mm or more and 20
mm or less.
- [5] The non-combustion-heating-type tobacco according to any one of [1] to [4], wherein
an airflow resistance of the filter segment in a longitudinal direction is 1.0 mmH2O/mm or more and 4.0 mmH2O/mm or less.
- [6] The non-combustion-heating-type tobacco according to any one of [1] to [5], wherein
a flavoring agent capsule is disposed inside the filter element.
- [7] An electric heating tobacco product comprising:
an electric heating device including a heater member, a battery unit serving as a
power source for the heater member, and a control unit for controlling the heater
member; and
the non-combustion-heating-type tobacco according to any one of [1] to [6], the non-combustion-heating-type
tobacco being inserted in the electric heating device so as to come into contact with
the heater member. Advantageous Effects of Invention
[0013] According to the present invention, a non-combustion-heating-type tobacco and an
electric heating tobacco product that increase the amount of delivery of the components
generated by heating can be provided.
Brief Description of Drawings
[0014]
[Fig. 1] Fig. 1 is a schematic diagram illustrating a non-combustion-heating-type
tobacco according to an embodiment of the present invention.
[Fig. 2] Fig. 2 is a schematic diagram illustrating an electric heating tobacco product
according to an embodiment of the present invention.
[Fig. 3] Fig. 3 is a schematic diagram illustrating an electric heating tobacco product
according to an embodiment of the present invention.
[Fig. 4] Fig. 4 is a diagram illustrating a mouth end side end of a region of a cooling
segment which is in contact with an electric heating device.
[Fig. 5] Fig. 5 is a diagram illustrating a mouth end side end of a region of a cooling
segment which is in contact with an electric heating device.
[Fig. 6] Fig. 6 is a graph illustrating the amounts of nicotine and glycerine delivered
in Examples.
[Fig. 7] Fig. 7 is a graph illustrating the amounts of nicotine and glycerine delivered
in Examples.
[Fig. 8] Fig. 8 is a graph illustrating the amounts of nicotine and glycerine delivered
in Examples.
[Fig. 9] Fig. 9 is a graph illustrating the amounts of nicotine and glycerine delivered
in Examples. Description of Embodiments
[0015] Details of embodiments of the present invention are described below. Note that the
following description is merely an example (typical example) of the embodiments of
the present invention and the present invention is not limited by the contents thereof
without departing from the summary thereof.
[0016] In the present specification, in the case where a range is expressed using "to" and
values or physical properties described before and after "to", it is considered that
the range includes the values described before and after "to".
[0017] In the present specification, the term "a plurality of" refers to "two or more" unless
otherwise specified.
<Non-Combustion-Heating-Type Tobacco>
[0018] A non-combustion-heating-type tobacco according to an embodiment of the present invention
(also referred to simply as "non-combustion-heating-type tobacco") is a rod-shaped
non-combustion-heating-type tobacco including a tobacco rod portion and a mouthpiece
portion.
[0019] The mouthpiece portion includes a filter segment including a filter element.
[0020] The filter element is composed of a fiber the cross section of which taken in the
circumferential direction is Y-shaped and which has a filament denier of 8 or more
and 12 or less.
[0021] Fig. 1 illustrates an example of the non-combustion-heating-type tobacco according
to the embodiment. The non-combustion-heating-type tobacco is described below with
reference to Fig. 1.
[0022] The rod-shaped non-combustion-heating-type tobacco 10 illustrated in Fig. 1 is a
rod-shaped non-combustion-heating-type tobacco that includes a tobacco rod portion
11, a mouthpiece portion 14, and a tipping paper 15 wrapped around the above members.
The mouthpiece portion 14 includes a cooling segment 12 and a filter segment 13 including
a filter element. The cooling segment 12 is arranged adjacent to the tobacco rod portion
11 and the filter segment 13 and sandwiched therebetween in the axial direction (also
referred to as "longitudinal direction") of the non-combustion-heating-type tobacco
10. Perforations V are formed concentrically in the cooling segment 12 in the circumferential
direction. The perforations V are usually perforations that facilitate the entry of
outside air by the inhalation of the user. The entry of air reduces the temperature
of the components and air taken in from the tobacco rod portion 11.
[0023] In the non-combustion-heating-type tobacco 10, components generated as a result of
heating of the tobacco rod portion 11 or the like are delivered into the mouth of
the user through the mouthpiece portion. Examples of the components generated by heating
include a flavor component derived from a flavoring agent, nicotine and tar derived
from tobacco leaves, and an aerosol component derived from an aerosol-source material.
In the present specification, the term "aerosol-source material" refers to a material
that generates an aerosol.
[0024] The non-combustion-heating-type tobacco 10 preferably has a pillar-like shape that
is a shape having an aspect ratio of 1 or more, the aspect ratio being defined as
described below.

where w represents the width of the bottom of the pillar-shaped body (in the present
specification, the width of the tobacco rod portion-side bottom), and h represents
the height of the pillar-shaped body. It is preferable that h ≥ w. In the present
specification, the longitudinal direction is defined as the direction represented
by h. Thus, even if w ≥ h, the direction represented by h is referred to as "longitudinal
direction" for the sake of simplicity. The shape of the bottom may be, but not limited
to, a polygonal shape, a polygonal shape having rounded corners, a circular shape,
an oval shape, or the like. When the bottom has a circular shape, the width w is the
diameter of the circle. When the bottom has an oval shape, the width w is the major-axis
length of the oval. When the bottom has a polygonal shape or a polygonal shape having
rounded corners, the width w is the diameter of the circle circumscribing the polygon
or the major-axis length of the oval circumscribing the polygon.
[0025] The length h of the non-combustion-heating-type tobacco 10 in the longitudinal direction
is not limited. The length h is, for example, usually 40 mm or more, is preferably
45 mm or more, and is more preferably 50 mm or more. The length h is usually 100 mm
or less, is preferably 90 mm or less, and is more preferably 80 mm or less.
[0026] The width w of the bottom of the pillar-shaped body of the non-combustion-heating-type
tobacco 10 is not limited. The width w is, for example, usually 5 mm or more and is
preferably 5.5 mm or more. The width w is usually 10 mm or less, is preferably 9 mm
or less, and is more preferably 8 mm or less.
[0027] The proportions of the lengths of the cooling segment and the filter segment to the
length of the non-combustion-heating-type tobacco in the longitudinal direction (cooling
segment: filter segment) is usually, but not limited to, 0.60:1.40 to 1.40:0.60, is
0.80 to 1.20:0.80 to 1.20, is preferably 0.85 to 1.15:0.85 to 1.15, is more preferably
0.90 to 1.10:0.90 to 1.10, and is further preferably 0.95 to 1.05:0.95 to 1.05 in
consideration of the amount of the flavoring agent delivered.
[0028] When the above ratio between the lengths of the cooling segment and the filter segment
falls within the above range, the cooling effect, the effect of reducing loss due
to the adhesion of the generated vapor and aerosol on the inner wall of the cooling
segment, and the function of the filter to adjust the amounts of air and flavor can
be all achieved in a balanced manner and a suitable flavor can be achieved. In particular,
when the length of the cooling segment is increased, the formation of aerosol particles
and the like is facilitated and, consequently, a suitable flavor can be achieved.
However, if the length of the cooling segment is excessively increased, the substance
that passes therethrough may adhere on the inner wall disadvantageously.
[0029] The airflow resistance of the non-combustion-heating-type tobacco 10 per stick in
the longitudinal direction is not limited. In consideration of ease of smoking, the
above airflow resistance is usually 8 mmH
2O or more, is preferably 10 mmH
2O or more, and is more preferably 12 mmH
2O or more, and is usually 100 mmH
2O or less, is preferably 80 mmH
2O or less, and is more preferably 60 mmH
2O or less.
[0030] The above airflow resistance is measured in conformity with an ISO standard method
(ISO6565:2015) using, for example, a filter airflow resistance gage produced by Cerulean.
The airflow resistance is the difference in the air pressure between one of the edge
surfaces (first edge surface) of the non-combustion-heating-type tobacco 10 and the
other edge surface (second edge surface) which occurs when air is passed through the
non-combustion-heating-type tobacco 10 in the direction from the first to second edge
surface at a predetermined air flow rate (17.5 cc/min) while the permeation of air
through the side surfaces of the non-combustion-heating-type tobacco 10 is blocked.
The airflow resistance is commonly expressed in units of mmH
2O. It is known that the airflow resistance is proportional to the length of the non-combustion-heating-type
tobacco when the length of the non-combustion-heating-type tobacco falls within a
usual range (length: 5 to 200 mm); if the length of the non-combustion-heating-type
tobacco doubles, the airflow resistance of the non-combustion-heating-type tobacco
doubles.
[Mouthpiece Portion]
[0031] The mouthpiece portion 14 may have any structure that includes a filter segment 13
including a filter element, the filter element being composed of fibers the cross
section of which taken in the circumferential direction is Y-shaped and which have
a filament denier of 8 or more and 12 or less. The mouthpiece portion 14 may include,
for example, a cooling segment 12 and a filter segment 13 including the above-described
filter element such that the cooling segment 12 is arranged adjacent to the tobacco
rod portion 11 and the filter segment 13 and sandwiched therebetween in the axial
direction of the non-combustion-heating-type tobacco 10 as illustrated in Fig. 1.
Details of the filter segment 13 and the cooling segment 12 are described below.
(Filter Segment)
[0032] The filter segment 13 includes a filter element. The filter element is composed of
fibers the cross section of which taken in the circumferential direction is Y-shaped
and which have a filament denier of 8 or more and 12 or less. The filter segment 13
is not limited and may be any filter segment that has common filter functions. Examples
of the common filter functions include a function of adjusting the amount of air that
enters upon the inhalation of an aerosol or the like, a function of reducing a flavor,
and a function of reducing nicotine and tar. However, the filter segment does not
necessarily have all of the above functions. Furthermore, for electric heating tobacco
products, which generate a smaller amount of components than paper-wrapped tobacco
products and the filling ratio of a tobacco filler is low compared with paper-wrapped
tobacco products, a function of suppressing the filtration function and preventing
detachment of the tobacco filler is one of the important functions.
[0033] The shape of the filter segment 13 is not limited; publicly known shapes may be used.
The filter segment 13 usually has a cylindrical shape. The filter segment 13 may have
the following structure.
[0034] The shape of cross section of the filter segment 13 which is taken in the circumferential
direction is substantially circular. The diameter of the circle can be changed appropriately
in accordance with the size of the product. The diameter of the circle is usually
4.0 mm or more and 9.0 mm or less, is preferably 4.5 mm or more and 8.5 mm or less,
and is more preferably 5.0 mm or more and 8.0 mm or less. In the case where the cross
section taken in the circumferential direction is not circular, the above diameter
is the diameter of a virtual circle having the same area as the cross section.
[0035] The perimeter of the shape of a cross section of the filter segment 13 which is taken
in the circumferential direction can be changed appropriately in accordance with the
size of the product. The above perimeter is usually 14.0 mm or more and 27.0 mm or
less, is preferably 15.0 mm or more and 26.0 mm or less, and is more preferably 16.0
mm or more and 25.0 mm or less.
[0036] The length of the filter segment 13 in the longitudinal direction can be changed
appropriately in accordance with the size of the product. The above length is usually
15 mm or more and 35 mm or less, is preferably 17.5 mm or more and 32.5 mm or less,
and is more preferably 20.0 mm or more and 30.0 mm or less.
[0037] The shape and dimensions of the filter element may be adjusted appropriately such
that the shape and dimensions of the filter segment 13 fall within the above ranges.
The length of the filter element in the longitudinal direction may be changed appropriately
in accordance with the size of the product. In order to achieve the intended hardness,
the above length is usually 3 mm or more and 30 mm or less, is preferably 5 mm or
more and 20 mm or less, is more preferably 8 mm or more and 18 mm or less, and is
further preferably 10 mm or more and 15 mm or less.
[0038] The airflow resistance of the filter segment 13 in the longitudinal direction is
usually, but not limited to, 1.0 mmH
2O/mm or more and 4.0 mmH
2O/mm or less in consideration of ease of smoking. In particular, in the case where
the filter element includes the flavoring agent capsules described below, the above
airflow resistance is preferably 1.5 mmH
2O/mm or more and 4.0 mmH
2O/mm or less in consideration of ease of smoking. In such a case, when the filter
element further includes the flavor agent described below, in particular, when the
filter element includes a crystalline substance, such as menthol, as a flavor agent,
the above airflow resistance is more preferably 2.5 mmH
2O/mm or more and 3.6 mmH
2O/mm or less. When the filter element does not include the flavor agent, the above
airflow resistance is more preferably 1.9 mmH
2O/mm or more and 3.0 mmH
2O/mm or less. In the case where the filter element does not include the flavoring
agent capsules described below, the above airflow resistance is preferably 1.3 mmH
2O/mm or more and 2.4 mmH
2O/mm or less in consideration of ease of smoking, regardless of whether the filter
element includes the flavor agent. The above conditions of airflow resistance may
be applied also to the airflow resistance of the filter element in the airflow direction.
[0039] The above airflow resistance is measured in conformity with an ISO standard method
(ISO6565) using, for example, a filter airflow resistance gage produced by Cerulean.
The airflow resistance of the filter segment 13 is the difference in the air pressure
between one of the edge surfaces (first edge surface) of the filter segment 13 and
the other edge surface (second edge surface) which occurs when air is passed through
the filter segment 13 in the direction from the first to second edge surface at a
predetermined air flow rate (17.5 cc/min) while the permeation of air through the
side surfaces of the filter segment 13 is blocked. The airflow resistance is commonly
expressed in units of mmH
2O. It is known that the airflow resistance of the filter segment 13 is proportional
to the length of the filter segment 13 when the length of the filter segment 13 falls
within a usual range (length: 5 to 200 mm); if the length of the filter segment 13
doubles, the airflow resistance of the filter segment 13 doubles.
[0040] The filter segment 13 may be, for example, a plain filter including a single filter
segment or a multi-segment filter including a plurality of filter segments, such as
a dual filter or a triple filter.
[0041] The filter segment 13 can be produced by a publicly known method. For example, in
the case where a synthetic fiber, such as cellulose acetate tow, is used as a material
for the filter element, the filter segment 13 can be produced by spinning a polymer
solution including a polymer and a solvent into thread and crimping the thread. Examples
of the above method include the method described in International Publication No.
2013/067511.
[0042] In the production of the filter segment 13, the above airflow resistance may be adjusted
as needed. Furthermore, additives (e.g., publicly known adsorbents and flavoring agents
(e.g., menthol), granular active carbon, and flavoring agent keeper) may be added
to the filter element as needed.
[0043] The filter element constituting the filter segment 13 is not limited and may be any
filter element composed of fibers the cross section of which taken in the circumferential
direction is Y-shaped and which have a filament denier of 8 or more and 12 or less.
The filter element may be produced by, for example, forming tow, such as cellulose
acetate tow, composed of fibers having a Y-shaped cross section in the circumferential
direction into a cylindrical shape.
[0044] The cross section of the fibers constituting the tow which is taken in the circumferential
direction is Y-shaped. In the case where tow composed of Y-shaped fibers is used,
a filter segment excellent in terms of amount of delivery is likely to be produced
because of the complexity of the fiber shape, compared with the case where a tow composed
of fibers having a common shape, such as a circular shape, is used. Specifically,
a filter segment that enables the delivery of a large amount of components and has
an intended hardness can be produced while the amount of materials used is reduced,
that is, the costs are saved.
[0045] The filament denier (g/9000m) of the fibers is not limited and may be 8 or more and
12 or less in order to increase the amount of delivery of the components generated
by heating. The above filament denier may be 9 or more and 11 or less. If the filament
denier of the fibers is less than the above range, the structure of the fibers constituting
the filter element may become excessively dense, which reduces the amount of delivery
of the components. If the filament denier of the fibers is more than the above range,
the structure of the fibers constituting the filter element may become excessively
sparse, which makes it impossible to achieve sufficiently high hardness. The total
denier (g/9000m) of the fibers may be, but not limited to, 12000 or more and 35000
or less and is preferably 15000 or more and 30000 or less in order to increase the
amount of delivery of the components generated by heating. The above filament denier
and total denier are particularly preferable when the perimeter of the mouthpiece
portion is 22 mm. In the case where a filter filled with the fibers is used, triacetin
may be added to the fibers such that the amount of triacetin is 5% by weight or more
and 10% by weight or less of the total weight of the fibers in order to enhance the
hardness of the filter.
[0046] The method for producing fibers the cross section of which in the circumferential
direction is Y-shaped is not limited. For example, in the case where the above fibers
are acetate fibers, acetate flakes (cellulose acetate) are produced by acetification
of a pulp material. The acetate flakes are dissolved in acetone with a dissolver (doping).
The resulting solution is spun into fibrous bundles. Fibers having a Y-shaped cross
section in the circumferential direction can be produced by changing the shape of
the nozzle plate used in this spinning step. Furthermore, the thickness (filament
denier) of the fibers can be changed by changing the diameter of the nozzle. Subsequently,
the total denier of the fibers is determined in accordance with the required airflow
resistance, and the number of filaments per bundle (total denier/filament denier)
is determined accordingly. Acetate fibers are spun using a required number of spinning
chambers and tied in a bundle. The bundles are corrugated (crimped) homogeneously
with a crimping machine. Tows transported in a ribbon-like manner are stacked on top
of one another and packaged while being traversed with a baling machine.
[0047] The density of the filter element (in particular, in the case where the filter element
includes the flavoring agent capsules described below, the density of the filter element
excluding the flavoring agent capsules) is usually, but not limited to, 0.09 g/cm
3 or more and 0.25 g/cm
3 or less, is preferably 0.09 g/cm
3 or more and 0.20 g/cm
3 or less, is more preferably 0.09 g/cm
3 or more and 0.14 g/cm
3 or less, and is further preferably 0.11 g/cm
3 or more and 0.14 g/cm
3 or less in order to achieve the intended hardness.
[0048] The compression change P of the filter element which is represented by Formula (1)
below is one of the measures of hardness and usually, but not limited to, 85% or more
and 98% or less, is preferably 88% or more and 95% or less, and is more preferably
90% or more and 93% or less in order to achieve the intended hardness. The method
for measuring the compression change P is not limited. For example, the compression
change P may be measured using SODIM-H Hardness module produced by Sodim SAS. The
compression change P may be adjusted by changing the density of the filter element
or the material constituting the filter element.
P (%): compression change
D1 (mm): the diameter of the filter element which is measured in the compressive direction
after the filter element has been compressed and deformed in a direction perpendicular
to the airflow direction (in the case where the filter element is cylindrical, the
circumferential direction) at a compressive load of 3 N/mm per unit length in the
longitudinal direction for a compression time of 10 seconds.
D2 (mm): the average diameter of the filter element before compression.
[0049] Since the compression change is one of the measures of the hardness of the filter
element, in the present specification, the compression change is also referred to
as "hardness".
[0050] The filter element may include, in addition to the flavoring agent capsules described
below, a component such as a flavoring material. Examples of the flavor agent include
menthol, spearmint, peppermint, fenugreek, clove, and medium-chain triglyceride (MCT).
Among these, menthol is preferable. Only one of the above components may be used alone.
Two or more types of the above components may be used in any combination at any ratio.
[0051] The content of the flavor agent (in particular, menthol) in the filter element (except
the flavor agent included in the flavoring agent capsules described below) is usually,
but not limited to, 0.5% by weight or more and 15% by weight or less, is preferably
3% by weight or more and 10% by weight or less, and is more preferably 10% by weight
or more and 5% by weight or less.
[0052] A crushable additive release container (e.g., a flavoring agent capsule) that includes
a crushable shell composed of gelatin or the like may be disposed inside the filter
element. The flavoring agent capsule (also referred to as "additive release container"
in the technical field) is not limited; publicly known flavoring agent capsules may
be employed. For example, the flavoring agent capsule may be a crushable additive
release container that includes a crushable shell composed of gelatin or the like.
In such a case, when the flavoring agent capsule is broken before, while, or after
the user uses the tobacco product, the flavoring agent capsule releases a liquid or
substance (usually, a flavor agent) included in the capsule. The liquid or substance
is transferred to tobacco smoke during the use of the tobacco product and then transferred
to the ambient environment after the use.
[0053] The form of the flavoring agent capsule is not limited. The flavoring agent capsule
may be, for example, an easy-to-crush flavoring agent capsule. The shape of the flavoring
agent capsule is preferably spherical. The flavoring agent capsule may include the
optional additives described above and particularly preferably include a flavor agent
and active carbon. One or more materials that assist the filtration of smoke may be
used as an additive. The form of the additive is usually, but not limited to, liquid
or individual. Note that the use of a capsule including an additive is known in the
technical field. An easy-to-crush flavoring agent capsule and the method for producing
such a capsule are known in the technical field.
[0054] Examples of the flavor agent include menthol, spearmint, peppermint, fenugreek, clove,
and medium-chain triglyceride (MCT). The flavor agent is menthol or may be menthol
or the like or a combination thereof.
[0055] In the case where the flavoring agent capsules are used, if the filament denier of
the fibers constituting the filter element is more than the upper limit of the above
range, penetration of the components released from the flavoring agent capsules is
unlikely to expand to a sufficient degree. If the above filament denier is less than
the lower limit, the expansion of the components that penetrate the filter may be
excessively facilitated and, consequently, the amount of delivery of the components
may be reduced by an excessive degree.
[0056] In order to increase strength and structural stiffness, the filter segment 13 may
include a filter wrapper (filter plug wrapper) with which the filter element, etc.
are wrapped. The filter wrapper is not limited and may include one or more seams including
an adhesive. The adhesive may include a hot-melt adhesive. The hot-melt adhesive may
include polyvinyl alcohol. In the case where the filter segment is constituted by
two or more segments, it is preferable that the two or more segments be collectively
wrapped with the filter wrapper.
[0057] The material constituting the filter wrapper is not limited; publicly known materials
may be used. The filter wrapper may include a filler, such as calcium carbonate.
[0058] The thickness of the filter wrapper is usually, but not limited to, 20 µm or more
and 140 µm or less, is preferably 30 µm or more and 130 µm or less, and is more preferably
30 µm or more and 120 µm or less.
[0059] The basis weight of the filter wrapper is usually, but not limited to, 20 gsm or
more and 100 gsm or less, is preferably 22 gsm or more and 95 gsm or less, and is
more preferably 23 gsm or more and 90 gsm or less.
[0060] The filter wrapper may be coated and is not necessarily coated. In order to impart
functions other than strength or structural stiffness, it is preferable to coat the
filter wrapper with an intended material.
[0061] The filter segment 13 may further include a center hole segment having one or a plurality
of hollow portions. The center hole segment is usually arranged closer to the cooling
segment than the filter element and is preferably arranged adjacent to the cooling
segment.
[0062] The center hole segment is constituted by a packed layer having one or a plurality
of hollow portions and an inner plug wrapper (inner wrapping paper) wrapped around
the packed layer. For example, the center hole segment is constituted by a packed
layer having a hollow portion and an inner plug wrapper wrapped around the packed
layer. The center hole segment increases the strength of the mouthpiece portion. The
packed layer is, for example, a rod having an inside diameter φ of 1.0 mm or more
and 5.0 mm or less which is filled with cellulose acetate fibers at a high density
and cured with a plasticizer including triacetin, the plasticizer being added in an
amount that is 6% by mass or more and 20% by mass or less of the mass of the cellulose
acetate. Since the pack density of fibers in the packed layer is high, during inhalation,
air and aerosols flow only through the hollow portion and hardly flow inside the packed
layer. Since the packed layer present inside the center hole segment is a fiber-packed
layer, the user seldom feel a sense of incongruity when touching the outside of the
product during use. The center hole segment does not necessarily include the inner
plug wrapper. In such a case, the shape of the product may be maintained by thermoforming.
[0063] The center hole segment and the filter element may be connected to each other with
an outer plug wrapper (outer wrapping paper) or the like. The outer plug wrapper can
be, for example, a cylindrical paper. The tobacco rod portion 11, the cooling segment
12, and the center hole segment and the filter element connected to each other may
be connected to one another with, for example, a mouthpiece lining paper The above
connection can be achieved by, for example, applying a vinyl acetate-based paste or
the like onto the inner surface of the mouthpiece lining paper, placing the tobacco
rod portion 11, the cooling segment 12, and the center hole segment and the filter
element connected to each other on the mouthpiece lining paper, and rolling the mouthpiece
lining paper. Note that the above members may be connected to one another using a
plurality of lining papers in a plurality of stages.
(Cooling Segment)
[0064] The cooling segment 12 is arranged adjacent to the tobacco rod portion and the filter
segment and sandwiched therebetween. The cooling segment 12 is a rod-shaped member
having a cavity formed therein such that a cross section taken in the circumferential
direction is hollow, such as a cylinder.
[0065] The cooling segment 12 may have perforations V (in the technical field, also referred
to as "ventilation filter (Vf)") formed concentrically therein in the circumferential
direction.
[0066] In the case where the tobacco rod portion includes an aerosol-source material, a
vapor containing an aerosol-source material and a tobacco flavor component which are
generated upon heating of the tobacco rod comes into contact with outside air and
the temperature of the vapor is reduced. Thus, the vapor becomes liquefied and the
generation of aerosol can be facilitated.
[0067] In the case where the perforations V arranged concentrically are considered as one
perforation group, the number of the perforation groups may be one or two or more.
In the case where two or more perforation groups are present, it is preferable that
the perforation groups be not arranged at a position less than 4 mm from the boundary
between the cooling segment and the filter segment toward the cooling segment in order
to increase the amount of the delivered components generated by heating.
[0068] In the case where the non-combustion-heating-type tobacco 10 includes the tobacco
rod portion 11, the cooling segment 12, the filter segment 13, and the tipping paper
15 wrapped around the above members, it is preferable that the tipping paper 15 have
perforations formed therein at positions directly above the perforations V formed
in the cooling segment 12. In the case where such a non-combustion-heating-type tobacco
10 is prepared, wrapping may be performed using a tipping paper 15 having perforations
arranged to overlap the perforations V However, in consideration of ease of production,
it is preferable to form perforations that penetrate both cooling segment 12 and tipping
paper 15 after the non-combustion-heating-type tobacco 10 has been prepared using
a cooling segment 12 that does not have the perforations V
[0069] In order to increase the amount of delivery of the components generated by heating,
the perforations V are preferably present at a position 4 mm or more from the boundary
between the cooling segment 12 and the filter segment 13 toward the cooling segment.
The above distance is more preferably 4.5 mm or more, is further preferably 5 mm or
more, and is particularly preferably 5.5 mm or more. In order to maintain the cooling
function, the above distance is preferably 15 mm or less, is more preferably 10 mm
or less, and is further preferably 7 mm or less.
[0070] In order to increase the amount of delivery of the components generated by heating,
the perforations V are preferably present at a position 22 mm or more from the mouth
end of the non-combustion-heating-type tobacco toward the cooling segment. The above
distance is preferably 23.5 mm or more, is preferably 24 mm or more, and is more preferably
25 mm or more. In order to maintain the cooling function, the above distance is preferably
38 mm or less, is more preferably 36.5 mm or less, and is further preferably 33 mm
or less.
[0071] When the boundary between the cooling segment 12 and the tobacco rod portion 11 is
used as a reference, in the case where the length of the cooling segment 12 in the
axial direction is 20 mm or more, in order to maintain the cooling function, the perforations
V are preferably present at a position 2 mm or more from the boundary between the
cooling segment 12 and the tobacco rod portion 11 toward the cooling segment. The
above distance is more preferably 3.5 mm or more and is further preferably 7 mm or
more. In order to increase the amount of delivery of the components generated by heating,
the above distance is preferably 18 mm or less, is more preferably 16.5 mm or less,
is further preferably 15 mm or less, and is particularly preferably 14.5 mm or less.
[0072] The diameter of the perforations V is preferably, but not limited to, 100 µm or more
and 1000 µm or less and is more preferably 300 µm or more and 800 µm or less. The
perforations are preferably substantially circular or substantially oval. In the case
where the perforations are substantially oval, the major-axis length of the perforations
is considered as diameter of the perforations.
[0073] The length of the cooling segment in the longitudinal direction may be changed appropriately
in accordance with the size of the product. The above length is usually 15 mm or more
and is preferably 20 mm or more. The above length is usually 40 mm or less, is preferably
35 mm or less, and is more preferably 30 mm or less. Setting the length of the cooling
segment in the longitudinal direction to be equal to or more than the above lower
limit enables a sufficiently high cooling effect to be maintained and allows a suitable
flavor to be produced. Setting the above length to be equal to or less than the above
upper limit reduces the loss of the generated vapor and aerosol which may be caused
as a result of the vapor and aerosol adhering on the inner wall of the cooling segment.
[0074] In the case where a cooling sheet for cooling or the like is charged into the cooling
segment 12, the total surface area of the cooling segment 12 may be, for example,
but not limited to, 150 mm
2/mm or more and 1000 mm
2/mm or less. The above surface area is the surface area of the cooling segment 12
per length (mm) of the cooling segment 12 in the airflow direction. The total surface
area of the cooling segment 12 is preferably 200 mm
2/mm or more and is more preferably 250 mm
2/mm or more. The above total surface area is preferably 600 mm
2/mm or less and is more preferably 400 mm
2/mm or less.
[0075] It is desirable that the inside structure of the cooling segment 12 have a large
total surface area. Therefore, in a preferable embodiment, the cooling segment 12
may be formed of a thin sheet material that has been wrinkled in order to form channels
and then pleated, gathered, or folded. The larger the number of folds or pleats per
unit volume of the component, the larger the total surface area of the cooling segment.
[0076] The thickness of the material constituting the cooling segment 12 is, for example,
5 µm or more and 500 µm or less and may be, for example, 10 µm or more and 250 µm
or less.
[Tobacco Rod Portion]
[0077] The structure of the tobacco rod portion 11 is not limited and may be any publicly
known structure. The tobacco rod portion 11 usually includes a tobacco filler and
a wrapping paper with which the tobacco filler is wrapped. The tobacco filler is not
limited; publicly known tobacco fillers, such as shredded tobacco and reconstructed
tobacco sheets, may be used. The tobacco filler may include an aerosol-source material.
An aerosol-source material is a material that generates an aerosol upon being heated.
Examples of the aerosol-source material include glycerine, propylene glycol, triacetin,
1,3-butanediol, and mixtures thereof.
[0078] The content of the aerosol-source material in the tobacco filler is not limited.
In order to generate aerosol in a sufficient manner and impart a good flavor, the
above content is usually 5% by weight or more and is preferably 10% by weight or more;
and is usually 50% by weight or less and is preferably 15% by weight or more and 25%
by weight or less of the total amount of the tobacco filler.
[0079] The tobacco rod portion 11 may have a fitting portion to which, for example, a heater
member used for heating the non-combustion-heating-type tobacco can be fit.
[0080] The tobacco rod portion 11, which includes a tobacco filler and a wrapping paper
with which the tobacco filler is wrapped, preferably has a pillar-like shape. In this
case, the aspect ratio that is the ratio of the height of the tobacco rod portion
11 in the longitudinal direction to the width of the bottom of the tobacco rod portion
11 is preferably 1 or more.
[0081] The shape of the bottom may be, but not limited to, a polygonal shape, a polygonal
shape having rounded corners, a circular shape, or an oval shape. When the bottom
has a circular shape, the above width is the diameter of the circle. When the bottom
has an oval shape, the width is the major-axis length of the oval. When the bottom
has a polygonal shape or a polygonal shape having rounded corners, the width is the
diameter of the circle circumscribing the polygon or the major-axis length of the
oval circumscribing the polygon. The height of the tobacco filler constituting the
tobacco rod portion 11 is preferably about 10 to 70 mm. The width of the tobacco filler
is preferably about 4 to 9 mm.
[0082] The length of the tobacco rod portion 11 in the longitudinal direction may be changed
appropriately in accordance with the size of the product. The above length is usually
10 mm or more, is preferably 12 mm or more, is more preferably 15 mm or more, and
is further preferably 18 mm or more. The above length is usually 70 mm or less, is
preferably 50 mm or less, is more preferably 30 mm or less, and is further preferably
25 mm or less. In consideration of the balance between the amount of delivery and
aerosol temperature, the proportion of the length of the tobacco rod portion 11 to
the length h of the non-combustion-heating-type tobacco 10 in the longitudinal direction
is usually 10% or more, is preferably 20% or more, is more preferably 25% or more,
and is further preferably 30% or more. The above proportion is usually 60% or less,
is preferably 50% or less, is more preferably 45% or less, and is further preferably
40% or less.
(Wrapping Paper)
[0083] The wrapping paper is not limited, and a common wrapping paper may be employed. Examples
of the wrapping paper include a wrapping paper that includes pulp as a principal component.
The wrapping paper may be a wrapping paper made of a wood pulp, such as a conifer
wood pulp or a broadleaf wood pulp, or a wrapping paper made of pulp mixture further
including a nonwood pulp commonly used for producing wrapping paper for tobacco products,
such as a flax pulp, a cannabis pulp, a sisal hemp pulp, or an esparto pulp.
[0084] Examples of the pulp that can be used include a chemical pulp, a ground pulp, a chemiground
pulp, or a thermomechanical pulp, which are produced by kraft cooking, acidic, neutral,
or alkaline sulfite cooking, sodium salt cooking, or the like.
[0085] A wrapping paper is produced with a fourdrinier paper machine, a cylinder paper machine,
a cylinder-tanmo hybrid paper machine, or the like using the pulp. In the papermaking
step, the formation is arranged and homogenization is performed. As needed, a wet
strength agent may be added to impart water resistance to the wrapping paper. In another
case, a sizing agent may be added to adjust the manner in which printing is performed
on the wrapping paper. Furthermore, aluminum sulfate, various anionic, cationic, nonionic,
and zwitterionic internal agents for papermaking, such as a yield improver, a freeness
improver, and a strength agent, and papermaking additives, such as a dye, a pH-controlling
agent, an antifoaming agent, a pitch-controlling agent, and a slime-controlling agent,
can also be added.
[0086] The basis weight of the base paper for the wrapping paper is, for example, usually
20 gsm or more and is preferably 25 gsm or more. The above basis weight is usually
65 gsm or less, is preferably 50 gsm or less, and is further preferably 45 gsm or
less.
[0087] The thickness of the wrapping paper having the above properties is not limited. In
consideration of stiffness, air permeability, and ease of control during papermaking,
the above thickness is usually 10 µm or more, is preferably 20 µm or more, and is
more preferably 30 µm or more. The above thickness is usually 100 µm or less, is preferably
75 µm or less, and is more preferably 50 µm or less.
[0088] Examples of the shape of the wrapping paper included in the non-combustion-heating-type
tobacco include square and rectangular.
[0089] In the case where the wrapping paper is used for wrapping the tobacco filler (for
preparing the tobacco rod portion), the length of a side of the wrapping paper is,
for example, about 12 to 70 mm. The length of the other side is, for example, 15 to
28 mm, is preferably 22 to 24 mm, and is further preferably about 23 mm. When the
tobacco filler is wrapped with the wrapping paper to form a pillar-shaped body, for
example, an edge portion of the wrapping paper which extends about 2 mm from one of
the edges of the wrapping paper in the w-direction is bonded to the other edge portion
with a glue such that they overlap each other. As a result, the wrapping paper is
formed into a pillar-shaped paper tube, in which the tobacco filler is filled. The
size of the rectangular wrapping paper can be determined in accordance with the size
of the final tobacco rod portion 11.
[0090] In the case where the wrapping paper is wrapped around the tobacco rod portion 11
and another member arranged adjacent to the tobacco rod portion 11 such that they
are connected to each other like a tipping paper, the length of a side of the wrapping
paper is, for example, 20 to 60 mm. The length of the other side is, for example,
15 to 28 mm.
[0091] The wrapping paper may include a filler in addition to the above pulp. The content
of the filler is, for example, 10% by weight or more and less than 60% by weight and
is preferably 15% by weight or more and 45% by weight or less of the total weight
of the wrapping paper.
[0092] The content of the filler in the wrapping paper is preferably 15% by weight or more
and 45% by weight or less when the basis weight falls within the preferable range
(25 gsm or more and 45 gsm or less).
[0093] When the basis weight is 25 gsm or more and 35 gsm or less, the above filler content
is preferably 15% by weight or more and 45% by weight or less. When the basis weight
is more than 35 gsm and 45 gsm or less, the above filler content is preferably 25%
by weight or more and 45% by weight or less.
[0094] Examples of the filler include calcium carbonate, titanium dioxide, and kaolin. For
example, in order to enhance a flavor and brightness, calcium carbonate is preferably
used.
[0095] Various agents may be added to the wrapping paper in addition to the base paper and
the filler. For example, a water resistance improver may be added in order to enhance
water resistance. Examples of the water resistance improver include a wet strength
agent (WS agent) and a sizing agent. Examples of the wet strength agent include a
urea formaldehyde resin, a melamine formaldehyde resin, and polyamide epichlorohydrin
(PAE). Examples of the sizing agent include a rosin soap, alkyl ketene dimer (AKD),
alkenylsuccinic anhydride (ASA), and highly saponified polyvinyl alcohol having a
degree of saponification of 90% or more.
[0096] A strength agent may be added as an agent. Examples of the strength agent include
polyacrylamide, a cationic starch, an oxidized starch, CMC, a polyamide epichlorohydrin
resin, and polyvinyl alcohol. In particular, it is known that the use of a trace amount
of oxidized starch enhances air permeability (
Japanese Unexamined Patent Application Publication No. 2017-218699).
[0097] The wrapping paper may be coated as needed.
[0098] A coating agent may be applied onto at least one of the two surfaces, that is, the
front and rear surfaces, of the wrapping paper. The coating agent is not limited.
It is preferable to use a coating agent capable of forming a film on the surface of
the paper and thereby reducing the permeability of the paper to liquids. Examples
thereof include alginic acid and salts thereof (e.g., sodium salt), polysaccharides,
such as pectin, cellulose derivatives, such as ethyl cellulose, methyl cellulose,
carboxymethyl cellulose, and nitro cellulose, and starch and derivatives thereof (e.g.,
ether derivatives, such as a carboxymethyl starch, a hydroxyalkyl starch, and a cationic
starch, and ester derivatives, such as starch acetate, starch phosphate, and starch
octenylsuccinate).
[Tipping Paper]
[0099] The tipping paper 15 is not limited and may be a common one, such as paper including
pulp as a principal component. The paper may be paper made of a wood pulp, such as
a conifer wood pulp or a broadleaf wood pulp, or paper made of pulp mixture further
including nonwood pulp commonly used for producing wrapping paper for tobacco items,
such as a flax pulp, a cannabis pulp, a sisal hemp pulp, or an esparto pulp. The above
pulp materials may be used alone. Alternatively, a plurality of types of pulp materials
may be used in combination at any ratio.
[0100] The tipping paper 15 may be constituted by one sheet or a plurality of sheets.
[0101] Examples of the pulp materials that can be used include a chemical pulp, a ground
pulp, a chemiground pulp, and a thermomechanical pulp, which are produced by kraft
cooking, acidic, neutral, or alkaline sulfite cooking, sodium salt cooking, or the
like.
[0102] The tipping paper 15 may be either a tipping paper produced by the production method
described below or a commercial tipping paper.
[0103] The shape of the tipping paper 15 is not limited. The tipping paper 15 may be, for
example, square or rectangle.
[0104] The basis weight of the tipping paper 15 is usually, but not limited to, 32 gsm or
more and 40 gsm or less, is preferably 33 gsm or more and 39 gsm or less, and is more
preferably 34 gsm or more and 38 gsm or less.
[0105] The air permeability of the tipping paper 15 is usually, but not limited to, 0 CORESTA
unit or more and 30000 CORESTA unit or less and is preferably more than 0 CORESTA
unit and 10000 CORESTA unit or less. The term "air permeability" used herein refers
to a value measured in conformity with ISO 2965:2009. Air permeability is expressed
as an amount (cm
3) of gas that passes through an area of 1 cm
2 per minute when a pressure difference between the surfaces of the paper is 1 kPa.
Note that 1 CORESTA unit (1 C.U.) is cm
3/(min·cm
2) at 1 kPa.
[0106] The tipping paper 15 may contain a filler in addition to the above pulp. Examples
thereof include metal carbonates, such as calcium carbonate and magnesium carbonate,
metal oxides, such as titanium oxide, titanium dioxide, and aluminum oxide, metal
sulfates, such as barium sulfate and calcium sulfate, metal sulfides, such as zinc
sulfide, quartz, kaolin, talc, diatomaceous earth, and gypsum. In order to enhance
brightness and opacity and increase heating rate, it is particularly preferable that
tipping paper 15 include calcium carbonate. The above fillers may be used alone or
in combination of two or more.
[0107] Various agents may be added to the tipping paper 15 in addition to the above pulp
and the above filler. For example, the tipping paper 15 may include a water resistance
improver in order to enhance. Examples of the water resistance improver include a
wet strength agent (WS agent) and a sizing agent. Examples of the wet strength agent
include a urea formaldehyde resin, a melamine formaldehyde resin, and polyamide epichlorohydrin
(PAE). Examples of the sizing agent include a rosin soap, an alkyl ketene dimer (AKD),
alkenylsuccinic anhydride (ASA), and highly saponified polyvinyl alcohol having a
degree of saponification of 90% or more.
[0108] A coating agent may be added onto at least one of the front and rear surfaces of
the tipping paper 15. The coating agent is not limited and is preferably a coating
agent with which a film can be formed on the surface of the paper and which thereby
reduces liquid permeability.
[0109] Although the structure of the non-combustion-heating-type tobacco according to this
embodiment can be applied to the electric heating tobacco product described below,
it can also be applied to cigarettes (paper-wrapped tobaccos), which involve combustion.
[Method for Producing Non-Combustion-Heating-Type Tobacco]
[0110] The method for producing the above-described non-combustion-heating-type tobacco
is not limited; publicly known methods may be used. For example, the non-combustion-heating-type
tobacco can be produced by wrapping the tipping paper around the tobacco rod portion
and the mouthpiece portion.
<Electric Heating Tobacco Product>
[0111] An electric heating tobacco product according to another embodiment of the present
invention (also referred to simply as "electric heating tobacco product") is an electric
heating tobacco product constituted by an electric heating device including a heater
member, a battery unit that serves as a power source for the heater member, and a
control unit that controls the heater member and the above-described non-combustion-heating-type
tobacco inserted in the electric heating device so as to come into contact with the
heater member.
[0112] The electric heating tobacco product may be an electric heating tobacco product that
heats the outer circumferential surface of the non-combustion-heating-type tobacco
10 as illustrated in Fig. 2 or an electric heating tobacco product that heats the
inside of the tobacco rod portion 11 of the non-combustion-heating-type tobacco 10
as illustrated in Fig. 3. Note that, although air introduction holes are formed in
the electric heating devices 20 illustrated in Figs. 2 and 3, they are not illustrated
in the drawings. An electric heating tobacco product 30 is described below with reference
to Fig. 3. In the non-combustion-heating-type tobaccos 10 illustrated in Figs. 2 and
3, reference numerals that denote the components illustrated in Figs. 2 and 3 are
partially omitted.
[0113] When an electric heating tobacco product 30 is used, the above-described non-combustion-heating-type
tobacco 10 is inserted into an electric heating device 20 so as to come into contact
with a heater member 21 disposed in the electric heating device 20.
[0114] The electric heating device 20 includes a body 24 formed of a resin or the like and
a battery unit 22 and a control unit 23 that are disposed inside the body 24.
[0115] When the non-combustion-heating-type tobacco 10 is inserted into the electric heating
device 20, the outer circumferential surface of the tobacco rod portion 11 is brought
into contact with the heater member 21 of the electric heating device 20 and, subsequently,
the entirety of the outer circumferential surface of the tobacco rod portion 11 and
a part of the outer circumferential surface of the tipping paper are brought into
contact with the heater member 21.
[0116] The heater member 21 of the electric heating device 20 produces heat due to the control
performed by the control unit 23. As a result of the heat transferring to the tobacco
rod portion 11 of the non-combustion-heating-type tobacco 10, the aerosol-source material,
flavor component, and the like included in the tobacco filler of the tobacco rod portion
11 become volatilized.
[0117] The heater member 21 may be, for example, a sheet-shaped heater, a tabular heater,
or a tubular heater. The sheet-shaped heater is a flexible, sheet-shaped heater. Examples
thereof include a heater including a film (thickness: about 20 to 225 µm) formed of
a heat-resistant polymer, such as polyimide. The tabular heater is a stiff, flat sheet-shaped
heater (thickness: about 200 to 500 µm). Examples thereof include a heater that includes,
for example, a flat-sheet substrate and a resistance circuit disposed on the substrate,
the resistance circuit serving as a heat-producing portion. The tubular heater is
a hollow or solid tube-shaped heater (thickness: about 200 to 500 µm). Examples thereof
include a heater that includes, for example, a cylinder made of a metal or the like
and a resistance circuit formed on the outer periphery of the cylinder, the resistance
circuit serving as a heat-producing portion. Examples of the tubular heater further
include rod-shaped and cone-shaped heaters made of a metal or the like which include
an internal resistance circuit that serves as a heat-producing portion. The cross-sectional
shape of the tubular heater taken in the circumferential direction may be, for example,
a circular shape, an oval shape, a polygonal shape, or the shape of a polygon with
rounded corners.
[0118] In the case where the electric heating tobacco product is an electric heating tobacco
product that heats the outer circumferential surface of the non-combustion-heating-type
tobacco 10 as illustrated in Fig. 2, the sheet-shaped heater, the tabular heater,
and the tubular heater can be used. In the case where the electric heating tobacco
product is an electric heating tobacco product that heats the inside of the tobacco
rod portion 11 included in the non-combustion-heating-type tobacco 10 as illustrated
in Fig. 3, the tabular heater, the pillar-shaped heater, and the cone-shaped heater
can be used.
[0119] The length of the heater member 21 in the longitudinal direction may fall within
the range of L ± 5.0 mm, where L [mm] represents the length of the tobacco rod portion
11 in the longitudinal direction. In order to transfer heat to the tobacco rod portion
11 in a sufficient manner and cause the aerosol-source material, flavor component,
and the like included in the tobacco filler to volatilize to a sufficient degree,
that is, in consideration of aerosol delivery, the length of the heater member 21
in the longitudinal direction is preferably L mm or more. In order to reduce the generation
of components that adversely affect the flavor and the like, the above length is preferably
L + 0.5 mm or less, L + 1.0 mm or less, L + 1.5 mm or less, L + 2.0 mm or less, L
+ 2.5 mm or less, L + 3.0 mm or less, L + 3.5 mm or less, L + 4.0 mm or less, L +
4.5 mm or less, or L + 5.0 mm or less.
[0120] The heating intensity, such as the amount of heating time during which the heater
member 21 heats the non-combustion-heating-type tobacco 10 and the heating temperature
at which the heater member 21 heats the non-combustion-heating-type tobacco 10, can
be predetermined for each electric heating tobacco product 30. For example, the heating
intensity can be predetermined such that, after the non-combustion-heating-type tobacco
10 has been inserted into the electric heating device 20, preheating is performed
for a predetermined period of time to increase the temperature of the outer circumferential
surface of the portion of the non-combustion-heating-type tobacco 10 which is inserted
in the electric heating device 20 to X(°C) and the temperature is subsequently maintained
to be a certain temperature equal to or less than X(°C).
[0121] The temperature X(°C) is preferably 80°C or more and 400°C or less in consideration
of the amount of the delivered components generated by heating or the like. Specifically,
the temperature X(°C) can be 80°C, 90°C, 100°C, 110°C, 120°C, 130°C, 140°C, 150°C,
160°C, 170°C, 180°C, 190°C, 200°C, 210°C, 220°C, 230°C, 240°C, 250°C, 260°C, 270°C,
280°C, 290°C, 300°C, 310°C, 320°C, 330°C, 340°C, 350°C, 360°C, 370°C, 380°C, 390°C,
or 400°C.
[0122] A vapor including components derived from the aerosol-source material, components
derived from the flavor component, etc. which are generated from the tobacco rod portion
11 as a result of heating performed by the heater member 21 is delivered into the
oral cavity of the user through the mouthpiece portion 14, which is constituted by
the cooling segment 12, the filter segment 13, etc.
[0123] In order to facilitate the entry of outside air and reduce the likelihood of the
components generated by heating and air being retained inside the cooling segment
12, the perforations V formed in the cooling segment 12 are preferably present at
a position closer to the mouth end than the mouth end side end (the position denoted
by the arrow X in the drawing) of a region of the cooling segment 12 which comes into
contact with the electric heating device 20, as illustrated in Fig. 4. The insertion
opening of the electric heating device 20 through which the non-combustion-heating-type
tobacco 10 is inserted into the electric heating device 20 may be tapered as illustrated
in Fig. 5 in order to make it easy to insert the non-combustion-heating-type tobacco
10 into the electric heating device 20. In this case, the mouth end side end of a
region of the cooling segment 12 which comes into contact with the electric heating
device 20 is the position denoted by the arrow Y in the drawing. In the non-combustion-heating-type
tobaccos 10 illustrated in Figs. 4 and 5, reference numerals that denote the components
illustrated in Figs. 1 to 3 are partially omitted.
EXAMPLES
[0124] The present invention is described further specifically with reference to Examples
below. The present invention is not limited by the following description of Examples
without departing from the summary thereof.
[0125] <Preparation of Non-Combustion-Heating-Type Tobacco>
[Example 1]
[0126] A mixture of 15 g/100 g of glycerine, 4 g/100 g of propylene glycol, and shredded
sheet tobacco was prepared as a tobacco filler. Using a high-speed wrapping machine,
the tobacco filler was wrapped with a wrapping paper (produced by Nippon Paper Papylia
Co., Ltd., basis weight: 35 g/m
2, thickness: 52 µm).
[0127] The weight of shreds per stick was 0.8 g. The perimeter of the stick was 22 mm. The
length of the stick was 68 mm .
[0128] For each standard, 200 wrapped tobacco rod portions were charged into a plastic closed
container and stored.
[0129] One of the stored tobacco rod portions was cut to a length of 20 mm. Subsequently,
the tobacco rod portion, a paper tube having a length of 20 mm, a center hole having
a length of 12 mm with a through-hole (diameter: 4.5 mm), and a filter element (density:
0.122 g/cm
3, compression change P (hereinafter, referred to as "hardness"): 88%) that had a length
of 8 mm and was composed of cellulose acetate fibers (filament denier (g/9000m): 12;
total denier (g/9000m): 28000), the cross section of which in the circumferential
direction was Y-shaped, were wrapped with the tipping paper prepared above. Hereby,
a non-combustion-heating-type tobacco having no perforations was prepared. Then, 17
holes were formed concentrically in the circumferential direction of the paper tube
at positions 5.5 mm from the boundary between the paper tube and the center hole filter
(25.5 mm from the mouth end side end of the non-combustion-heating-type tobacco) toward
the paper tube so as to penetrate both tipping paper and the paper tube. Hereby, perforations
were formed, and a non-combustion-heating-type tobacco of Example 1 was prepared.
The airflow resistance of the filter segment of the non-combustion-heating-type tobacco
in the longitudinal direction was 1.35 mmH
2O/mm.
[0130] Note that the compression change P (hardness) of the filter element, which is represented
by Formula (1) above, was measured using, for example, SODIM-H Hardness module represented
by Sodim SAS. The same applies to all of the examples and comparative examples below.
[Comparative Example 1]
[0131] A non-combustion-heating-type tobacco of Comparative Example 1 was prepared as in
the preparation of the non-combustion-heating-type tobacco of Example 1, except that
the filter element (density: 0.122 g/cm
3) having a filament denier (g/9000m) of 12 and a total denier (g/9000m) of 28000 was
changed to a filter element (density: 0.143 g/cm
3, hardness: 87%) having a filament denier (g/9000m) of 5.9 and a total denier (g/9000m)
of 35000. The airflow resistance of the filter segment included in the non-combustion-heating-type
tobacco in the longitudinal direction was 2.62 mmH
2O/mm.
[Example 2]
[0132] A non-combustion-heating-type tobacco of Example 2 was prepared as in the preparation
of the non-combustion-heating-type tobacco of Example 1, except that flavoring agent
capsules (spherical shape having a diameter of 3.5 mm; the same applies to the flavoring
agent capsules used in the other examples and comparative examples) including menthol
were disposed inside the filter element, the length of the center hole was changed
from 12 mm to 8 mm, and the length of the filter element was changed from 8 mm to
12 mm. The density of the filter segment included in the non-combustion-heating-type
tobacco (density excluding the flavoring agent capsules), the hardness of the filter
segment, and the airflow resistance of the filter segment in the longitudinal direction
were 0.122 g/cm
3, 88%, and 1.93 mmH
2O/mm, respectively. Note that the parameters related to the filter segment were determined
without crushing the flavoring agent capsules. The same applies to the other examples
and comparative examples where flavoring agent capsules were used.
[Example 3]
[0133] A non-combustion-heating-type tobacco of Example 3 was prepared as in the preparation
of the non-combustion-heating-type tobacco of Example 1, except that the filter element
(density: 0.122 g/cm
3) having a filament denier (g/9000m) of 12 and a total denier (g/9000m) of 28000 was
changed to a filter element (density: 0.119 g/cm
3, hardness: 89%) having a filament denier (g/9000m) of 8 and a total denier (g/9000m)
of 28000. The airflow resistance of the filter segment included in the non-combustion-heating-type
tobacco in the longitudinal direction was 1.69 mmH
2O/mm.
[Example 4]
[0134] A non-combustion-heating-type tobacco of Example 4 was prepared as in the preparation
of the non-combustion-heating-type tobacco of Example 1, except that the flavoring
agent capsules including menthol were disposed inside the filter element, the length
of the center hole was changed from 12 mm to 8 mm, the length of the filter element
was changed from 8 mm to 12 mm, and the filter element (density: 0.122 g/cm
3, hardness: 88%) having a filament denier (g/9000m) of 12 and a total denier (g/9000m)
of 28000 was changed to a filter element (density: 0.123 g/cm
3, hardness: 91%) having a filament denier (g/9000m) of 8 and a total denier (g/9000m)
of 28000. The airflow resistance of the filter segment included in the non-combustion-heating-type
tobacco in the longitudinal direction was 2.76 mmH
2O/mm.
[Example 5]
[0135] A non-combustion-heating-type tobacco of Example 5 was prepared as in the preparation
of the non-combustion-heating-type tobacco of Example 1, except that the length of
the center hole was changed from 12 mm to 6 mm, and the length of the filter element
was changed from 8 mm to 14 mm. The density of the filter segment included in the
non-combustion-heating-type tobacco, the hardness of the filter segment, and the airflow
resistance of the filter segment in the longitudinal direction were 0.129 g/cm
3, 90%, and 1.58 mmH
2O/mm, respectively.
[Example 6]
[0136] A non-combustion-heating-type tobacco of Example 6 was prepared as in the preparation
of the non-combustion-heating-type tobacco of Example 1, except that the length of
the center hole was changed from 12 mm to 6 mm, the length of the filter element was
changed from 8 mm to 14 mm, and the filter element (density: 0.122 g/cm
3, hardness: 88%) having a filament denier (g/9000m) of 12 and a total denier (g/9000m)
of 28000 was changed to a filter element (density: 0.119 g/cm
3, hardness: 89%) having a filament denier (g/9000m) of 8 and a total denier (g/9000m)
of 28000. The airflow resistance of the filter segment included in the non-combustion-heating-type
tobacco in the longitudinal direction was 1.69 mmH
2O/mm.
[Example 7]
[0137] A non-combustion-heating-type tobacco of Example 7 was prepared as in the preparation
of the non-combustion-heating-type tobacco of Example 1, except that the flavoring
agent capsules including menthol were disposed inside the filter element, 6 mg/12mm
of menthol was added to the filter element, the length of the center hole was changed
from 12 mm to 8 mm, and the length of the filter element was changed from 8 mm to
12 mm. The density of the filter segment included in the non-combustion-heating-type
tobacco (density excluding the flavoring agent capsules), the hardness of the filter
segment, and the airflow resistance of the filter segment in the longitudinal direction
were 0.122 g/cm
3, 91%, and 2.48 mmH
2O/mm, respectively.
[Comparative Example 2]
[0138] A non-combustion-heating-type tobacco of Comparative Example 2 was prepared as in
the preparation of the non-combustion-heating-type tobacco of Example 1, except that
the flavoring agent capsules including menthol were disposed inside the filter element,
6 mg/12mm of menthol was added to the filter element, the length of the center hole
was changed from 12 mm to 8 mm, the length of the filter element was changed from
8 mm to 12 mm, and the filter element (density: 0.122 g/cm
3, hardness: 88%) having a filament denier (g/9000m) of 12 and a total denier (g/9000m)
of 28000 was changed to a filter element (density (density excluding the flavoring
agent capsules): 0.152 g/cm
3, hardness: 94%) having a filament denier (g/9000m) of 5.9 and a total denier (g/9000m)
of 35000. The airflow resistance of the filter segment included in the non-combustion-heating-type
tobacco in the longitudinal direction was 6.23 mmH
2O/mm.
[Comparative Example 3]
[0139] A non-combustion-heating-type tobacco of Comparative Example 3 was prepared as in
the preparation of the non-combustion-heating-type tobacco of Example 1, except that
the filter element (density: 0.122 g/cm
3) having a filament denier (g/9000m) of 12 and a total denier (g/9000m) of 28000 was
changed to a filter element (density: 0.113 g/cm
3, hardness: 85%) having a filament denier (g/9000m) of 20 and a total denier (g/9000m)
of 25000. The airflow resistance of the filter segment included in the non-combustion-heating-type
tobacco in the longitudinal direction was 0.80 mmH
2O/mm. In Comparative Example 3, the evaluation of the amount of delivery was not conducted
because the non-combustion-heating-type tobacco of Comparative Example 3 did not have
a sufficient degree of hardness.
[0140] Table 1 summarizes the production conditions and properties of each of the non-combustion-heating-type
tobaccos prepared in Examples above.
[Table 1]
|
|
Example 1 |
Comparative Example 1 |
Example 2 |
Example 3 |
Example 4 |
Example 5 |
Example 6 |
Example 7 |
Comparative Example 2 |
Comparative Example 3 |
Glycerine |
(g/100g) |
15 |
is |
15 |
15 |
15 |
15 |
15 |
15 |
15 |
15 |
Propylene glycol |
(g/100g) |
4 |
4 |
4 |
4 |
4 |
4 |
4 |
4 |
4 |
4 |
Wrapping paper |
Basis weight (g/m2) |
35 |
35 |
35 |
35 |
35 |
35 |
35 |
35 |
35 |
35 |
Thickness (µm) |
52 |
52 |
52 |
52 |
52 |
52 |
52 |
52 |
52 |
52 |
Weight of shreds |
(g) |
0.8 |
0.8 |
0.8 |
0.8 |
0.8 |
0.8 |
0.8 |
0.8 |
0.8 |
0.8 |
Perimeter of stick |
(mm) |
22 |
22 |
22 |
22 |
22 |
22 |
22 |
22 |
22 |
22 |
Length of stick |
(mm) |
68 |
68 |
68 |
68 |
68 |
68 |
68 |
68 |
68 |
68 |
Length of flavor-generating segment |
(mm) |
20 |
20 |
20 |
20 |
20 |
20 |
20 |
20 |
20 |
20 |
Length of paper tube |
(mm) |
20 |
20 |
20 |
20 |
20 |
20 |
20 |
20 |
20 |
20 |
Center hole |
Length (mm) |
12 |
12 |
8 |
12 |
8 |
6 |
6 |
8 |
8 |
12 |
Inside diameter (mm) |
4.5 |
4.5 |
4.5 |
4.5 |
4.5 |
4.5 |
4.5 |
4.5 |
4.5 |
4.5 |
Filter element |
Length (mm) |
8 |
8 |
12 |
8 |
12 |
14 |
14 |
12 |
12 |
8 |
Filament denier (-) |
12 |
5.9 |
12 |
8 |
8 |
12 |
8 |
12 |
5.9 |
20 |
Total denier (-) |
28000 |
35000 |
28000 |
28000 |
28000 |
28000 |
28000 |
28000 |
35000 |
25000 |
Density (g/cm3) |
0.122 |
0.143 |
0.122 |
0.119 |
0.123 |
0.129 |
0.119 |
0.122 |
0.152 |
0.113 |
Airflow resistance (mmH2O/mm) |
1.35 |
2.62 |
1.93 |
1.69 |
2.76 |
1.58 |
1.69 |
2.48 |
6.23 |
0.80 |
Addition of menthol |
No |
No |
No |
No |
No |
No |
No |
Yes |
Yes |
No |
Addition of capsules |
No |
No |
Yes |
No |
Yes |
No |
No |
Yes |
Yes |
No |
Compression change P |
(%) |
88 |
87 |
88 |
89 |
91 |
90 |
89 |
91 |
94 |
85 |
<Evaluation of Amount Delivered>
[0141] Each of the non-combustion-heating-type tobaccos prepared in Examples 1 to 7 and
Comparative Examples 1 to 3 was subjected to a smoking test in order to evaluate the
amounts of the delivered components generated by heating.
[0142] The smoking test was conducted under the following conditions in accordance with
Canadian Intense Smoking (CIR).
[0143] Using an electric heating device capable of peripheral heating, after the non-combustion-heating-type
tobacco had been inserted into the electric heating device, the heater temperature
was increased to 295°C within 21 seconds and then reduced to 260°C within 5 seconds.
Subsequently, the temperature was maintained at 260°C until the evaluation was completed
(for about 330 seconds). Then, in the smoking test, automated smoking was performed
using a single-port automated smoking machine produced by Borgwaldt at a flow rate
of 55 cc/2 sec and smoking intervals of 30 sec. In this test, the positions of the
perforations formed in the cooling segment were adjusted to be 25.5 mm from the mouth
end side end of the region of the non-combustion-heating-type tobacco which came into
contact with the electric heating device. The mainstream smoke generated in the smoking
test was collected with a Cambridge pad. After a puff action had been performed 12
times as for Examples 1 to 6 and Comparative Example 1 and 10 times as for Examples
7 and 8 and Comparative Examples 2 and 3, the Cambridge pad was removed and extraction
was performed with 10 mL of ethanol. The amounts of the components included in the
mainstream smoke which were taken by the puff actions were measured by GC-MS.
[0144] Tables 2 and 3 list and Figs. 6 to 9 illustrate the measures of the components of
the mainstream smoke, that is, the amounts of nicotine and glycerine included in the
mainstream smoke generated from each of the non-combustion-heating-type tobaccos prepared
in Examples 1 to 9 and Comparative Example 1 which were obtained by the above measurement.
Specifically, Fig. 6 illustrates the results obtained in Examples 1 and 3 and Comparative
Example 1 (studies of impacts of fiber denier under the following conditions: use
of capsules: No, use of menthol: No, center hole length: filter segment length = 12:8),
Fig. 7 illustrates the results obtained in Example 7 and Comparative Example 2 (studies
of impacts of fiber denier under the following conditions: use of capsules: Yes, use
of menthol: Yes, center hole length: filter segment length = 8:12), Fig. 8 illustrates
the results obtained in Examples 2 and 4 (studies of impacts of fiber denier under
the following conditions: use of capsules: Yes, use of menthol: No, center hole length:
filter segment length = 12:8), and Fig. 9 illustrates the results obtained in Examples
5 and 6 (studies of impacts of filament denier under the following conditions: use
of capsules: No, use of menthol: No, center hole length: filter segment length = 6:14).
Note that, in some of the examples and comparative examples where the capsules were
used, the above evaluations were conducted after the flavoring agent capsules had
been crushed.
[Table 2]
|
Puff (number of times) |
1 |
2 |
3 |
4 |
5 |
6 |
7 |
8 |
9 |
10 |
Total |
Nicotine (mg) |
Example 1 |
0.041 |
0.123 |
0.210 |
0.165 |
0.121 |
0.096 |
0.081 |
0.073 |
0.065 |
0.060 |
1.035 |
Comparative Example 1 |
0.024 |
0.082 |
0.152 |
0.141 |
0.112 |
0.089 |
0.074 |
0.065 |
0.059 |
0.055 |
0.852 |
Example 2 |
0.014 |
0.072 |
0.166 |
0.151 |
0.109 |
0.084 |
0.070 |
0.062 |
0.056 |
0.051 |
0.836 |
Example 3 |
0.034 |
0.117 |
0.182 |
0.153 |
0.114 |
0.092 |
0.078 |
0.068 |
0.062 |
0.057 |
0.957 |
Example 4 |
0.010 |
0.045 |
0.114 |
0.128 |
0.107 |
0.088 |
0.073 |
0.063 |
0.055 |
0.049 |
0.732 |
Example 5 |
0.021 |
0.096 |
0.187 |
0.155 |
0.111 |
0.089 |
0.075 |
0.067 |
0.061 |
0.055 |
0.916 |
Example 6 |
0.019 |
0.081 |
0.175 |
0.155 |
0.124 |
0.098 |
0.080 |
0.069 |
0.061 |
0.054 |
0.917 |
Example 7 |
0.014 |
0.082 |
0.168 |
0.172 |
0.144 |
0.118 |
0.093 |
0.082 |
0.075 |
0.069 |
1.017 |
Comparative Example 2 |
0.005 |
0.041 |
0.090 |
0.103 |
0.104 |
0.089 |
0.079 |
0.070 |
0.062 |
0.057 |
0.701 |
[Table 3]
|
Puff (number of times) |
1 |
2 |
3 |
4 |
5 |
6 |
7 |
8 |
9 |
10 |
Total |
Glycerine (mg) |
Example 1 |
0.366 |
0.882 |
1.808 |
1.743 |
1.266 |
0.934 |
0.736 |
0.600 |
0.509 |
0.440 |
9.283 |
Comparative Example 1 |
0.209 |
0.569 |
1.120 |
1.275 |
1.055 |
0.809 |
0.634 |
0.533 |
0.462 |
0.403 |
7.070 |
Example 2 |
0.234 |
0.947 |
2.227 |
2.340 |
1.564 |
1.043 |
0.765 |
0.601 |
0.511 |
0.442 |
10.675 |
Example 3 |
0.336 |
0.996 |
1.571 |
1.575 |
1.169 |
0.892 |
0.706 |
0.585 |
0.506 |
0.448 |
8.683 |
Example 4 |
0.194 |
0.621 |
1.469 |
1.736 |
1.434 |
1.033 |
0.788 |
0.613 |
0.492 |
0.402 |
8.782 |
Example 5 |
0.322 |
0.981 |
2.065 |
2.068 |
1.425 |
1.001 |
0.760 |
0.602 |
0.514 |
0.434 |
10.173 |
Example 6 |
0.277 |
0.803 |
1.742 |
1.809 |
1.468 |
1.082 |
0.823 |
0.650 |
0.542 |
0.448 |
9.643 |
Example 7 |
0.148 |
0.604 |
1.422 |
1.546 |
1.275 |
0.846 |
0.598 |
0.479 |
0.413 |
0.356 |
7.687 |
Comparative Example 2 |
0.107 |
0.332 |
0.694 |
0.899 |
0.815 |
0.640 |
0.513 |
0.423 |
0.352 |
0.303 |
5.080 |
[0145] The results listed in Tables 1 and 2 above and illustrated in Figs. 6 to 9 confirm
that, regardless of whether the flavoring agent capsules were added to the filter
element and whether menthol was added to the filter element, a non-combustion-heating-type
tobacco having a filament denier of 8 or more and 12 or less is superior to a non-combustion-heating-type
tobacco the short-fiber denier of which deviates from the above range, in terms of
the amounts of delivery of nicotine and glycerine, which are the measures of the amounts
of components of the mainstream smoke.
Reference Signs List
[0146]
- 10
- non-combustion-heating-type tobacco
- 11
- tobacco rod portion
- 12
- cooling segment
- 13
- filter segment
- 14
- mouthpiece portion
- 15
- tipping paper
- V
- perforation
- 20
- electric heating device
- 21
- heater member
- 22
- battery unit
- 23
- control unit
- 24
- body
- 30
- electric heating tobacco product