(19) |
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(11) |
EP 4 389 969 A8 |
(12) |
CORRECTED EUROPEAN PATENT APPLICATION |
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Note: Bibliography reflects the latest situation |
(15) |
Correction information: |
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Corrected version no 1 (W1 A1) |
(48) |
Corrigendum issued on: |
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07.08.2024 Bulletin 2024/32 |
(43) |
Date of publication: |
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26.06.2024 Bulletin 2024/26 |
(22) |
Date of filing: 14.11.2023 |
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(51) |
International Patent Classification (IPC):
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(84) |
Designated Contracting States: |
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AL AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HR HU IE IS IT LI LT LU LV MC ME MK MT
NL NO PL PT RO RS SE SI SK SM TR |
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Designated Extension States: |
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BA |
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Designated Validation States: |
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KH MA MD TN |
(30) |
Priority: |
28.11.2022 PL 44296422
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(71) |
Applicant: Uniwersytet Przyrodniczy w Poznaniu |
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60-637 Poznan (PL) |
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(72) |
Inventors: |
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- MAZELA, Bartlomiej
61-058 Poznan (PL)
- GRZESKOWIAK, Wojciech
62-023 Kamionki (PL)
- PERDOCH, Waldemar
63-006 Sródka (PL)
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(74) |
Representative: Augustyniak, Magdalena Anna et al |
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Polservice
Kancelaria Rzecznikow
Patentowych sp. z o.o.
Bluszczanska 73 00-712 Warszawa 00-712 Warszawa (PL) |
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(54) |
A METHOD OF PRODUCING A PLATE COMPOSITE WITH THE USE OF CELLULOSE AND CARBON PARTICLES
WITH INCREASED FIRE RESISTANCE |
(57) A method of producing a plate composite with the use of cellulose and carbon particles
with increased fire resistance is that
1.1. particles rich in elemental carbon, i.e. with a carbon content >90%, selected
from expanding graphite (EG) and carbon nanotubes (CNT), are dispersed in water in
weight ratios ranging from 0.2:1 to 1:0.2. in an aqueous system, the weight ratio
of carbon particles to water is from 1:1 to 100:1.
1.2. a cellulose pulp with a concentration of 1-25% in water is produced
1.3. a dispersed suspension of carbon particles is introduced into the cellulose pulp.
1.4. a composite is formed on a paper machine
1.5. the composite is dried and pressed
wherein the EG/CNT dispersion is kept in water for a period of 24 hours, and resulting
particle dispersion is homogenized for 30-45 s by means of a homogenizer with a rotation
speed from 400 to 4000 rpm until a homogeneous water dispersion is obtained and the
homogeneous the particle dispersion is added to the pulp produced in parallel in an
amount of 1-75% by weight based on the total mass of the product and the mixture is
further grounded for 10 s in the refiner, and cellulose pulp is produced in such a
way that the cellulose in the form of sheets is initially comminuted into particles
size 1-4 cm
2, soaked for 24 hours in deionized water, the weight ratio of cellulose to water is
1:10, and after 24 hours the cellulose is defibrated in a defiberizer and water is
added until the total cellulose to water ratio is at the level of 1:50, then the homogeneous
pulp is transferred to a sheet forming apparatus and diluted with water to a mass
concentration ranging from 2-20%, and cellulose-carbon sheets are formed.