TECHNICAL FIELD
[0001] The present invention relates to an extruded, multi-hole-pipe manufacturing method.
BACKGROUND ART
[0002] An extruded, multi-hole pipe comprises: an outer-wall portion, which constitutes
an outer-perimeter portion thereof; and partition portions, which partition spaces
surrounded by the outer-wall portion; and is formed such that a fluid can be caused
to flow through passageways surrounded by the outer-wall portion and the partition
portions. To form a complex, cross-sectional shape having such a fine structure by
extrusion, extruded, multi-hole pipes are often constituted from an aluminum alloy
having a relatively low alloying-element content and exceling in extrudability.
[0003] For example, in Patent Document 1, a heat-exchanger, extruded, flat, multi-hole pipe
excelling in corrosion resistance is described that is composed of an aluminum alloy
that contains, by mass%, Si: 0.01%-0.3%, Fe: 0.01%-0.3%, Cu: 0.05%-0.4%, Mn: 0.05%-0.3%,
Zr: 0.05%-0.25%, and Ti: 0%-0.15% and in which the total of Zr and Ti is 0.3% or less,
the remainder being composed of Al and unavoidable impurities, wherein, of the particles
having a particle surface area of 1.0 µm
2 or more that are dispersed in the matrix, the surface-area ratio occupied by an AlFeSi
stable phase is 0.1% or more and less than 0.5%.
PRIOR ART LITERATURE
Patent Documents
SUMMARY OF THE INVENTION
PROBLEMS TO BE SOLVED BY THE INVENTION
[0005] In recent years, owing to the increase in environmental awareness, the importance
of techniques to reuse aluminum scrap material as casting material has been increasing.
However, aluminum scrap material contains various elements other than aluminum. In
addition, depending on the situation, aluminum scrap material sometimes also contains
metal materials other than aluminum, such as iron. Consequently, in situations in
which aluminum scrap material is to be reused as a casting material, the content of
elements other than aluminum will increase, thereby leading to the occurrence of various
problems, such as an increase in deformation resistance during hot extrusion, a decrease
in extrusion speed, and the like. For this reason, according to the existing state
of the art, in situations in which aluminum scrap material is used as a casting material,
it is considered difficult to manufacture an extruded, multi-hole pipe having a complex,
cross-sectional shape.
[0006] The present invention was conceived considering this background, and an object of
the present invention is to provide an extruded, multi-hole-pipe manufacturing method
in which hot extrusion can be performed easily even in the situation in which the
content of elements other than aluminum is relatively high.
MEANS FOR SOLVING THE PROBLEMS
[0007] One aspect of the present invention is an extruded, multi-hole-pipe manufacturing
method, comprising:
preparing an ingot having a chemical composition that contains one or two or more
elements selected from the group consisting of Si (silicon): 2.00 mass% or less, Fe
(iron): 0.60 mass% or less, Cu (copper): 0.60 mass% or less, Mn (manganese): 2.00
mass% or less, Mg (magnesium): 0.40 mass% or less, Cr (chromium): 0.10 mass% or less,
Zn (zinc): 1.50 mass% or less, Ti (titanium): 0.10 mass% or less, and B (boron): 0.10
mass% or less, the remainder being composed of Al (aluminum) and unavoidable impurities,
wherein the total of the Si content and the Mn content is 3.20 mass% or less, and
the Si content is less than the Mn content;
performing a first homogenizing process by holding the ingot at a temperature of 550°C
or higher and 650°C or lower for 2 h or more;
subsequently performing a second homogenizing process by holding the ingot at a temperature
of 450°C or higher and 540°C or lower for 3 h or more; and
subsequently preparing an extruded, multi-hole pipe by performing hot extrusion on
the ingot.
EFFECTS OF THE INVENTION
[0008] In the above-mentioned extruded, multi-hole-pipe manufacturing method, the first
homogenizing process and the second homogenizing process are performed on an ingot
having a chemical composition within the above-mentioned specific ranges. Thus, by
performing the homogenizing process in two stages and by setting the hold temperature
and hold time of the homogenizing process in each stage to within the above-mentioned
specific ranges, respectively, an increase in deformation resistance during hot extrusion
can be curtailed even in the situation in which the content of elements other than
aluminum is relatively high.
[0009] According to the above-mentioned aspect as described above, it is possible to provide
an extruded, multi-hole-pipe manufacturing method in which hot extrusion can be performed
easily even in the situation in which the content of elements other than aluminum
is relatively high.
BRIEF DESCRIPTION OF THE DRAWINGS
[0010] FIG. 1 is an oblique view of an extruded, multi-hole pipe according to Working Example
1.
MODES FOR CARRYING OUT THE INVENTION
[0011] In the above-mentioned extruded, multi-hole-pipe manufacturing method, first, an
ingot having the above-mentioned specific chemical composition is prepared. The ingot
contains one or two or more elements selected from the group consisting of Si, Fe,
Cu, Mn, Mg, Cr, Zn, Ti, and B. These elements include casting materials such as aluminum
metals, aluminum scrap material, intermediate alloys, and the like. In the situation
in which aluminum scrap material is to be used as the casting material, the elements
described above may be derived principally from the aluminum scrap material.
· Si: 2.00 mass% or less
[0012] The ingot may contain greater than 0 mass% and 2.00 mass% or less of Si. Si is an
element that is contained in: aluminum metals; Si-containing aluminum alloys (e.g.,
4000-series alloy and 6000-series alloy) in aluminum scrap material; intermediate
alloys; and the like. Si acts to increase the strength of the extruded, multi-hole
pipe. From the viewpoint of further increasing the strength of the extruded, multi-hole
pipe, the Si content preferably is 0.20 mass% or more, more preferably is 0.40 mass%
or more, yet more preferably is 0.60 mass% or more, particularly preferably is 0.70
mass% or more, and most preferably is 0.80 mass% or more.
[0013] On the other hand, if the Si content becomes excessively high, there is a risk that
it will lead to an increase in the deformation resistance of the ingot during hot
extrusion, thereby decreasing extrudability. By making the Si content 2.00 mass% or
less, preferably 1.50 mass% or less, more preferably 1.40 mass% or less, and yet more
preferably 1.30 mass% or less, the strength of the extruded, multi-hole pipe can be
increased while curtailing an increase in the deformation resistance of the ingot
during hot extrusion.
· Mn: 2.00 mass% or less
[0014] The ingot may contain greater than 0 mass% and 2.00 mass% or less of Mn. Mn is an
element that is contained in: aluminum metals; Mn-containing aluminum alloys (e.g.,
3000-series alloy) in aluminum scrap material; intermediate alloys; and the like.
Mn acts to increase the strength of the extruded, multi-hole pipe. From the viewpoint
of further increasing the strength of the extruded, multi-hole pipe, the Mn content
preferably is 0.40 mass% or more, more preferably is 0.60 mass% or more, yet more
preferably is 0.80 mass% or more, particularly preferably is 0.9 mass% or more, and
most preferably is 1.00 mass% or more.
[0015] On the other hand, if the Mn content becomes excessively high, there is a risk that
it will lead to an increase in the deformation resistance of the ingot during hot
extrusion, thereby decreasing extrudability. By making the Mn content 2.00 mass% or
less, preferably 1.8 mass% or less, and more preferably 1.70 mass% or less, the strength
of the extruded, multi-hole pipe can be increased while curtailing an increase in
the deformation resistance of the ingot during hot extrusion.
[0016] In addition, the total of the Si content and the Mn content in the ingot is 3.20
mass% or less, and the Si content is lower than the Mn content. By adding Si and Mn
within the above-mentioned specific ranges to the chemical composition of the above-mentioned
ingot so as to satisfy the above-described relationship between the Si content and
the Mn content, it becomes possible to easily prepare an extruded, multi-hole pipe
having a complex, cross-sectional shape while more effectively curtailing an increase
in the deformation resistance of the ingot during hot extrusion. From the viewpoint
of further enhancing the action described above, the total of the Si content and the
Mn content preferably is 3.00 mass% or less.
[0017] In the situation in which the total of the Si content and the Mn content is greater
than 3.20 mass%, there is a risk that it will lead to a decrease in extrudability
during hot extrusion. In addition, in the situation in which the Si content is greater
than or equal to the Mn content, there is a risk that it will become difficult to
precipitate fine Al-Mn-Si-series intermetallic compounds in the ingot, which will
lead to degradation in extrudability. In addition, in this situation, there is a risk
that the extrusion limit speed will tend to decrease, which will lead to a decrease
in manufacturing productivity of the extruded, multi-hole pipe. It is noted that,
when preparing an ingot, in the situation in which the total amount of Mn contained
in the aluminum metal and the aluminum scrap material is less than or equal to the
total amount of Si, the chemical composition can be adjusted by a method such as adding
an intermediate alloy that contains Mn.
· Fe: 0.60 mass% or less
[0018] The ingot may include greater than 0 mass% and 0.60 mass% or less of Fe. Fe is an
element that is contained in aluminum metals, aluminum scrap material, and the like.
In particular, aluminum scrap material contains components composed of Fe-based metals,
and, in situations in which such an aluminum scrap material is used as the casting
material, the Fe content in the ingot tends to become high. By making the Fe content
preferably to be 0.10 mass% or more, more preferably to be 0.15 mass% or more, yet
more preferably to be 0.20 mass% or more, and particularly preferably to be 0.25 mass%
or more, it is possible to make the proportion of the aluminum scrap material in the
casting material even higher.
[0019] On the other hand, if the Fe content becomes excessively high, coarse AlFe-series
intermetallic compounds tend to be formed in the ingot. There is a risk that coarse
AlFe-series intermetallic compounds in the ingot will lead to degradation in the surface
properties of the extruded, multi-hole pipe, such as an increase in surface roughness,
which is not preferable. By making the Fe content to be 0.60 mass% or less and preferably
to be 0.50 mass% or less, degradation in surface properties can be avoided.
· Cu: 0.60 mass% or less
[0020] The ingot may contain greater than 0 mass% and 0.60 mass% or less of Cu. Cu is an
element that is contained in aluminum metals, aluminum scrap material, and the like.
In particular, aluminum scrap material sometimes contains components composed of aluminum
alloys (e.g., 2000-series alloys) that contain a large amount of Cu; in the situation
in which such an aluminum scrap material is used as the casting material, the Cu content
in the ingot tends to become high. Cu acts to increase the natural electric potential
of the extruded, multi-hole pipe, thereby increasing the corrosion resistance of the
extruded, multi-hole pipe. From the viewpoint of further increasing the corrosion
resistance of the extruded, multi-hole pipe, the Cu content preferably is 0.05 mass%
or more, more preferably is 0.10 mass% or more, yet more preferably is 0.15 mass%
or more, and particularly preferably is 0.20 mass% or more. In addition, in this situation,
the proportion of the aluminum scrap material in the casting material can be easily
made even higher.
[0021] On the other hand, when the Cu content becomes excessively high, the amount of the
Cu that has formed a solid solution in the ingot becomes larger, and there is a risk
that this will lead to an increase in the deformation resistance of the ingot during
hot extrusion and thereby a decrease in extrudability. By making the Cu content to
be 0.60 mass% or less and preferably to be 0.40 mass% or less, the corrosion resistance
of the extruded, multi-hole pipe can be increased while curtailing an increase in
the deformation resistance of the ingot during hot extrusion.
· Mg: 0.40 mass% or less
[0022] The ingot may contain greater than 0 mass% and 0.40 mass% or less of Mg. Mg is an
element that is contained in aluminum metals, aluminum scrap material, and the like.
In particular, aluminum scrap material sometimes contains components composed of aluminum
alloys (e.g., 5000-series alloys and 6000-series alloys) that contain a large amount
of Mg; in the situation in which such an aluminum scrap material is used as the casting
material, the Mg content in the ingot tends to become high. Mg acts to increase the
strength of the extruded, multi-hole pipe. From the viewpoint of further increasing
the strength of the extruded, multi-hole pipe, the Mg content preferably is 0.03 mass%
or more, more preferably is 0.05 mass% or more, and yet more preferably is 0.07 mass%
or more. In addition, in this situation, the proportion of the aluminum scrap material
in the casting material can be easily made even higher.
[0023] On the other hand, when the Mg content becomes excessively high, the amount of Mg
that has formed a solid solution in the ingot becomes large, and there is a risk that
this will lead to an increase in the deformation resistance of the ingot during hot
extrusion and thereby a decrease in extrudability. By making the Mg content to be
0.40 mass% or less and preferably to be 0.30 mass% or less, an increase in the deformation
resistance of the ingot during hot extrusion can be curtailed.
· Cr: 0.10 mass% or less
[0024] The ingot may contain greater than 0 mass% and 0.10 mass% or less of Cr. Cr is an
element that is contained in aluminum metals, aluminum scrap material, and the like.
In particular, aluminum scrap material sometimes contains components composed of aluminum
alloys (e.g., 5000-series alloys, 7000-series alloys, and the like) that contain a
large amount of Cr; in the situation in which such an aluminum scrap material is used
as the casting material, the Cr content in the ingot tends to become high. By making
the Cr content preferably to be 0.01 mass% or more, more preferably to be 0.02 mass%
or more, and yet more preferably to be 0.03 mass% or more, the proportion of the aluminum
scrap material in the casting material can be easily made even higher.
[0025] On the other hand, when the Cr content becomes excessively high, coarse AlCr-series
intermetallic compounds tend to form in the ingot. When coarse AlCr-series intermetallic
compounds exist in the ingot, there is a risk that cracks will tend to form during
hot extrusion or during secondary processing after hot extrusion, which is not preferable.
By making the Cr content to be 0.10 mass% or less, the formation of coarse AlCr-series
intermetallic compounds can be avoided.
· Zn: 1.50 mass% or less
[0026] The above-mentioned ingot may contain greater than 0 mass% and 1.50 mass% or less
of Zn. Zn is an element that is contained in aluminum metals, aluminum scrap material,
and the like. In particular, aluminum scrap material sometimes contains components
composed of aluminum alloys (e.g., 7000-series alloys, and the like) that contain
a large amount of Zn; in the situation in which such an aluminum scrap material is
used as the casting material, the Zn content in the ingot tends to become high. Zn
acts to increase corrosion resistance by making the surface oxide film on the extruded,
multi-hole pipe brittle and by distributing the occurrences of pitting corrosion.
From the viewpoint of further enhancing such functions and effects, the Zn content
preferably is 0.05 mass% or more, more preferably is 0.10 mass% or more, and yet more
preferably is 0.15 mass% or more. In addition, in this situation, the proportion of
the aluminum scrap material in the casting material can be easily made even higher.
[0027] On the other hand, when the Zn content becomes excessively high, the solidus temperature
of the aluminum alloy decreases, and consequently there is a risk that partial melting
of the ingot or the extruded, multi-hole pipe will tend to occur during the homogenizing
process or during hot extrusion. By making the Zn content to be 1.50 mass% or less
and preferably to be 1.00 mass% or less, the functions and effects due to Zn can be
obtained while avoiding partial melting of the ingot or the extruded, multi-hole pipe.
· Ti: 0.10 mass% or less
[0028] The above-mentioned ingot may contain greater than 0 mass% and 0.10 mass% or less
of Ti. Ti acts to increase the fineness of the crystal grains in the metallographic
structure of the ingot. From the viewpoint of further enhancing such an effect, the
Ti content preferably is 0.005 mass% or more, more preferably is 0.007 mass% or more,
and yet more preferably is 0.010 mass% or more.
[0029] On the other hand, when the Ti content becomes excessively high, coarse AlTi-series
intermetallic compounds tend to be formed in the ingot. When coarse AlTi-series intermetallic
compounds exist in the ingot, there is a risk that cracks will tend to form during
hot extrusion or during secondary processing after hot extrusion, which is not preferable.
By making the Ti content to be 0.10 mass% or less, the crystal grains in the metallographic
structure of the ingot can be made sufficiently fine while avoiding the formation
of coarse AlTi-series intermetallic compounds.
. B: 0.10 mass% or less
[0030] The above-mentioned ingot may contain greater than 0 mass% and 0.10 mass% or less
of B. By making the B content in the extruded, multi-hole pipe to be within the above-mentioned
specific range, the crystal grains in the metallographic structure of the extruded,
multi-hole pipe can be made sufficiently fine. From the viewpoint of more reliably
obtaining such functions and effects, the B content in the ingot preferably is 0.005
mass% or more and 0.10 mass% or less.
· Other Elements
[0031] The ingot may contain, as unavoidable impurities, elements other than the elements
described above. For example, Zr (zirconium), V (vanadium), etc. can be given as examples
of such elements. The content of the elements existing as unavoidable impurities should
be, for example, 0.05 mass% or less for each element. In addition, the total content
of the elements existing as unavoidable impurities should be 0.50 mass% or less.
[0032] From the viewpoint of more reliably obtaining the effect of increasing extrudability
described above, the ingot preferably has a chemical composition that contains Si:
0.60 mass% or more and 1.40 mass% or less and Mn: 0.80 mass% or more and 1.80 mass%
or less, the remainder being composed of Al and unavoidable impurities, wherein the
total of the Si content and the Mn content is 3.20 mass% or less, and the Si content
is less than the Mn content. In this situation, the ingot may further contain, as
optional components, one or two or more elements selected from the group consisting
of Fe: 0.10 mass% or more and 0.50 mass% or less, Cu: 0.05 mass% or more and 0.40
mass% or less, Mg: 0.05 mass% or more and 0.30 mass% or less, Cr: 0.01 mass% or more
and 0.10 mass% or less, Zn: 0.10 mass% or more and 1.00 mass% or less, Ti: 0.005 mass%
or more and 0.10 mass% or less, and B: 0.005 mass% or more and 0.10 mass% or less.
[0033] From the same viewpoint, the ingot preferably has a chemical composition that essentially
contains Si: 0.70 mass% or more and 1.30 mass% or less, Fe: 0.10 mass% or more and
0.50 mass% or less, Cu: 0.05 mass% or more and 0.40 mass% or less, Mn: 0.90 mass%
or more and 1.70 mass% or less, Mg: 0.05 mass% or more and 0.30 mass% or less, Cr:
0.01 mass% or more and 0.10 mass% or less, Zn: 0.10 mass% or more and 1.00 mass% or
less, Ti: 0.005 mass% or more and 0.10 mass% or less, and B: 0.005 mass% or more and
0.10 mass% or less, the remainder being composed of Al and unavoidable impurities,
wherein the total of the Si content and the Mn content is 3.00 mass% or less, and
the Si content is less than the Mn content.
[0034] In the preparation of the ingot, a well-known casting method, such as DC casting
or CC casting, can be used. For example, aluminum virgin metal, aluminum scrap material,
or the like can be used as the casting material when preparing the ingot.
[0035] In the above-mentioned extruded, multi-hole-pipe manufacturing method, it is preferable
to use aluminum scrap material as at least a portion of the casting material. Here,
end materials and chips produced in manufacturing processes of aluminum products,
used aluminum products, aluminum products that have been separated from used products,
and the like are included in aluminum scrap material.
[0036] As described above, in the situation in which aluminum scrap material is reused as
the casting material, the content of elements other than aluminum becomes high, which
leads to the occurrence of various problems such as an increase in deformation resistance
during hot extrusion and a decrease in extrusion speed. For this reason, in the existing
state of the art, in the situation in which aluminum scrap material is used as the
casting material, it is considered difficult to manufacture an extruded, multi-hole
pipe having a complex, cross-sectional shape.
[0037] In contrast, in the above-mentioned extruded, multi-hole-pipe manufacturing method,
the chemical composition of the ingot is made to be within the above-mentioned specific
ranges, and moreover by performing the homogenizing process in two stages as described
below, an increase in deformation resistance during hot extrusion can be curtailed
even in the situation in which the content of elements other than aluminum is relatively
high. For this reason, according to the method of manufacturing in the above-mentioned
aspect, even in the situation in which aluminum scrap material is used as at least
a portion of the casting material and the content of elements other than aluminum
is relatively high, an extruded, multi-hole pipe having a complex, cross-sectional
shape can be manufactured easily.
[0038] Furthermore, by using aluminum scrap material as at least a portion of the casting
material, the amount of aluminum virgin metal used can be reduced. As a result, the
environmental load can be further reduced in manufacturing processes of extruded,
multi-hole pipes, and the cost of materials of the extruded, multi-hole pipe can be
further lowered. From the viewpoint of further enhancing such effects, the proportion
of the aluminum scrap material in the casting material preferably is made to be 35
mass% or more, more preferably is made to be 45 mass% or more, and particularly preferably
is made to be 60 mass% or more.
[0039] In the above-mentioned extruded, multi-hole-pipe manufacturing method, after the
ingot has been prepared, a first homogenizing process is performed by holding the
ingot at a temperature of 550°C or higher and 650°C or lower for 2 h or more. By setting
the hold temperature and the hold time in the first homogenizing process respectively
to the above-mentioned specific ranges, coarse crystallized products in the ingot
can disintegrate, granulate, and thereby once again form a solid solution in the Al
parent phase.
[0040] From the viewpoint of further promoting the disintegration and the like of crystallized
products in the ingot, it is preferable that the hold temperature in the first homogenizing
process is 580°C or higher and 620°C or lower. From the same viewpoint, it is preferable
that the hold time in the first homogenizing process is 10 h or more. In addition,
the hold time in the first homogenizing process preferably is 24 h or less from the
viewpoint of productivity.
[0041] In the situation in which the hold temperature in the first homogenizing process
is lower than 550°C or in the situation in which the hold time is less than 2 h, there
is a risk that the disintegration and the like of the crystallized products will become
insufficient. In the situation in which the hold temperature in the first homogenizing
process is higher than 650°C, there is a risk that the ingot will partially melt.
[0042] In the above-mentioned extruded, multi-hole-pipe manufacturing method, a second homogenizing
process is performed on the ingot after the first homogenizing process has been performed.
The hold temperature in the second homogenizing process is 450°C or higher and 540°C
or lower, and the hold time is 3 h or more. As described above, the first homogenizing
process is performed for the principal purpose of disintegrating, granulating, and
once again forming a solid solution of the coarse crystallized products that crystallized
in the ingot during casting. However, in the situation in which the hold temperature
and the hold time in the first homogenizing process have been set to within the above-mentioned
specific ranges, the disintegration and granulation of the crystallized products and
the re-forming of a solid solution are promoted, and the formation of a solid solution
of Mn and Si, which are solute elements, in the Al parent phase is also promoted.
When the solid solution amounts of solute elements in the Al parent phase becomes
excessively large, it leads to a decrease in the speed with which dislocations move
in the parent phase during hot extrusion, and thereby deformation resistance tends
to increase.
[0043] In contrast, in the second homogenizing process, when the ingot is heated under the
above-mentioned specific conditions, the Si and Mn that have formed a solid solution
in the Al parent phase in the first homogenizing process can be caused to finely precipitate
as Al-Mn-Si-series intermetallic compounds. As a result, the solid solution amounts
of solute elements in the Al parent phase can be reduced, and thereby deformation
resistance during hot extrusion can be decreased. Accordingly, by performing the second
homogenizing process by heating the ingot, under the above-mentioned specific conditions,
after the first homogenizing process has been performed, extrudability during hot
extrusion can be increased.
[0044] From the viewpoint of further enhancing the effect of increasing extrudability, the
hold temperature in the second homogenizing process preferably is 480°C or higher
and 520°C or lower. From the same viewpoint, the hold time in the second homogenizing
process preferably is 5 h or more. In addition, the hold time in the second homogenizing
process preferably is 24 h or less from the viewpoint of productivity, and more preferably
is 15 h or less.
[0045] In the situation in which the hold temperature in the second homogenizing process
is lower than 450°C, or in the situation in which the hold time is less than 3 h,
there is a risk that the precipitated amount of the Al-Mn-Si-series intermetallic
compounds will tend to become small, which will lead to degradation in extrudability
during hot extrusion. In the situation in which the hold temperature in the second
homogenizing process is higher than 540°C, there is a risk that it will become difficult
for the Si and Mn that have formed a solid solution in the Al parent phase to form
intermetallic compounds, which will lead to degradation in extrudability during hot
extrusion.
[0046] In the above-mentioned manufacturing method, the first homogenizing process and the
second homogenizing process can be performed in series. Here, performing the first
homogenizing process and the second homogenizing process in series means that, after
the first homogenizing process has completed, the temperature of the ingot is lowered
until the hold temperature of the second homogenizing process, and the second homogenizing
process is started at the point in time at which the temperature of the ingot has
reached the hold temperature of the second homogenizing process.
[0047] In the situation in which the first homogenizing process and the second homogenizing
process are performed in series, after the first homogenizing process has been completed,
it is preferable that the above-mentioned ingot is cooled at an average cooling rate
of 20°C/h or more and 60°C/h or less until the hold temperature of the above-mentioned
second homogenizing process.
[0048] In addition, in the above-mentioned manufacturing method, after the first homogenizing
process has been completed, it is also possible to first cool the ingot to a temperature
that is lower than the hold temperature of the second homogenizing process and subsequently
to perform the second homogenizing process. In this situation, the temperature of
the ingot when cooling has completed can be set to, for example, 200°C or lower. When
heating the ingot, after completion of the cooling, to the hold temperature of the
second homogenizing process, it is preferable to heat the ingot at an average temperature-rise
rate of 20°C/h or more and 60°C/h or less to the hold temperature of the second homogenizing
process.
[0049] In the above-mentioned extruded, multi-hole-pipe manufacturing method, by performing
hot extrusion on the ingot after the second homogenizing process has been performed,
the extruded, multi-hole pipe can be obtained. During hot extrusion, the temperature
of the ingot at the start of extrusion, the temperature of the extruded, multi-hole
pipe at the completion of extrusion, and the like should be set as appropriate in
accordance with the chemical composition of the extruded, multi-hole pipe. For example,
the temperature of the ingot at the start of extrusion can be set as appropriate to
within the range of 450°C or higher and 550°C or lower. The extruded, multi-hole pipe
obtained in this manner may be used as is or may be used after the performance of
a postprocess, such as: straightening work for adjusting dimensions, shape, or the
like; cutting; a heat treatment to adjust strength; zinc spraying to increase corrosion
resistance; coating; or the like. These postprocesses can be combined as appropriate
in accordance with the application or the like of the extruded, multi-hole pipe.
[0050] The extruded, multi-hole pipe obtained by the above-mentioned manufacturing method
has: an outer-wall portion, which partitions the exterior space and the interior of
the above-mentioned extruded, multi-hole pipe; and a plurality of partition portions,
which partitions the interior space of the above-mentioned outer-wall portion. In
addition, the extruded, multi-hole pipe has a plurality of passageways that are surrounded
by the outer-wall portion and the partition portions and are configured such that
a liquid, a gas, or the like can be caused to circulate through these passageways.
The cross-sectional shape of the extruded, multi-hole pipe is not particularly limited
and, for example, can take on a variety of cross-sectional shapes such as an elliptical
shape, an oblong shape, and the like. In addition, the cross-sectional shape of the
passageways of the extruded, multi-hole pipe are likewise not particularly limited
and, for example, can take on a variety of cross-sectional shapes such as a circular
shape, a triangular shape, a quadrangular shape, and the like.
[0051] The extruded, multi-hole pipe may have a flat, cross-sectional shape. In this situation,
the width-to-thickness ratio of the extruded, multi-hole pipe can be made to be 2
or more and 50 or less and preferably to be 3 or more and 30 or less. Generally, in
the situation in which the extruded, multi-hole pipe has a flat shape, the higher
the width-to-thickness ratio, the more difficult that extrusion becomes, and the greater
the extrudability that is required. In the process of manufacturing the above-mentioned
extruded, multi-hole pipe, by performing the homogenizing process in two stages on
the aluminum-alloy ingot having the above-mentioned specific chemical composition,
an increase in deformation resistance during hot extrusion can be curtailed, and thereby
extrudability can be increased. For this reason, an extruded, multi-hole pipe having
a cross-sectional shape requiring such great extrudability can be obtained easily.
[0052] In addition, the extruded, multi-hole pipe may have an outer-wall portion, which
partitions the exterior space and the interior of the above-mentioned extruded, multi-hole
pipe, and a plurality of partition portions, which partitions the interior space of
the above-mentioned outer-wall portion, wherein the thickness of the above-mentioned
outer-wall portion and the above-mentioned partition portions may be 0.10 mm or more
and 2.0 mm or less and preferably may be 0.15 mm or more and 1.5 mm or less. In the
extruded, multi-hole pipe, the same as in the width-to-thickness ratio described above,
the thinner the thickness of the outer-wall portion and the partition portions, the
more difficult that extrusion becomes, and the greater the extrudability that is required.
In the process of manufacturing the above-mentioned extruded, multi-hole pipe, by
performing the homogenizing process in two stages on the aluminum-alloy ingot having
the above-mentioned specific chemical composition, an increase in deformation resistance
during hot extrusion can be curtailed, and thereby extrudability can be increased.
For this reason, an extruded, multi-hole pipe having a cross-sectional shape requiring
such great extrudability can be obtained easily.
[Working Examples]
[0053] A working example of the extruded, multi-hole-pipe manufacturing method is explained
below. In the multi-hole-pipe manufacturing method an ingot is prepared having a chemical
composition that contains one or two or more elements selected from the group consisting
of Si: 2.00 mass% or less, Fe: 0.60 mass% or less, Cu: 0.60 mass% or less, Mn: 2.00
mass% or less, Mg: 0.40 mass% or less, Cr: 0.10 mass% or less, Zn: 1.50 mass% or less,
Ti: 0.10 mass% or less, and B: 0.10 mass% or less, the remainder being composed of
Al and unavoidable impurities, wherein the total of the Si content and the Mn content
is 3.20 mass% or less, and the Si content is less than the Mn content. Subsequently,
a first homogenizing process is performed by holding the ingot at a temperature of
550°C or higher and 650°C or lower for 2 h or more. After the first homogenizing process
has completed, a second homogenizing process is performed by holding the ingot at
a temperature of 450°C or higher and 540°C or lower for 3 h or more. Furthermore,
after the second homogenizing process has completed, the extruded, multi-hole pipe
is prepared by performing hot extrusion on the ingot.
[0054] As shown in FIG. 1, an extruded, multi-hole pipe 1 according to the present example
has a flat, cross-sectional shape. More specifically, the extruded, multi-hole pipe
1 has an elliptical, cross-sectional shape. The width of the extruded, multi-hole
pipe 1 is, for example, 14.0 mm, and the thickness is, for example, 2.5 mm.
[0055] In addition, the extruded, multi-hole pipe 1 has an outer-wall portion 11, which
partitions the exterior space and the interior thereof, and partition portions 13,
which partition the space surrounded by the outer-wall portion 11 into nineteen passageways
12. Each of the passageways 12 of the extruded, multi-hole pipe 1 in the present example
has a circular, cross-sectional shape. The thickness of the thinnest portion of the
outer-wall portion 11 and the partition portions 13 is, for example, 0.4 mm.
[0056] Examples of the extruded, multi-hole-pipe manufacturing method according to the present
example are explained more specifically below. First, casting materials containing
aluminum scrap material were used to prepare, by DC casting, ingots having the chemical
compositions (alloy symbols A1-A3) listed in Table 1. It is noted that "Bal." in Table
1 is a notation indicating that that element is the remainder.
[0057] After the ingots had been prepared, a first homogenizing process was performed by
holding the ingots at a temperature of 600°C for 10 h. After the first homogenizing
process completed, a second homogenizing process was performed by holding the ingots
at a temperature of 500°C for 10 h. The first homogenizing process and the second
homogenizing process may be performed in series; or, in the interval from when the
first homogenizing process has completed until the second homogenizing process is
performed, the temperature of the ingots may be lowered below the hold temperature
of the second homogenizing process.
[0058] After the second homogenizing process had completed, the extruded, multi-hole pipes
1 were prepared by performing hot extrusion on the ingots in the state in which the
temperature of the ingots was 500°C. Based on the above, Test Materials S1-S3 listed
in Table 2 could be obtained. It is noted that Test Materials R1-R4 listed in Table
2 were test materials for comparison with Test Materials S1-S3. The method of preparing
Test Materials R1-R3 was the same as that for Test Materials S1-S3, other than that
the chemical compositions of the ingots were changed to Alloy Symbols A4-A6 listed
in Table 1. In addition, the method of preparing Test Material R4 was the same as
for Test Materials S1-S3, other than that the chemical composition of the ingot was
changed to Alloy Symbol A7 listed in Table 1, and that the second homogenizing process
was omitted.
[0059] The method of evaluating the extrudability of each test material is explained below.
· Extrudability
[0060] It was possible to evaluate extrudability based on the external appearance of each
test material. More specifically, the external appearance of each test material was
observed visually, and the presence/absence of cracks, streak patterns along the extrusion
direction, and the like was evaluated. The presence/absence of cracks and streak patterns
at the end portion of each test material is listed in Table 2.
Table 1
| Alloy Symbol |
Chemical Composition (mass%) |
Si + Mn (mass %) |
Relative Amount |
| Si |
Fe |
Mn |
Mg |
Cr |
Zn |
Ti |
Al |
| A1 |
0.98 |
0.29 |
1.49 |
0.10 |
0.05 |
0.23 |
0.05 |
Bal. |
2.47 |
Si < Mn |
| A2 |
1.45 |
0.29 |
1.58 |
0.10 |
0.05 |
0.24 |
0.05 |
Bal. |
3.03 |
Si < Mn |
| A3 |
1.09 |
0.30 |
1.91 |
0.10 |
0.05 |
0.22 |
0.05 |
Bal. |
3.00 |
Si < Mn |
| A4 |
1.31 |
0.30 |
0.99 |
0.10 |
0.05 |
0.26 |
0.05 |
Bal. |
2.30 |
Si > Mn |
| A5 |
1.53 |
0.30 |
1.70 |
0.10 |
0.05 |
0.23 |
0.05 |
Bal. |
3.23 |
Si < Mn |
| A6 |
0.99 |
0.29 |
2.12 |
0.09 |
0.05 |
0.21 |
0.05 |
Bal. |
3.11 |
Si < Mn |
| A7 |
0.98 |
0.29 |
1.49 |
0.10 |
0.05 |
0.23 |
0.05 |
Bal. |
2.47 |
Si < Mn |
Table 2
| Test Material Symbol |
Alloy Symbol |
Second Homogenizing Process |
Extrudability |
| Cracks in End Portion |
Streak Pattern |
| S1 |
Al |
Performed |
None |
None |
| S2 |
A2 |
Performed |
None |
None |
| S3 |
A3 |
Performed |
None |
None |
| R1 |
A4 |
Performed |
None |
Present |
| R2 |
A5 |
Performed |
Present |
Present |
| R3 |
A6 |
Performed |
None |
Present |
| R4 |
A7 |
Not performed |
None |
Present |
[0061] As shown in Table 1 and Table 2, in the process of manufacturing Test Materials S1-S3,
because the first homogenizing process and the second homogenizing process were performed,
under the above-mentioned specific conditions, on the ingots having the above-mentioned
specific chemical compositions, it was possible to decrease the deformation resistance
of each ingot during hot extrusion. For this reason, each of the Test Materials S1-S3
had a satisfactory external appearance.
[0062] On the other hand, with regard to Test Material R1, because the Si content was greater
than or equal to the Mn content, extrudability was poor compared with Test Materials
S 1-S3, and streak patterns occurred on the surface of the test material.
[0063] With regard to Test Material R2, because the total of the Si content and the Mn content
was excessively large, extrudability was poor compared with Test Materials S1-S3,
cracks occurred at the end portion of the test material in the width direction, and
streak patterns occurred on the surface of the test material.
[0064] With regard to Test Material R3, because the Mn content was excessively high, extrudability
was poor compared with Test Materials S1-S3, and streak patterns occurred on the surface
of the test material.
[0065] With regard to Test Material R4, because the second homogenizing process was not
performed in that manufacturing process, extrudability was poor compared with Test
Materials S1-S3, and streak patterns occurred on the surface of the test material.
[0066] Specific aspects of the extruded, multi-hole-pipe manufacturing method according
to the present invention were explained above based on the working examples, but the
specific aspects of the extruded, multi-hole-pipe manufacturing method according to
the present invention are not limited to the aspects of the working examples, and
the composition can be modified as appropriate within a range that does not depart
from the gist of the present invention.