[0001] The present invention relates to casting articles by directional solidification,
a process which is favoured when the article to be produced benefits from having a
particular crystallographic structure/ orientation, e.g. turbine blades.
[0002] In a simple directional solidification casting process, the melt is cooled at a water
cooled copper chill plate where nucleation occurs randomly at first, but which, after
an initial growth zone, develops into a reasonably uniform grain growth pattern. Thus,
a structure is produced composed of a number of crystals having a primary vertical
grain growth direction and a lateral grain growth abutting adjacent crystals to form
finite continuous grain boundaries.
[0003] It has also been proposed to cast articles by directional solidification, as a single,
crystal. This has been carried out by initially employing the copper chill plate to
produce directionally solidified crystals but after the growth zone, the solidification
is forced to take place via a constriction which allows only one crystal to develop
thereby producing a single crystal casting.
[0004] As an alternative method of single crystal casting, it has been proposed to use "seed"
crystals to act as a "starter" for crystal growth in each case. The crystal which
grows from the seed crystal has a crystallographic orientation identical to that of
the seed crystal. Thus, results which are more predictable can be obtained once one
has managed to obtain seed crystals with a known and acceptable crystallographic orientation.
[0005] In each of these proposals, the general objective is to achieve a direction of crystal
growth wherein the primary 001 growth direction of the crystal follows essentially
the major stress axis of the component and for this direction of growth to be generally
axial with respect to the geometry of the article. However, it is suggested by the
applicants that it might be advantageous to employ a crystallographic oreintation
in which the lOO plane of the crystal is inclined to the axis of the article at a
predetermined angle and in a specific direction relative to the component geometry.
It is therefore an object of the present invention to provide a method of producing
a cast article in which the crystallographic orientation of an individual crystal
or crystals within the article relative to its geometry can be accurately predetermined.
[0006] According to the invention there is provided a method for producing a cast article
having a specific crystallographic orientation relative to the goemetry of the article
which comprises: forming a mould, locating relative to the mould cavity a seed crystal
which has been calibrated to determine the angle and direction of inclination of its
100 plane relative to a reference direction, arranging the seed crystal so that the
orientation of its 100 plane coincides with that desired in the article relative to
the geometry of the article, admitting to the mould in the molten state the material
from which the article is to be cast, and cooling the mould so that solidification
of the cast article takes place in a direction away from the seed crystal.
[0007] The seed crystals may be produced by any convenient method, for example by way of
a growth restrictor which may be in a helical form or alternatively by "cloning" from
existing seed crystals. They are preferably calibrated by an X-ray diffraction technique
to determine the angle of inclination of the 100 plane from a reference direction
and the direction of inclination is preferably marked on the seed crystal relative
to a reference line marked along the length of the seed crystal.
[0008] The seed crystal may be located within the mould cavity after the mould has been
completely formed. If the mould is made by a lost-wax process, then the seed crystal
may be located at the wax assembly stage.
[0009] It will be appreciated that, using the method of the invention, it is possible to
incline the 100 plane direction relative to the stress axis in the article to any
desired extent and in any desired direction.
[0010] It is sometimes a requirement in the production of, for example turbine blades, that
the articles produced have a minimum number of grains. While this can generally be
achieved by the simple chill plate directional solidification method, their number
and orientation cannot be accurately predetermined. It is therefore a further object
of the present invention to provide a method of casting an article by directional
solidification in which the number of grains and their crystallographic orientations
can be predetermined with accuracy.
[0011] In a preferred method therefore a plurality of seed crystals are located relative
to the mould cavity and arranged so that the orientation of their 100 planes coincides
with that desired in corresponding crystals making up the article. In this way, it
may be possible to produce an article made up from a specific number of directionally
solidified grains, each having its own optimum crystallographic orientation.
[0012] In all cases, it should be possible to enhance the properties of the article and
in addition, to reduce the percentage of wastage due to unsuitable crystallographic
orientations.
[0013] The invention may be carried into practice in various ways and some embodiments will
now be described by way of example with reference to the accompanying drawings, in
which:-
Figure 1 is a plan view of a seed crystal which has been calibrated;
Figure 2 is an isometric sketch of the seed crystal of Figure 1;
Figure 3 is a diagrammatic representation of the crystallographic orientation of the
seed crystal of Figures 1 and 2;
Figure 4 is an isometric sketch showing the grain growth in a turbine blade produced
from a number of seed crystals; and
Figure 5 is a horizontal section through the turbine blade of Figure 4.
[0014] Figures 1 and 2 show a calibrated seed crystal. The seed crystal is elongate and
cylindrical in shape It has a central axis X-X and a reference line O-O parallel to
X-X inscribed upon its outer surface. The inclination 6 of the 100 plane relative
to the axis X-X and the reference line O-O is determined by an X-ray diffraction technique.
This inclination is indicated by the arrow A. The direction of the inclination of
the 100 plane is indicated by a point Y on the circumference of the seed crystal.
Thus, the 100 plane of the seed crystal is inclined by an angle θ relative to the
X
-X reference axis in a direction towards the point Y from the X-X reference axis. This
is shown schematically in Figure 3 in which the 100 plane of a notional cube is cross-hatched.
[0015] Figure 4 shows the casting of a turbine blade 11. The turbine blade is composed of
six individual metal crystals 12 to 18 each having its 100 plane in a particular desired
orientation. The apparatus used to cast the turbine blade comprises a chill plate
19 having a bayonet fitting 20 and upon which a ceramic mould 21 is located. The mould
may have conveniently been produced by a conventional lost-wax process.
[0016] The mould cavity comprises a starter block 22, above that a blade section 23, and
below the starter block, a seed block 24. A molten alloy inlet 25 leads into the mould
cavity. Alternatively, molten alloy may be introduced through the major mould aeorfoil
cavity or any other suitable direction above the seed crystal or crystals.
[0017] The blade section 23 has a contour which corresponds to the desired contour of the
finished product. The starter block 22 is merely a zone in which crystal growth is
allowed to develop as a result of directional solidification. The seed block 24 comprises
a series of cylindrical bores 32 to 38.
[0018] The bores 32 to 38 are intended to receive seed crystals 42 to 48 which are of the
same alloy as that of the component to be cast and which act as starters for the metal
crystals 13 to 18 making up the final turbine blade. Each bore 32 to 38 is therefore
marked with a point Z with which the corresponding point Y on the appropriate seed
crystal is aligned prior to moulding so that the eventual crystals 13 to 18 have the
desired crystallographic orientation. Each seed crystal 42 to 48 is fixed in position
with the aid of a ceramic air-drying cement. In an alternative method, the seed crystals
42 to 48 can be located in position at the wax assembly stage.
[0019] After the seed crystals 42 to 48 have been correctly positioned, the molten casting
alloy is admitted to the mould cavity via the alloy inlet 25. The seed crystals are
then partially melted back and then directionally solidified grains with the same
crystallographic orientation as the seeds develop growing upwards to the blade section
23 via the starter block.22. The crystallographic orientation of the seed crystals
is reproduced in the crystals making up the solidified casting alloy.
[0020] As can be seen from Figure 5, in this embodiment, the 100 planes of the crystals
making up the blade section 23 are generally inclined towards the convex surface of
the aerofoil section with the exception of the end crystals which lean towards the
component trailing edge and the component leading edge. These directions are indicated
by the arrows A. Naturally, this particular crystallographic orientation is merely
an example and it will be appreciated that any alternative crystallographic orientation
may be achieved if desired, using the same general method, including control of the
relative orientation of crystal to crystal for property optimisation and grain boundary
defect minimisation.
1. A method for producing a cast article (11) having a specific crystallographic orientation
relative to the geometry of the article which comprises; forming a mould (21), locating
relative to the mould cavity aseed crystal (43); admitting to the mould (21) in the molten state the material from which
the article is to be cast, and cooling the mould (21) so that solidification of the
cast article (11) takes place in a direction away from the seed crystal (13), characterised
in that the seed crystal (43) has been calibrated to determine the angle and direction
of inclination of its 100 plane relative to a reference direction and by arranging
the seed crystal (43) so that the orientation of its 100 plane coincides with that
desired in the article (11) relative to the geometry of the article (11).
2. A method as claimed in Claim 1 characterised in that the seed crystal (43) is located
within the mould cavity after the mould has been completely formed.
3. A method as claimed in Claim 1 characterised in that the mould is made by a lost-wax
process and the seed crystal (43) is located at the wax assembly stage.
4. A method as claimed in any preceding claim characterised in that a plurality of
seed crystals (43 to 48) are located relative to the mould cavity and arranged so
that the orientation of each of their 100 planes coincides with that desired in corresponding
crystals (13 to 18) making up the article (11).
5. A method as claimed in Claim 4 characterised in that the mould includes a seed
section (24) comprising a series of bores (32 to 38) for the location of the seed
crystals (42 to 48) and the molten material is brought into contact with the seed
crystals (42 to 48) in the bores (32 to 58).
6. A method as claimed in Claim 5 characterised in that the mould includes a starter
section (22) between the seed section (24) and the section (23) in which the final
article (11) is to be cast, in which starter section (22) solidification takes place
prior to casting of the final article (11).
7. A method as claimed in Claim 6 characterised in that the calibration of the seed
crystals (42 to 48) includes marking a point (Y) on each crystal (42 to 48) corresponding
to the direction of inclination of its 100 plane, marking a point (Z) on each bore
(32 to 38) corresponding to the desired direction of crystallographic inclination
and aligning the points (Y) on seed crystals (42 to 48) with the points (Z) on the
bores.